A review on phase-inversion technique-based polymer microsphere fabrication

In this review, the preparation method of polymer microspheres (MCs) by phase-inversion is addressed and discussed in detail. An interesting advantage of MCs prepared by the PI method is tailor-made morphology that is a critical factor in separation/adsorption/transport systems. This is relevant sin...

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Published inColloid and interface science communications Vol. 40; p. 100329
Main Authors Duraikkannu, Shanthana Lakshmi, Castro-Muñoz, Roberto, Figoli, Alberto
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.01.2021
Subjects
Absorbent
Emulsification
Membrane
Microspheres
Phase-inversion
Absorbent
PSF
PLA
Emulsification
PU
EIPS
Phase-inversion
SPG
BMIM
PSt
Microspheres
AOA
PLGA
MC
O/W
PEEKWC
Membrane
PI
NIPS
PIT
VIPS
PES
TIPS
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Abstract In this review, the preparation method of polymer microspheres (MCs) by phase-inversion is addressed and discussed in detail. An interesting advantage of MCs prepared by the PI method is tailor-made morphology that is a critical factor in separation/adsorption/transport systems. This is relevant since MCs are useful storage device to load chemical, biological components (e.g. drug, enzyme, antioxidant, among others) for physiological and environmental pollution control applications (towards metal ions/organic moieties from different effluents). Different parameters have been reviewed, such as preparation mechanism, the effect of loading material used (e.g. chemical and biomaterials) and their morphologies. Microsized range polymeric materials have been identified as the most suitable in several high-end applications, where the main requirement is a high active surface area and inert host polymer matrix. Several conventional techniques (physical and chemical) have been explored for MCs preparation, as well as the most used structured materials for valuable and sensitive components loading. The current review also compiles the phase-inversion (PI) methodology, as well-adopted membrane preparation protocol, for MCs preparation and the main parameters that influence in their size, shape and loading concentration. Special attention has been given to summarize the MCs (mimic membrane morphology) preparation and its application carried out at ITM-CNR in last decade. [Display omitted] •Assessment of different approaches for microsphere preparation.•Critical review for microsphere fabrication by phase-inversion (PI) technique•Synthetic polymer-based microsphere structure (mimic membranes), shape and nature depend on PI conditions involved•Polymer dope solution physical properties (viscosity, density, etc.,) influence the MC cross section structures
AbstractList In this review, the preparation method of polymer microspheres (MCs) by phase-inversion is addressed and discussed in detail. An interesting advantage of MCs prepared by the PI method is tailor-made morphology that is a critical factor in separation/adsorption/transport systems. This is relevant since MCs are useful storage device to load chemical, biological components (e.g. drug, enzyme, antioxidant, among others) for physiological and environmental pollution control applications (towards metal ions/organic moieties from different effluents). Different parameters have been reviewed, such as preparation mechanism, the effect of loading material used (e.g. chemical and biomaterials) and their morphologies. Microsized range polymeric materials have been identified as the most suitable in several high-end applications, where the main requirement is a high active surface area and inert host polymer matrix. Several conventional techniques (physical and chemical) have been explored for MCs preparation, as well as the most used structured materials for valuable and sensitive components loading. The current review also compiles the phase-inversion (PI) methodology, as well-adopted membrane preparation protocol, for MCs preparation and the main parameters that influence in their size, shape and loading concentration. Special attention has been given to summarize the MCs (mimic membrane morphology) preparation and its application carried out at ITM-CNR in last decade. [Display omitted] •Assessment of different approaches for microsphere preparation.•Critical review for microsphere fabrication by phase-inversion (PI) technique•Synthetic polymer-based microsphere structure (mimic membranes), shape and nature depend on PI conditions involved•Polymer dope solution physical properties (viscosity, density, etc.,) influence the MC cross section structures
ArticleNumber 100329
Author Duraikkannu, Shanthana Lakshmi
Castro-Muñoz, Roberto
Figoli, Alberto
Author_xml – sequence: 1
  givenname: Shanthana Lakshmi
  orcidid: 0000-0002-0158-3864
  surname: Duraikkannu
  fullname: Duraikkannu, Shanthana Lakshmi
  email: shans@uoalkitab.edu.iq, lakshaluv@gmail.com
  organization: Institute on Membrane Technology, ITM-CNR, University of Calabria, Via P. Bucci 17/C, Rende 87030, CS, Italy
– sequence: 2
  givenname: Roberto
  surname: Castro-Muñoz
  fullname: Castro-Muñoz, Roberto
  organization: Tecnologico de Monterrey, Campus Toluca. Av. Eduardo, Monroy Cárdenas 2000, San Antonio Buenavista, Toluca de Lerdo 50110, Mexico
– sequence: 3
  givenname: Alberto
  surname: Figoli
  fullname: Figoli, Alberto
  organization: Institute on Membrane Technology, ITM-CNR, University of Calabria, Via P. Bucci 17/C, Rende 87030, CS, Italy
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Keywords Absorbent
PSF
PLA
Emulsification
PU
EIPS
Phase-inversion
SPG
BMIM
PSt
Microspheres
AOA
PLGA
MC
O/W
PEEKWC
Membrane
PI
NIPS
PIT
VIPS
PES
TIPS
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Snippet In this review, the preparation method of polymer microspheres (MCs) by phase-inversion is addressed and discussed in detail. An interesting advantage of MCs...
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SubjectTerms Absorbent
Emulsification
Membrane
Microspheres
Phase-inversion
Title A review on phase-inversion technique-based polymer microsphere fabrication
URI https://dx.doi.org/10.1016/j.colcom.2020.100329
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