Lead-free perovskite Cs2XCl6 (X = Hf, Zr, Te) microcrystals for photocatalytic CO2 reduction

The lead halide perovskites have broad application prospects in the fields of optoelectronics and photocatalysis. However, their toxicity and limited stability are the main obstacles restricting their large-scale photocatalytic applications. In order to solve these problems, a set of lead-free stabl...

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Published inMaterials today energy Vol. 28; p. 101067
Main Authors Tian, Changqing, Huang, Qiang, Wu, Daofu, Lai, Junan, Qi, Fei, Zhang, Nan, Zhang, Wenxia, Tang, Xiaosheng
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.08.2022
Subjects
CO2 reduction
Cs2XCl6
Double perovskite
Lead-free
Photocatalytic
Double perovskite
Photocatalytic
CO2 reduction
Lead-free
Cs2XCl6
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Abstract The lead halide perovskites have broad application prospects in the fields of optoelectronics and photocatalysis. However, their toxicity and limited stability are the main obstacles restricting their large-scale photocatalytic applications. In order to solve these problems, a set of lead-free stable Cs2XCl6 (X = Hf, Zr, Te) perovskite microcrystals were synthesized via a solvothermal solution. For the first time, the Cs2XCl6 (X = Hf, Zr, Te) perovskite microcrystals were employed as efficient photocatalysts for the conversion of CO2 into CO and CH4. Among them, the Cs2TeCl6 microcrystals showed the best photocatalytic performance under light irradiation for 3 h, while the yields of CO and CH4 were 284.4 μmol/g and 48.96 μmol/g respectively. Our strategy may provide a new idea for the CO2 photoreduction based on lead-free halide perovskites. [Display omitted] •Lead-free Cs2XCl6 (X = Hf, Zr, Te) perovskites were first applied to CO2 photocatalytic field.•The Cs2XCl6 (X = Hf, Zr, Te) perovskites exhibited excellent stability under continuous illumination, constant heating, and air conditions.•The Cs2TeCl6 microcrystals showed the best photocatalytic performance.
AbstractList The lead halide perovskites have broad application prospects in the fields of optoelectronics and photocatalysis. However, their toxicity and limited stability are the main obstacles restricting their large-scale photocatalytic applications. In order to solve these problems, a set of lead-free stable Cs2XCl6 (X = Hf, Zr, Te) perovskite microcrystals were synthesized via a solvothermal solution. For the first time, the Cs2XCl6 (X = Hf, Zr, Te) perovskite microcrystals were employed as efficient photocatalysts for the conversion of CO2 into CO and CH4. Among them, the Cs2TeCl6 microcrystals showed the best photocatalytic performance under light irradiation for 3 h, while the yields of CO and CH4 were 284.4 μmol/g and 48.96 μmol/g respectively. Our strategy may provide a new idea for the CO2 photoreduction based on lead-free halide perovskites. [Display omitted] •Lead-free Cs2XCl6 (X = Hf, Zr, Te) perovskites were first applied to CO2 photocatalytic field.•The Cs2XCl6 (X = Hf, Zr, Te) perovskites exhibited excellent stability under continuous illumination, constant heating, and air conditions.•The Cs2TeCl6 microcrystals showed the best photocatalytic performance.
ArticleNumber 101067
Author Tian, Changqing
Huang, Qiang
Lai, Junan
Zhang, Nan
Tang, Xiaosheng
Wu, Daofu
Zhang, Wenxia
Qi, Fei
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Keywords Double perovskite
Photocatalytic
CO2 reduction
Lead-free
Cs2XCl6
Language English
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Snippet The lead halide perovskites have broad application prospects in the fields of optoelectronics and photocatalysis. However, their toxicity and limited stability...
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StartPage 101067
SubjectTerms CO2 reduction
Cs2XCl6
Double perovskite
Lead-free
Photocatalytic
Title Lead-free perovskite Cs2XCl6 (X = Hf, Zr, Te) microcrystals for photocatalytic CO2 reduction
URI https://dx.doi.org/10.1016/j.mtener.2022.101067
Volume 28
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