Synthesis of crystalline graphite from disordered graphite by acoustic shock waves: Hot-spot nucleation approach
[Display omitted] •Shock wave induced disorder into order graphite structure is reported.•The control and 750 shocked ID/IG ratio values are 0.709 and 0.251.•The correlation of the magnetic properties and degree of crystalline nature is discussed.•The proposed technique is highly suitable for the sy...
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| Published in | Applied surface science Vol. 655; p. 159632 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.05.2024
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| Subjects | |
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| Abstract | [Display omitted]
•Shock wave induced disorder into order graphite structure is reported.•The control and 750 shocked ID/IG ratio values are 0.709 and 0.251.•The correlation of the magnetic properties and degree of crystalline nature is discussed.•The proposed technique is highly suitable for the synthesis of large-scale crystalline graphite.
The existence of the long-range order under extreme conditions is a highly unusual structural concept that remains one of the top-class fundamental questions for every high-pressure researcher to resolve. In the present study, it is probably the first time that we report the acoustical shock wave-induced conversion from disordered graphite (ID/IG- 0.709) to highly-ordered graphite (ID/IG- 0.251) at the 750-shocked condition and the obtained long-range ordering is comprehensively examined by a few representative microscopic observations which include the Raman spectroscopy, photoelectric X-ray spectrometry and transmission electronic microscopy. Furthermore, the shock wave-induced hot-spot nucleation mechanism for the graphitization is put forward in combination with the outcome of the obtained magnetic, electrical and thermal experimental data. All of these acquired results clearly demonstrate that by using the acoustical shock waves, it is possible to provide one distinctive insight into deeply disclosing the large-scale synthesis of crystalline graphite, which has the potential to be utilized extensively in future commercial applications. |
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| AbstractList | [Display omitted]
•Shock wave induced disorder into order graphite structure is reported.•The control and 750 shocked ID/IG ratio values are 0.709 and 0.251.•The correlation of the magnetic properties and degree of crystalline nature is discussed.•The proposed technique is highly suitable for the synthesis of large-scale crystalline graphite.
The existence of the long-range order under extreme conditions is a highly unusual structural concept that remains one of the top-class fundamental questions for every high-pressure researcher to resolve. In the present study, it is probably the first time that we report the acoustical shock wave-induced conversion from disordered graphite (ID/IG- 0.709) to highly-ordered graphite (ID/IG- 0.251) at the 750-shocked condition and the obtained long-range ordering is comprehensively examined by a few representative microscopic observations which include the Raman spectroscopy, photoelectric X-ray spectrometry and transmission electronic microscopy. Furthermore, the shock wave-induced hot-spot nucleation mechanism for the graphitization is put forward in combination with the outcome of the obtained magnetic, electrical and thermal experimental data. All of these acquired results clearly demonstrate that by using the acoustical shock waves, it is possible to provide one distinctive insight into deeply disclosing the large-scale synthesis of crystalline graphite, which has the potential to be utilized extensively in future commercial applications. |
| ArticleNumber | 159632 |
| Author | Sivakumar, Aswathappa Eniya, Palaniyasan Dai, Lidong Martin Britto Dhas, S.A Almansour, Abdulrahman I. Sahaya Jude Dhas, S Suresh Kumar, Raju |
| Author_xml | – sequence: 1 givenname: Aswathappa orcidid: 0000-0002-3640-2031 surname: Sivakumar fullname: Sivakumar, Aswathappa organization: Key Laboratory of High-temperature and High-Pressure Study of the Earth’s Interior, Institute of Geochemistry, Chinese Academy of Sciences, Guiyang, Guizhou 550081, China – sequence: 2 givenname: Lidong orcidid: 0000-0002-9081-765X surname: Dai fullname: Dai, Lidong email: dailidong@vip.gyig.ac.cn organization: Key Laboratory of High-temperature and High-Pressure Study of the Earth’s Interior, Institute of Geochemistry, Chinese Academy of Sciences, Guiyang, Guizhou 550081, China – sequence: 3 givenname: S surname: Sahaya Jude Dhas fullname: Sahaya Jude Dhas, S organization: Saveetha School of Engineering, Saveetha Institute of Medical and Technical Sciences, Saveetha University, Chennai, Tamil Nadu 602105, India – sequence: 4 givenname: S.A surname: Martin Britto Dhas fullname: Martin Britto Dhas, S.A organization: Shock Wave Research Laboratory, Department of Physics, Abdul Kalam Research Center, Sacred Heart College, Tirupattur, Tamil Nadu 635 601, India – sequence: 5 givenname: Palaniyasan orcidid: 0000-0003-3156-9657 surname: Eniya fullname: Eniya, Palaniyasan organization: Department of Physics, Periyar University, Salem 636011, Tamil Nadu, India – sequence: 6 givenname: Raju surname: Suresh Kumar fullname: Suresh Kumar, Raju organization: Department of Chemistry, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia – sequence: 7 givenname: Abdulrahman I. surname: Almansour fullname: Almansour, Abdulrahman I. organization: Department of Chemistry, College of Science, King Saud University, P.O. Box 2455, Riyadh 11451, Saudi Arabia |
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| Title | Synthesis of crystalline graphite from disordered graphite by acoustic shock waves: Hot-spot nucleation approach |
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