Electrochemical activation of graphite electrode for nitrate reduction: Energetic performance and application potential
Electrocatalysis is a potential technology to remove nitrate from wastewater. However, developing an efficient electrode with long-term stability is still a great challenge. Herein, we reported a facile electrochemical activation method to improve nitrate reduction ability of graphite electrodes. Re...
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| Published in | Applied catalysis. B, Environmental Vol. 329; p. 122553 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.07.2023
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| Abstract | Electrocatalysis is a potential technology to remove nitrate from wastewater. However, developing an efficient electrode with long-term stability is still a great challenge. Herein, we reported a facile electrochemical activation method to improve nitrate reduction ability of graphite electrodes. Results of cyclic voltammetry and electrochemical impedance spectroscopy showed that the nitrate reduction activity was enhanced and the solid-liquid interfacial resistance was decreased. The activated electrode displayed nitrate reduction rate of 0.0409 min−1, which was 10.8 times that of pristine graphite and closed to Fe and Cu electrodes. Furthermore, taking solution including 50.0 mg/L nitrate-N as target, the activated electrode performed above 90.0 % of nitrate removal during 81 days of continuous running. When activated graphite electrode was enlarged to 2500.0 cm2, its performance in nitrate reduction was maintained well. These results suggested electrochemical activated graphite electrode was a promising alternative in the real application of nitrate removal from water and wastewater.
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•An electrochemical reduction method was used to activate graphite electrode.•Activated graphite electrode reduced solid-liquid interfacial resistance and increased the defect content.•The nitrate reduction rate of the activated graphite electrode was close to those of metal electrodes.•The activated graphite electrode showed satisfactory stability and scale-up potential. |
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| AbstractList | Electrocatalysis is a potential technology to remove nitrate from wastewater. However, developing an efficient electrode with long-term stability is still a great challenge. Herein, we reported a facile electrochemical activation method to improve nitrate reduction ability of graphite electrodes. Results of cyclic voltammetry and electrochemical impedance spectroscopy showed that the nitrate reduction activity was enhanced and the solid-liquid interfacial resistance was decreased. The activated electrode displayed nitrate reduction rate of 0.0409 min−1, which was 10.8 times that of pristine graphite and closed to Fe and Cu electrodes. Furthermore, taking solution including 50.0 mg/L nitrate-N as target, the activated electrode performed above 90.0 % of nitrate removal during 81 days of continuous running. When activated graphite electrode was enlarged to 2500.0 cm2, its performance in nitrate reduction was maintained well. These results suggested electrochemical activated graphite electrode was a promising alternative in the real application of nitrate removal from water and wastewater.
[Display omitted]
•An electrochemical reduction method was used to activate graphite electrode.•Activated graphite electrode reduced solid-liquid interfacial resistance and increased the defect content.•The nitrate reduction rate of the activated graphite electrode was close to those of metal electrodes.•The activated graphite electrode showed satisfactory stability and scale-up potential. |
| ArticleNumber | 122553 |
| Author | Kang, Wenda Li, Zhangliang Wu, Shuai Yu, Hongtao Tang, Jiahao Yan, Liming |
| Author_xml | – sequence: 1 givenname: Wenda surname: Kang fullname: Kang, Wenda organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 2 givenname: Liming surname: Yan fullname: Yan, Liming organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 3 givenname: Jiahao surname: Tang fullname: Tang, Jiahao organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 4 givenname: Shuai surname: Wu fullname: Wu, Shuai organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 5 givenname: Hongtao surname: Yu fullname: Yu, Hongtao email: yuhongtao@dlut.edu.cn organization: Key Laboratory of Industrial Ecology and Environmental Engineering (Ministry of Education), School of Environmental Science and Technology, Dalian University of Technology, Dalian 116024, China – sequence: 6 givenname: Zhangliang surname: Li fullname: Li, Zhangliang email: ptulizhangliang@126.com organization: Fujian Provincial Key Laboratory of Ecology-Toxicological Effects & Control for Emerging Contaminants, College of Environmental and Biological Engineering, Putian University, Putian 351100, China |
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| Keywords | Graphite electrode Stability Electrochemical activation Scale-up application Nitrate reduction |
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