Mechanistic investigation of defect-engineered, non-stoichiometric, and Morphology-regulated hierarchical rhombus-/spindle-/peanut-like ZnCo2O4 microstructures and their applications toward high-performance supercapacitors
Formation Mechanism of Rhombus-, Spindle-, and Peanut-Like Self-Assemblies of Zinc Cobalt Oxide Microstructures were Engineered through Solvothermal Synthesis Method. And Their Non-Stoichiometric such as Cation-Deficient (Zn ions)/Excess (Co ions)-Dependent Enhanced Specific Capacitance was Examined...
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Published in | Applied surface science Vol. 529; p. 147123 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.11.2020
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Abstract | Formation Mechanism of Rhombus-, Spindle-, and Peanut-Like Self-Assemblies of Zinc Cobalt Oxide Microstructures were Engineered through Solvothermal Synthesis Method. And Their Non-Stoichiometric such as Cation-Deficient (Zn ions)/Excess (Co ions)-Dependent Enhanced Specific Capacitance was Examined for Supercapacitors.
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•Self-assembled hierarchical rhombus-, spindle-, and peanut-like ZnCo2O4 microstructures were engineered.•A mechanistic study of the precursor concentration-dependent ZCO was studied.•Cation defect-mediated (Zn/Co ions) electrochemical performance of the ZCO was examined.•Peanut-like ZCO has a high surface area 70.04 m2 g−1 and a specific capacitance of 1608.95F g−1 at 0.35 A g−1.
Self-assembled hierarchical rhombus-, spindle-, and peanut-like zinc cobaltite (ZnCo2O4, ZCO) microstructures have strategically engineered using an effective solvothermal approach. The various morphology-regulated ZCO samples have obtained by altering the concentration of precursors in the solvent. Effective strategic methods led to various regulated morphologies, as well as different physicochemical properties, such as the surface area/pore size/volume, crystalline nature, and non-stoichiometry of Zn and Co in the ZCO samples. The metal (Zn/Co)/O deficiencies have quantitatively estimated via X-ray photoelectron spectroscopy and confirmed by the Rietveld refinement of ZCO samples using X-ray diffraction data. A mechanistic study has performed to investigate the formation mechanism of the precursor concentration-dependent self-assembled ZCO microstructures. We demonstrate that the specific capacitance of ZCO has proportional to the Zn-deficiency/Co-excess. The Co-deficient-dependent electrochemical properties have studied for three samples and a decline in the following order: P-ZCO (1608.95 F g−1 at 0.35 A g−1) > S-ZCO (1007.48 F g−1 at 0.35 A g−1) > R-ZCO (629.05 F g−1 at 0.35 A g−1). The simple and inexpensive method of synthesized non-stoichiometric ternary metal oxides micro/nanostructures will introduce new directions in this emerging energy field. |
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AbstractList | Formation Mechanism of Rhombus-, Spindle-, and Peanut-Like Self-Assemblies of Zinc Cobalt Oxide Microstructures were Engineered through Solvothermal Synthesis Method. And Their Non-Stoichiometric such as Cation-Deficient (Zn ions)/Excess (Co ions)-Dependent Enhanced Specific Capacitance was Examined for Supercapacitors.
[Display omitted]
•Self-assembled hierarchical rhombus-, spindle-, and peanut-like ZnCo2O4 microstructures were engineered.•A mechanistic study of the precursor concentration-dependent ZCO was studied.•Cation defect-mediated (Zn/Co ions) electrochemical performance of the ZCO was examined.•Peanut-like ZCO has a high surface area 70.04 m2 g−1 and a specific capacitance of 1608.95F g−1 at 0.35 A g−1.
Self-assembled hierarchical rhombus-, spindle-, and peanut-like zinc cobaltite (ZnCo2O4, ZCO) microstructures have strategically engineered using an effective solvothermal approach. The various morphology-regulated ZCO samples have obtained by altering the concentration of precursors in the solvent. Effective strategic methods led to various regulated morphologies, as well as different physicochemical properties, such as the surface area/pore size/volume, crystalline nature, and non-stoichiometry of Zn and Co in the ZCO samples. The metal (Zn/Co)/O deficiencies have quantitatively estimated via X-ray photoelectron spectroscopy and confirmed by the Rietveld refinement of ZCO samples using X-ray diffraction data. A mechanistic study has performed to investigate the formation mechanism of the precursor concentration-dependent self-assembled ZCO microstructures. We demonstrate that the specific capacitance of ZCO has proportional to the Zn-deficiency/Co-excess. The Co-deficient-dependent electrochemical properties have studied for three samples and a decline in the following order: P-ZCO (1608.95 F g−1 at 0.35 A g−1) > S-ZCO (1007.48 F g−1 at 0.35 A g−1) > R-ZCO (629.05 F g−1 at 0.35 A g−1). The simple and inexpensive method of synthesized non-stoichiometric ternary metal oxides micro/nanostructures will introduce new directions in this emerging energy field. |
ArticleNumber | 147123 |
Author | Rajavaram, Ramaraghavulu Nagajyothi, P.C. Dillip, G.R. Raju, B. Deva Prasad Reddy, G. Rajasekhara Shim, J. Sreekanth, T.V.M. |
Author_xml | – sequence: 1 givenname: G. Rajasekhara surname: Reddy fullname: Reddy, G. Rajasekhara organization: Department of Instrumentation, Sri Venkateswara University, Tirupati 517502, India – sequence: 2 givenname: G.R. surname: Dillip fullname: Dillip, G.R. email: dillipgr@iisc.ac.in organization: Solid State and Structural Chemistry Unit, Indian Institute of Science, Bengaluru 560012, India – sequence: 3 givenname: T.V.M. surname: Sreekanth fullname: Sreekanth, T.V.M. organization: School of Mechanical Engineering, Yeungnam University, Gyeongsan 38541, Republic of Korea – sequence: 4 givenname: Ramaraghavulu surname: Rajavaram fullname: Rajavaram, Ramaraghavulu organization: Department of Humanities and Sciences, Annamacharya Institute of Technology & Sciences, Rajampet, Kadapa 516126, India – sequence: 5 givenname: B. Deva Prasad surname: Raju fullname: Raju, B. Deva Prasad email: drdevaprasadraju@gmail.com organization: Department of Physics, Sri Venkateswara University, Tirupati 517502, India – sequence: 6 givenname: P.C. surname: Nagajyothi fullname: Nagajyothi, P.C. email: nagajyothi@ynu.ac.kr organization: School of Mechanical Engineering, Yeungnam University, Gyeongsan 38541, Republic of Korea – sequence: 7 givenname: J. surname: Shim fullname: Shim, J. organization: School of Mechanical Engineering, Yeungnam University, Gyeongsan 38541, Republic of Korea |
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Keywords | Supercapacitors Hierarchical ZnCo2O4 microstructures Non-stoichiometry Solvothermal method X-ray photoelectron spectroscopy |
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