Theoretical and experimental investigation of four ionic liquids for their ability to prevent carbon steel corrosion in 1 M HCl

•Four ionic liquids have been investigated as corrosion inhibitors in acidic solution.•The new ionic liquids are potent mixed corrosion inhibitors.•Langmuir model accurately defined their adsorption on a steel substrate.•Ionic liquid inhibition effectiveness increases with the rising temperature.•NO...

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Published inJournal of molecular liquids Vol. 349; p. 118414
Main Authors Deyab, M.A., Nessim, M.I., Haikal, Abdelfattah, Mohsen, Q., Khalil, N.A.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.03.2022
Subjects
Acid solution
Adsorption
Cations part
Corrosion
Imidazolium
Ionic liquids
Ionic liquids
Imidazolium
Cations part
Corrosion
Adsorption
Acid solution
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Abstract •Four ionic liquids have been investigated as corrosion inhibitors in acidic solution.•The new ionic liquids are potent mixed corrosion inhibitors.•Langmuir model accurately defined their adsorption on a steel substrate.•Ionic liquid inhibition effectiveness increases with the rising temperature.•NO2 group has a negative effect on the adsorption of ionic liquid molecules. The inhibitory mechanism of four ionic liquids (ILs) generated from imidazolium is reported in this study. The goal of the research was to see how the cation structure of ILs affected the corrosion inhibition of carbon steel in 1 M HCl. The chemical structure of ILs was verified by elements analysis, Fourier-transform-infrared (FTIR), thermo gravimetric (TGA), nuclearmagnetic resonance (1HNMR, D2O, 13C NMR) and hetero-nuclear single-quantum correlation (HSQC). The inhibitory efficiency was measured using mass loss and electrochemical tests and varied from 62.5% to 97.2%. The Langmuir model accurately defined their adsorption on a steel substrate. Adsorption of novel ILs on steel substrates is a mixed physisorption and chemisorption method. To ensure the mechanism of adsorption of current ionic liquids, FTIR and ultraviolet (UV) spectra were employed.
AbstractList •Four ionic liquids have been investigated as corrosion inhibitors in acidic solution.•The new ionic liquids are potent mixed corrosion inhibitors.•Langmuir model accurately defined their adsorption on a steel substrate.•Ionic liquid inhibition effectiveness increases with the rising temperature.•NO2 group has a negative effect on the adsorption of ionic liquid molecules. The inhibitory mechanism of four ionic liquids (ILs) generated from imidazolium is reported in this study. The goal of the research was to see how the cation structure of ILs affected the corrosion inhibition of carbon steel in 1 M HCl. The chemical structure of ILs was verified by elements analysis, Fourier-transform-infrared (FTIR), thermo gravimetric (TGA), nuclearmagnetic resonance (1HNMR, D2O, 13C NMR) and hetero-nuclear single-quantum correlation (HSQC). The inhibitory efficiency was measured using mass loss and electrochemical tests and varied from 62.5% to 97.2%. The Langmuir model accurately defined their adsorption on a steel substrate. Adsorption of novel ILs on steel substrates is a mixed physisorption and chemisorption method. To ensure the mechanism of adsorption of current ionic liquids, FTIR and ultraviolet (UV) spectra were employed.
ArticleNumber 118414
Author Nessim, M.I.
Mohsen, Q.
Deyab, M.A.
Haikal, Abdelfattah
Khalil, N.A.
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  organization: Egyptian Petroleum Research Institute (EPRI), Nasr City, Cairo, Egypt
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CitedBy_id crossref_primary_10_1038_s41598_024_61368_w
crossref_primary_10_1016_j_colsurfa_2023_132720
crossref_primary_10_1016_j_sajce_2023_07_008
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Keywords Ionic liquids
Imidazolium
Cations part
Corrosion
Adsorption
Acid solution
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Snippet •Four ionic liquids have been investigated as corrosion inhibitors in acidic solution.•The new ionic liquids are potent mixed corrosion inhibitors.•Langmuir...
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SubjectTerms Acid solution
Adsorption
Cations part
Corrosion
Imidazolium
Ionic liquids
Title Theoretical and experimental investigation of four ionic liquids for their ability to prevent carbon steel corrosion in 1 M HCl
URI https://dx.doi.org/10.1016/j.molliq.2021.118414
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