Thermal behaviour study of some sol-gel iron-silica nanocomposites
Two series of nanocomposites from the FexOy-SiO2 system, containing 20 mass% iron oxide were prepared by the alkoxide route of the sol-gel method, in the absence and presence of catalyst. The silica gel has been obtained using tetraethoxysilane. The iron(III) nitrate nonahydrate has been used as iro...
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Published in | Journal of thermal analysis and calorimetry Vol. 88; no. 1; pp. 163 - 169 |
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Main Authors | , , , , , , , |
Format | Conference Proceeding Journal Article |
Language | English |
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Dordrecht
Springer
01.04.2007
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Abstract | Two series of nanocomposites from the FexOy-SiO2 system, containing 20 mass% iron oxide were prepared by the alkoxide route of the sol-gel method, in the absence and presence of catalyst. The silica gel has been obtained using tetraethoxysilane. The iron(III) nitrate nonahydrate has been used as iron oxides source. The samples have been prepared in identical conditions, differing only by the gelation times, induced by different surface of evaporation/volume (S/V) ratios of sol let to gelify. Thermal analysis data have established the thermal treatments conditions of the prepared samples and were correlated with X-ray diffraction, IR spectroscopy and TEM results, in order to accomplish a complete structural characterization. The correlation between the structural modifications of the FexOy-SiO2 nanocomposites and different conditions of drying has been established. |
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AbstractList | Two series of nanocomposites from the FexOy-SiO2 system, containing 20 mass% iron oxide were prepared by the alkoxide route of the sol-gel method, in the absence and presence of catalyst. The silica gel has been obtained using tetraethoxysilane. The iron(III) nitrate nonahydrate has been used as iron oxides source. The samples have been prepared in identical conditions, differing only by the gelation times, induced by different surface of evaporation/volume (S/V) ratios of sol let to gelify. Thermal analysis data have established the thermal treatments conditions of the prepared samples and were correlated with X-ray diffraction, IR spectroscopy and TEM results, in order to accomplish a complete structural characterization. The correlation between the structural modifications of the FexOy-SiO2 nanocomposites and different conditions of drying has been established. |
Author | CRISAN, D MADARASZ, J BRAILEANU, Ana POKOL, G CRISAN, M RAILEANU, M BIRJEGA, R MARINESCU, V. E |
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Keywords | Thermogravimetry iron-silica nanocomposites Transition metal Differential thermal analysis Iron Nanostructure X ray diffraction Silica Composite material Surface structure Infrared spectrometry Transmission electron microscopy Sol gel process Morphology Nanocomposite Thermal analysis sol-gel method |
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References | M Răileanu (8124_Cr3) 2003; 5 C Cannas (8124_Cr17) 2002; 57a G Ennas (8124_Cr18) 2002; 17 A Jitianu (8124_Cr2) 2002; 12 G Piccaluga (8124_Cr13) 2000; 13 M Popovici (8124_Cr8) 2004; 16 G Ennas (8124_Cr9) 1998; 10 C Cannas (8124_Cr6) 2002; 12 AC Pierre (8124_Cr15) 1992 C Chanéac (8124_Cr7) 1995; 6 JP Jolivet (8124_Cr4) 2000; AP 10 A Jitianu (8124_Cr12) 2006; 40 S Solinas (8124_Cr5) 2001; 49 S Bruni (8124_Cr16) 1999; 11 F del Monte (8124_Cr10) 1997; 13 T López (8124_Cr1) 1992; 30 G Ennas (8124_Cr11) 1999; 14 SC Mojumdar (8124_Cr14) 2006; 85 |
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SubjectTerms | Applied sciences Composites Exact sciences and technology Forms of application and semi-finished materials Polymer industry, paints, wood Technology of polymers |
Title | Thermal behaviour study of some sol-gel iron-silica nanocomposites |
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