Bi-active sites of stable and highly dispersed platinum and oxygen vacancy constructed by reducing a loaded perovskite-type oxide for CO oxidation

Schematic illustration of the structural evolution of Pt/LaCoxNi1−xO3/SiO2 from LaCoxNi0.87−xPt0.13O3/SiO2. [Display omitted] •A facile method for constructing stable and highly dispersed bi-active catalytic sites were proposed.•Pt clusters and oxygen vacancies could be constructed.•Pt/LaCoxNi1−xO3...

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Published inApplied surface science Vol. 532; p. 147455
Main Authors Zhang, Siran, An, Kang, Li, Shuangshuang, Zhang, Ziyang, Sun, Ruolin, Liu, Yuan
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.12.2020
Subjects
Bi-active sites
Carbon monoxide oxidation
Oxygen vacancy
Perovskite-type oxide
Platinum cluster
Platinum cluster
Carbon monoxide oxidation
Bi-active sites
Perovskite-type oxide
Oxygen vacancy
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Abstract Schematic illustration of the structural evolution of Pt/LaCoxNi1−xO3/SiO2 from LaCoxNi0.87−xPt0.13O3/SiO2. [Display omitted] •A facile method for constructing stable and highly dispersed bi-active catalytic sites were proposed.•Pt clusters and oxygen vacancies could be constructed.•Pt/LaCoxNi1−xO3 loaded on SiO2 was obtained by using a perovskite-type oxide as the precursor.•The catalyst showed excellent activity and stability for CO oxidation. A new scheme for constructing bi-active sites of highly dispersed Pt and oxygen vacancies on a catalyst was put forward in this study. Pt/LaCoxNi1−xO3/SiO2 was synthesized by reducing LaCoxNi0.87−xPt0.13O3 with the structure of perovskite loaded on silica. The catalytic performance for carbon monoxide oxidation over the catalysts were studied. The catalysts were characterized via using XRD, XPS, XAFS, N2 adsorption–desorption, H2-TPR, TEM, O2 and CO-TPD techniques. The results pointed out that nanocrystal lines of LaCoxNi0.87−xPt0.13O3 were supported on SiO2. Pt clusters could be formed through reduction process at 300 °C and highly dispersed on catalyst’s surface, and the catalyst transformed to Pt/LaCoxNi1−xO3/SiO2; at the same time, oxygen vacancies also formed on the surface of LaCoxNi1−xO3. The catalytic test revealed that LaCo0.44Ni0.43Pt0.13O3/SiO2 displayed high activity and good stability for the oxidation of CO. The highly dispersed closely contact bi-active sites, the confinement of oxygen vacancies and strong interaction between Pt clusters and support were responsible for the significant catalytic activity and stability of LaCo0.44Ni0.43Pt0.13O3/SiO2 catalyst.
AbstractList Schematic illustration of the structural evolution of Pt/LaCoxNi1−xO3/SiO2 from LaCoxNi0.87−xPt0.13O3/SiO2. [Display omitted] •A facile method for constructing stable and highly dispersed bi-active catalytic sites were proposed.•Pt clusters and oxygen vacancies could be constructed.•Pt/LaCoxNi1−xO3 loaded on SiO2 was obtained by using a perovskite-type oxide as the precursor.•The catalyst showed excellent activity and stability for CO oxidation. A new scheme for constructing bi-active sites of highly dispersed Pt and oxygen vacancies on a catalyst was put forward in this study. Pt/LaCoxNi1−xO3/SiO2 was synthesized by reducing LaCoxNi0.87−xPt0.13O3 with the structure of perovskite loaded on silica. The catalytic performance for carbon monoxide oxidation over the catalysts were studied. The catalysts were characterized via using XRD, XPS, XAFS, N2 adsorption–desorption, H2-TPR, TEM, O2 and CO-TPD techniques. The results pointed out that nanocrystal lines of LaCoxNi0.87−xPt0.13O3 were supported on SiO2. Pt clusters could be formed through reduction process at 300 °C and highly dispersed on catalyst’s surface, and the catalyst transformed to Pt/LaCoxNi1−xO3/SiO2; at the same time, oxygen vacancies also formed on the surface of LaCoxNi1−xO3. The catalytic test revealed that LaCo0.44Ni0.43Pt0.13O3/SiO2 displayed high activity and good stability for the oxidation of CO. The highly dispersed closely contact bi-active sites, the confinement of oxygen vacancies and strong interaction between Pt clusters and support were responsible for the significant catalytic activity and stability of LaCo0.44Ni0.43Pt0.13O3/SiO2 catalyst.
ArticleNumber 147455
Author Zhang, Siran
Li, Shuangshuang
Zhang, Ziyang
Liu, Yuan
An, Kang
Sun, Ruolin
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Keywords Platinum cluster
Carbon monoxide oxidation
Bi-active sites
Perovskite-type oxide
Oxygen vacancy
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Snippet Schematic illustration of the structural evolution of Pt/LaCoxNi1−xO3/SiO2 from LaCoxNi0.87−xPt0.13O3/SiO2. [Display omitted] •A facile method for constructing...
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elsevier
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StartPage 147455
SubjectTerms Bi-active sites
Carbon monoxide oxidation
Oxygen vacancy
Perovskite-type oxide
Platinum cluster
Title Bi-active sites of stable and highly dispersed platinum and oxygen vacancy constructed by reducing a loaded perovskite-type oxide for CO oxidation
URI https://dx.doi.org/10.1016/j.apsusc.2020.147455
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