Structural, vibrational and magnetic properties of monoclinic La2FeMnO6 double perovskite
We report the synthesis of the double perovskite La2FeMnO6 and a complete characterization of this system by using X-ray diffraction, Raman and Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), vibrating sample magnetometer, Mossbauer spectroscopy and lattice dynam...
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| Published in | Vacuum Vol. 202; p. 111140 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.08.2022
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| Abstract | We report the synthesis of the double perovskite La2FeMnO6 and a complete characterization of this system by using X-ray diffraction, Raman and Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), vibrating sample magnetometer, Mossbauer spectroscopy and lattice dynamic calculations. The ambient structure of the La2FeMnO6 was well refined using monoclinic system and P21/n-space group, with two formulas per unit cell (Z = 2). SEM reveals that the sample is formed by particles with quasi-spherical morphology, randomly distributed in clusters. The investigation by Mössbauer spectroscopy identified that the incorporation of iron atoms occurred successfully in the analyzed structure since two paramagnetic phases were identified. The magnetization versus applied field (MxH) curve of La2FeMnO6 at room temperature is discussed. The LFMO double perovskite EPR spectrum indicates the coexistence of paramagnetic resonance (PM) and antiferromagnetic resonance (AFM), being a strong indication of the coexistence of PM and AFM clusters. Moreover, vibrational properties were calculated using a rigid ion model in order to assign the experimental Raman and infrared bands. All these results making the La2FeMnO6 an interesting material with practical applications and for the scientific investigations.
•Synthesis and characterization of the double perovskite La2FeMnO6 system.•Vibrational properties of the La2FeMnO6 at room temperature.•Lattice dynamic calculations based on a rigid ion model.•The magnetization versus applied field (MxH) curve of La2FeMnO6 at room temperature. |
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| AbstractList | We report the synthesis of the double perovskite La2FeMnO6 and a complete characterization of this system by using X-ray diffraction, Raman and Fourier transform infrared (FT-IR) spectroscopy, scanning electron microscopy (SEM), vibrating sample magnetometer, Mossbauer spectroscopy and lattice dynamic calculations. The ambient structure of the La2FeMnO6 was well refined using monoclinic system and P21/n-space group, with two formulas per unit cell (Z = 2). SEM reveals that the sample is formed by particles with quasi-spherical morphology, randomly distributed in clusters. The investigation by Mössbauer spectroscopy identified that the incorporation of iron atoms occurred successfully in the analyzed structure since two paramagnetic phases were identified. The magnetization versus applied field (MxH) curve of La2FeMnO6 at room temperature is discussed. The LFMO double perovskite EPR spectrum indicates the coexistence of paramagnetic resonance (PM) and antiferromagnetic resonance (AFM), being a strong indication of the coexistence of PM and AFM clusters. Moreover, vibrational properties were calculated using a rigid ion model in order to assign the experimental Raman and infrared bands. All these results making the La2FeMnO6 an interesting material with practical applications and for the scientific investigations.
•Synthesis and characterization of the double perovskite La2FeMnO6 system.•Vibrational properties of the La2FeMnO6 at room temperature.•Lattice dynamic calculations based on a rigid ion model.•The magnetization versus applied field (MxH) curve of La2FeMnO6 at room temperature. |
| ArticleNumber | 111140 |
| Author | Jucá, Raí F. Souza, G.D.S. Paraguassu, W. Ramiro de Castro, A.J. Saraiva, Gilberto D. Oliveira, Francisco G.S. Soares, João M. Cordeiro, Carlos H.N. Sousa, Francisco F.de Vasconcelos, Igor F. |
| Author_xml | – sequence: 1 givenname: Raí F. orcidid: 0000-0001-6489-4814 surname: Jucá fullname: Jucá, Raí F. organization: Departamento de Física, Universidade Federal de Sergipe, São Cristóvão, 49100-000, Sergipe, Brazil – sequence: 2 givenname: Gilberto D. orcidid: 0000-0003-4912-6213 surname: Saraiva fullname: Saraiva, Gilberto D. email: gilberto.saraiva@uece.br organization: Faculdade de Educação Ciências e Letras do Sertão Central, Universidade Estadual do Ceará, Quixadá, CE, 63902-098, Brazil – sequence: 3 givenname: A.J. orcidid: 0000-0003-3489-8712 surname: Ramiro de Castro fullname: Ramiro de Castro, A.J. organization: Universidade Federal do Ceará, 63902-580, Quixadá, CE, Brazil – sequence: 4 givenname: Francisco F.de surname: Sousa fullname: Sousa, Francisco F.de organization: Instituto de Ciências Exatas e Naturais, Universidade Federal do Pará, CEP, 66075-110, Belém, PA, Brazil – sequence: 5 givenname: Francisco G.S. surname: Oliveira fullname: Oliveira, Francisco G.S. organization: Pós-graduação em Engenharia e Ciências de Materiais, Centro de Tecnologia, Universidade Federal do Ceara, Campus do Pici, Bloco 729, 60440-900, Fortaleza, CE, Brazil – sequence: 6 givenname: Igor F. orcidid: 0000-0002-6172-805X surname: Vasconcelos fullname: Vasconcelos, Igor F. organization: Pós-graduação em Engenharia e Ciências de Materiais, Centro de Tecnologia, Universidade Federal do Ceara, Campus do Pici, Bloco 729, 60440-900, Fortaleza, CE, Brazil – sequence: 7 givenname: G.D.S. orcidid: 0000-0001-5769-2923 surname: Souza fullname: Souza, G.D.S. organization: Instituto de Ciências Exatas e Naturais, Universidade Federal do Pará, CEP, 66075-110, Belém, PA, Brazil – sequence: 8 givenname: João M. surname: Soares fullname: Soares, João M. organization: Departamento de Física, Universidade do Estado do Rio Grande do Norte, Mossoró-RN, CEP, 59610-210, Brazil – sequence: 9 givenname: Carlos H.N. surname: Cordeiro fullname: Cordeiro, Carlos H.N. organization: Departamento de Física, Universidade Federal do Ceará, Caixa Postal 6030, Campus do Pici, CEP, 60455-970, Fortaleza, Ceará, Brazil – sequence: 10 givenname: W. surname: Paraguassu fullname: Paraguassu, W. organization: Instituto de Ciências Exatas e Naturais, Universidade Federal do Pará, CEP, 66075-110, Belém, PA, Brazil |
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