Functionalized Zn/Al N-doped carbon nanocomposites with tunable morphology: Synergistic ultrafast low-temperature synthesis and tetracycline adsorption
[Display omitted] •Fabrication of mixed-metal composites via combustion reaction under low temperature.•Promotion influence of fuel type on physicochemical properties of sample.•Combustion reaction can provide inspiration for the time-saving preparation (0–10 s).•The adsorbents prepared in study hav...
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| Published in | Separation and purification technology Vol. 278; p. 119548 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.01.2022
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Fabrication of mixed-metal composites via combustion reaction under low temperature.•Promotion influence of fuel type on physicochemical properties of sample.•Combustion reaction can provide inspiration for the time-saving preparation (0–10 s).•The adsorbents prepared in study have excellent adsorption capacity (>336 mg/g).•The adsorption capacity was enhanced by 32.5 % in 10 mg/L humic acid solution.
The fast and efficient combustion technology was used to design zinc/alumina oxide N-doped carbon nanocomposites (Zn/Al-NCs) with assorted structures as pollutants adsorbent for capturing tetracycline (TC). XRD, SEM, TEM, EDX mapping, BET, and FTIR analysis techniques demonstrated the morphology and physicochemical properties of Zn/Al-NCs synthesized under mild conditions. The experimental results show that the pseudo-second-order kinetic and Langmuir model described the adsorption process well, indicating chemisorption and a monolayer adsorption nature. All Zn/Al-NCs exhibits excellent adsorption performance (>336 mg/g) to TC and the presence of humic acid (10 mg/L) made the adsorption capacity achieved a huge increasement (>446 mg/g) by forming a bridge bond. The adsorption mechanisms were pore-filling, electrostatic interactions, complexation, and H-bonds, confirming by BET, zeta potential, XPS, and FT-IR. The proposed synthesis strategy provides an efficient, excellent versatility, and time-saving way for preparing potential and high-performance materials for adsorbents. |
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| AbstractList | [Display omitted]
•Fabrication of mixed-metal composites via combustion reaction under low temperature.•Promotion influence of fuel type on physicochemical properties of sample.•Combustion reaction can provide inspiration for the time-saving preparation (0–10 s).•The adsorbents prepared in study have excellent adsorption capacity (>336 mg/g).•The adsorption capacity was enhanced by 32.5 % in 10 mg/L humic acid solution.
The fast and efficient combustion technology was used to design zinc/alumina oxide N-doped carbon nanocomposites (Zn/Al-NCs) with assorted structures as pollutants adsorbent for capturing tetracycline (TC). XRD, SEM, TEM, EDX mapping, BET, and FTIR analysis techniques demonstrated the morphology and physicochemical properties of Zn/Al-NCs synthesized under mild conditions. The experimental results show that the pseudo-second-order kinetic and Langmuir model described the adsorption process well, indicating chemisorption and a monolayer adsorption nature. All Zn/Al-NCs exhibits excellent adsorption performance (>336 mg/g) to TC and the presence of humic acid (10 mg/L) made the adsorption capacity achieved a huge increasement (>446 mg/g) by forming a bridge bond. The adsorption mechanisms were pore-filling, electrostatic interactions, complexation, and H-bonds, confirming by BET, zeta potential, XPS, and FT-IR. The proposed synthesis strategy provides an efficient, excellent versatility, and time-saving way for preparing potential and high-performance materials for adsorbents. |
| ArticleNumber | 119548 |
| Author | Yang, Hongbing Gao, Ming Li, Yongsheng Wang, Wei Cao, Mengbo Liu, Xun |
| Author_xml | – sequence: 1 givenname: Mengbo surname: Cao fullname: Cao, Mengbo – sequence: 2 givenname: Xun surname: Liu fullname: Liu, Xun – sequence: 3 givenname: Wei surname: Wang fullname: Wang, Wei – sequence: 4 givenname: Ming surname: Gao fullname: Gao, Ming – sequence: 5 givenname: Yongsheng surname: Li fullname: Li, Yongsheng – sequence: 6 givenname: Hongbing surname: Yang fullname: Yang, Hongbing email: yhb_tea@163.com |
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| Keywords | Tetracycline adsorption Mechanisms Self-sustaining combustion Mixed metal oxides nanocomposites Ultrafast low-temperature synthesis Fuel type |
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| Title | Functionalized Zn/Al N-doped carbon nanocomposites with tunable morphology: Synergistic ultrafast low-temperature synthesis and tetracycline adsorption |
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