Fabrication and characterization of mesoporous guar gum/NiWO4 nanocomposite for efficient adsorption of phloxine B and crystal violet from aqueous solution and evaluation of its antioxidant activity

Guar gum/nickel tungstate (GG/NiWO4) nanocomposite is prepared using simple and cost-effective sol-gel technique, while NiWO4 nanoparticles are formed by co-precipitation method. The nanocomposite is characterized by FTIR, XRD, BET, SEM-EDX and TEM techniques. The effectivity of GG/NiWO4 nanocomposi...

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Published inColloid and interface science communications Vol. 44; p. 100488
Main Authors Hussain, Daud, Khan, Suhail Ayoub, Khan, Tabrez Alam
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.09.2021
Subjects
Adsorption
Antioxidant activity
Dyes
Guar gum
Nanocomposite
NiWO4
Nanocomposite
Dyes
Adsorption
NiWO4
Antioxidant activity
Guar gum
Online AccessGet full text
ISSN2215-0382
2215-0382
DOI10.1016/j.colcom.2021.100488

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Abstract Guar gum/nickel tungstate (GG/NiWO4) nanocomposite is prepared using simple and cost-effective sol-gel technique, while NiWO4 nanoparticles are formed by co-precipitation method. The nanocomposite is characterized by FTIR, XRD, BET, SEM-EDX and TEM techniques. The effectivity of GG/NiWO4 nanocomposite is investigated for the sequestration of phloxine B (PB) and crystal violet (CV) from wastewater. The effect of dose, agitation time, initial solution pH, and initial dyes concentration is appraised. The adsorption isotherm, kinetics and thermodynamic parameters are also studied. Langmuir isotherm and pseudo-second order models are best fitted to the equilibrium data. The thermodynamic parameters confirm that adsorption is spontaneous, exothermic and entropy-driven. An excellent desorption of PB and CV from the loaded adsorbent is acquired by utilizing either ethanol or acetone with a desorption ability in the range of 57.60%–91%. The antioxidant activities of synthesized nanocomposite are also studied. [Display omitted] •GG/NiWO4 nanocomposite efficiently removes PB and CV dyes from water.•Maximum saturation capacity is 220.21 and 170.42 mg/g for PB and CV, respectively.•Thermodynamic parameters suggest spontaneity and exothermic adsorption procedure.•Nanocomposite depicts good adsorption-desorption reusability for seven cycles.
AbstractList Guar gum/nickel tungstate (GG/NiWO4) nanocomposite is prepared using simple and cost-effective sol-gel technique, while NiWO4 nanoparticles are formed by co-precipitation method. The nanocomposite is characterized by FTIR, XRD, BET, SEM-EDX and TEM techniques. The effectivity of GG/NiWO4 nanocomposite is investigated for the sequestration of phloxine B (PB) and crystal violet (CV) from wastewater. The effect of dose, agitation time, initial solution pH, and initial dyes concentration is appraised. The adsorption isotherm, kinetics and thermodynamic parameters are also studied. Langmuir isotherm and pseudo-second order models are best fitted to the equilibrium data. The thermodynamic parameters confirm that adsorption is spontaneous, exothermic and entropy-driven. An excellent desorption of PB and CV from the loaded adsorbent is acquired by utilizing either ethanol or acetone with a desorption ability in the range of 57.60%–91%. The antioxidant activities of synthesized nanocomposite are also studied. [Display omitted] •GG/NiWO4 nanocomposite efficiently removes PB and CV dyes from water.•Maximum saturation capacity is 220.21 and 170.42 mg/g for PB and CV, respectively.•Thermodynamic parameters suggest spontaneity and exothermic adsorption procedure.•Nanocomposite depicts good adsorption-desorption reusability for seven cycles.
ArticleNumber 100488
Author Hussain, Daud
Khan, Suhail Ayoub
Khan, Tabrez Alam
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  email: takhan@jmi.ac.in
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Keywords Nanocomposite
Dyes
Adsorption
NiWO4
Antioxidant activity
Guar gum
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Snippet Guar gum/nickel tungstate (GG/NiWO4) nanocomposite is prepared using simple and cost-effective sol-gel technique, while NiWO4 nanoparticles are formed by...
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elsevier
SourceType Enrichment Source
Index Database
Publisher
StartPage 100488
SubjectTerms Adsorption
Antioxidant activity
Dyes
Guar gum
Nanocomposite
NiWO4
Title Fabrication and characterization of mesoporous guar gum/NiWO4 nanocomposite for efficient adsorption of phloxine B and crystal violet from aqueous solution and evaluation of its antioxidant activity
URI https://dx.doi.org/10.1016/j.colcom.2021.100488
Volume 44
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