Study of phase transformation and surface microstructure of alumina ceramic under irradiation of intense pulsed ion beam

Intense pulsed ion beam (IPIB), featured with pulsed high-power density, has been widely used in the modification of structural material, especially in high strength materials. The effects of IPIB treatment on phase transformation and surface microstructure of alumina ceramics were investigated in t...

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Published inVacuum Vol. 187; p. 110154
Main Authors Zhang, Shijian, Yu, Xiao, Zhang, Jie, Shen, Jie, Zhong, Haowen, Liang, Guoying, Xu, Mofei, Zhang, Nan, Ren, Jianhui, Kuang, Shicheng, Shang, Xuying, Adegboyega, Oluwasogo, Yan, Sha, Remnev, Gennady Efimovich, Le, Xiaoyun
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LanguageEnglish
Published Elsevier Ltd 01.05.2021
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Abstract Intense pulsed ion beam (IPIB), featured with pulsed high-power density, has been widely used in the modification of structural material, especially in high strength materials. The effects of IPIB treatment on phase transformation and surface microstructure of alumina ceramics were investigated in this work. Experiments were carried out on the BIPPAB-450 accelerator with peak accelerating voltage and current density of 360 kV and 170 A/cm2. X-ray diffraction (XRD), scanning electron microscope (SEM) and atomic force microscope (AFM) were used to analyze the phase transformation and cross-section and surface morphology of alumina ceramics under IPIB treatment. The XRD pattern indicated that phase transformation from α-Al2O3 to γ-Al2O3 occurred on the irradiated area due to the combined effect of rapid re-solidification and thermal stress caused by IPIB. The SEM cross-section images indicated that homogeneous modified layer with thickness up to 1.53 μm was produced and cracks inside sample were observed as well after IPIB irradiation. The evolution of cracks on surface of samples with pulse number was investigated in this work. Micro-holes distributed on the net structure of cracks were observed after IPIB irradiation and the evolution of size and number of micro-holes with pulse number was discussed. •Phase transformation from α-Al2O3 to γ-Al2O3 was confirmed by XRD after irradiation of intense pulsed ion beam.•The relationship between the evolution of micro-holes caused by IPIB and pulse number was investigated.•The roughness of surface decreased to minimum after 1 pulse irradiation of IPIB.
AbstractList Intense pulsed ion beam (IPIB), featured with pulsed high-power density, has been widely used in the modification of structural material, especially in high strength materials. The effects of IPIB treatment on phase transformation and surface microstructure of alumina ceramics were investigated in this work. Experiments were carried out on the BIPPAB-450 accelerator with peak accelerating voltage and current density of 360 kV and 170 A/cm2. X-ray diffraction (XRD), scanning electron microscope (SEM) and atomic force microscope (AFM) were used to analyze the phase transformation and cross-section and surface morphology of alumina ceramics under IPIB treatment. The XRD pattern indicated that phase transformation from α-Al2O3 to γ-Al2O3 occurred on the irradiated area due to the combined effect of rapid re-solidification and thermal stress caused by IPIB. The SEM cross-section images indicated that homogeneous modified layer with thickness up to 1.53 μm was produced and cracks inside sample were observed as well after IPIB irradiation. The evolution of cracks on surface of samples with pulse number was investigated in this work. Micro-holes distributed on the net structure of cracks were observed after IPIB irradiation and the evolution of size and number of micro-holes with pulse number was discussed. •Phase transformation from α-Al2O3 to γ-Al2O3 was confirmed by XRD after irradiation of intense pulsed ion beam.•The relationship between the evolution of micro-holes caused by IPIB and pulse number was investigated.•The roughness of surface decreased to minimum after 1 pulse irradiation of IPIB.
ArticleNumber 110154
Author Kuang, Shicheng
Shen, Jie
Le, Xiaoyun
Zhang, Nan
Zhong, Haowen
Yan, Sha
Shang, Xuying
Yu, Xiao
Liang, Guoying
Zhang, Shijian
Adegboyega, Oluwasogo
Xu, Mofei
Remnev, Gennady Efimovich
Zhang, Jie
Ren, Jianhui
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  fullname: Yu, Xiao
  organization: School of Physics, Beihang University, Beijing, 100191, PR China
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  givenname: Jie
  surname: Zhang
  fullname: Zhang, Jie
  organization: Nuclear and Radiation Safety Center, Ministry of Ecology and Environment, Beijing, 100082, China
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  organization: School of Physics, Beihang University, Beijing, 100191, PR China
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  surname: Ren
  fullname: Ren, Jianhui
  organization: School of Physics, Beihang University, Beijing, 100191, PR China
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  givenname: Shicheng
  surname: Kuang
  fullname: Kuang, Shicheng
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  givenname: Xuying
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  organization: School of Physics, Beihang University, Beijing, 100191, PR China
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– sequence: 13
  givenname: Sha
  surname: Yan
  fullname: Yan, Sha
  organization: Institute of Heavy Ion Physics, Peking University, Beijing, 100871, PR China
– sequence: 14
  givenname: Gennady Efimovich
  surname: Remnev
  fullname: Remnev, Gennady Efimovich
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  givenname: Xiaoyun
  surname: Le
  fullname: Le, Xiaoyun
  email: xyle@buaa.edu.cn
  organization: School of Physics, Beihang University, Beijing, 100191, PR China
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Keywords Phase transformation
Intense pulsed ion beam
Surface microstructure
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Snippet Intense pulsed ion beam (IPIB), featured with pulsed high-power density, has been widely used in the modification of structural material, especially in high...
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SubjectTerms Intense pulsed ion beam
Phase transformation
Surface microstructure
Title Study of phase transformation and surface microstructure of alumina ceramic under irradiation of intense pulsed ion beam
URI https://dx.doi.org/10.1016/j.vacuum.2021.110154
Volume 187
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