Construction of Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction with multiple built-in electric fields for effectively boosting visible-light photocatalytic degradation of broad-spectrum antibiotics

•Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction was synthesized by a solvothermal route.•Cu3P-ZnSnO3-g-C3N4 shows outstanding visible-light photocatalytic activity.•Multiple built-in electric fields in heterojunction facilitate charge transfer. The design of advanced semiconductor photocatalysts is an effe...

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Published in	Separation and purification technology Vol. 265; p. 118477
Main Authors	Guo, Feng, Huang, Xiliu, Chen, Zhihao, Cao, Longwen, Cheng, Xiaofang, Chen, Lizhuang, Shi, Weilong
Format	Journal Article
Language	English
Published	Elsevier B.V 15.06.2021
Subjects	Cu3P G-C3N4 p-n-n heterojunction Photocatalytic activity ZnSnO3 Photocatalytic activity ZnSnO3 G-C3N4 p-n-n heterojunction Cu3P
Online Access	Get full text
ISSN	1383-5866 1873-3794
DOI	10.1016/j.seppur.2021.118477

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Abstract	•Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction was synthesized by a solvothermal route.•Cu3P-ZnSnO3-g-C3N4 shows outstanding visible-light photocatalytic activity.•Multiple built-in electric fields in heterojunction facilitate charge transfer. The design of advanced semiconductor photocatalysts is an effective approach to promote environmental remediation. The p-n-n heterojunction photocatalyst has a strong built-in electric field in the photocatalytic reaction, which provides an effective space for the separation of photo-generated carriers, thereby achieving high-efficient photocatalytic activity. Herein, a facile solvothermal method was developed to manufacture a unique Cu3P-ZSO-CN p-n-n heterojunction photocatalyst for the photodegradation of broad-spectrum antibiotics under visible light irradiation. Benefiting from the novel p-n-n heterojunction structure, the obtained 5% Cu3P-ZSO-CN photocatalyst exhibits the highest degradation efficiency, and the degradation rates for tetracycline (TC), oxytetracycline (OTC), chlortetracycline (CTC) and ciprofloxacin (CIP) are assigned to 98.45%, 54.71%, 63.52% and 87.57%, respectively. Furthermore, based on the detection of intermediate products via liquid chromatography mass spectrometry (LC-MS), the possible photodegradation pathway of TC was analyzed. Finally, the possible Cu3P-ZSO-CN p-n-n heterojunction photocatalytic reaction mechanism was revealed in detail by the examination of optical properties and capturing experiments of active species. This work provides a new perspective for the application of p-n-n heterojunction photocatalysts in environmental remediation.
AbstractList	•Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction was synthesized by a solvothermal route.•Cu3P-ZnSnO3-g-C3N4 shows outstanding visible-light photocatalytic activity.•Multiple built-in electric fields in heterojunction facilitate charge transfer. The design of advanced semiconductor photocatalysts is an effective approach to promote environmental remediation. The p-n-n heterojunction photocatalyst has a strong built-in electric field in the photocatalytic reaction, which provides an effective space for the separation of photo-generated carriers, thereby achieving high-efficient photocatalytic activity. Herein, a facile solvothermal method was developed to manufacture a unique Cu3P-ZSO-CN p-n-n heterojunction photocatalyst for the photodegradation of broad-spectrum antibiotics under visible light irradiation. Benefiting from the novel p-n-n heterojunction structure, the obtained 5% Cu3P-ZSO-CN photocatalyst exhibits the highest degradation efficiency, and the degradation rates for tetracycline (TC), oxytetracycline (OTC), chlortetracycline (CTC) and ciprofloxacin (CIP) are assigned to 98.45%, 54.71%, 63.52% and 87.57%, respectively. Furthermore, based on the detection of intermediate products via liquid chromatography mass spectrometry (LC-MS), the possible photodegradation pathway of TC was analyzed. Finally, the possible Cu3P-ZSO-CN p-n-n heterojunction photocatalytic reaction mechanism was revealed in detail by the examination of optical properties and capturing experiments of active species. This work provides a new perspective for the application of p-n-n heterojunction photocatalysts in environmental remediation.
ArticleNumber	118477
Author	Huang, Xiliu Shi, Weilong Cheng, Xiaofang Cao, Longwen Chen, Lizhuang Guo, Feng Chen, Zhihao
Author_xml	– sequence: 1 givenname: Feng surname: Guo fullname: Guo, Feng organization: School of Energy and Power, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003, PR China – sequence: 2 givenname: Xiliu surname: Huang fullname: Huang, Xiliu organization: School of Environmental and Chemical Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, PR China – sequence: 3 givenname: Zhihao surname: Chen fullname: Chen, Zhihao organization: School of Environmental and Chemical Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, PR China – sequence: 4 givenname: Longwen surname: Cao fullname: Cao, Longwen organization: School of Environmental and Chemical Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, PR China – sequence: 5 givenname: Xiaofang surname: Cheng fullname: Cheng, Xiaofang organization: School of Environmental and Chemical Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, PR China – sequence: 6 givenname: Lizhuang surname: Chen fullname: Chen, Lizhuang email: clz1977@sina.com organization: School of Environmental and Chemical Engineering, Jiangsu University of Science and Technology, Zhenjiang, 212003, PR China – sequence: 7 givenname: Weilong surname: Shi fullname: Shi, Weilong email: shiwl@just.edu.cn organization: School of Material Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003, PR China
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Snippet	•Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction was synthesized by a solvothermal route.•Cu3P-ZnSnO3-g-C3N4 shows outstanding visible-light photocatalytic...
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SubjectTerms	Cu3P G-C3N4 p-n-n heterojunction Photocatalytic activity ZnSnO3
Title	Construction of Cu3P-ZnSnO3-g-C3N4 p-n-n heterojunction with multiple built-in electric fields for effectively boosting visible-light photocatalytic degradation of broad-spectrum antibiotics
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