Closed-loop cobalt recycling from spent lithium-ion batteries based on a deep eutectic solvent (DES) with easy solvent recovery

The recycling of LCO is realized in a closed-loop protocol, where the dissolution/extraction of the cobalt element involves no additional precipitates, thus enabling the reusability of the leaching solution. [Display omitted] Efficient recycling technology for the rapid growth of spent lithium-ion b...

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Published inJournal of energy chemistry Vol. 72; pp. 532 - 538
Main Authors Li, Taibai, Xiong, Yige, Yan, Xiaohui, Hu, Tao, Jing, Siqi, Wang, Zhongjie, Ge, Xiang
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.09.2022
Subjects
Closed-loop
Deep eutectic solvent
High efficiency
Lithium-ion batteries recycle
Solvent recovery
Solvent recovery
Deep eutectic solvent
Closed-loop
Lithium-ion batteries recycle
High efficiency
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Abstract The recycling of LCO is realized in a closed-loop protocol, where the dissolution/extraction of the cobalt element involves no additional precipitates, thus enabling the reusability of the leaching solution. [Display omitted] Efficient recycling technology for the rapid growth of spent lithium-ion batteries (LIBs) is essential to tackle the resources and environmental crisis. Hydrometallurgical approach has attracted extensive research due to its potential to reduce the consumption of energy and threat to the environment. However, the simultaneous realization of green, efficient and closed-loop recycling is still challenging. Herein, we report a closed-loop and highly efficient approach to recycle lithium cobalt oxide from spent LIBs based on a choline chloride:oxalic acid (ChCl:OA) type deep eutectic solvent (DES). An ultrafast leaching process is observed at 180 °C for 10 s with no observable residues. The energy barrier during leaching is calculated to be 113.9 kJ/mol. Noteworthy, the solubility of cobalt ions can be reversibly tuned by simply adding/evaporating deionized water, thus avoiding the addition of precipitant and enabling the easy recovery of the leaching solvent for realizing a closed-loop recycling process. The simultaneous realization of high efficiency, green and closed-loop process is expected to push the DES into practical application for recycling the electrodes of LIBs.
AbstractList The recycling of LCO is realized in a closed-loop protocol, where the dissolution/extraction of the cobalt element involves no additional precipitates, thus enabling the reusability of the leaching solution. [Display omitted] Efficient recycling technology for the rapid growth of spent lithium-ion batteries (LIBs) is essential to tackle the resources and environmental crisis. Hydrometallurgical approach has attracted extensive research due to its potential to reduce the consumption of energy and threat to the environment. However, the simultaneous realization of green, efficient and closed-loop recycling is still challenging. Herein, we report a closed-loop and highly efficient approach to recycle lithium cobalt oxide from spent LIBs based on a choline chloride:oxalic acid (ChCl:OA) type deep eutectic solvent (DES). An ultrafast leaching process is observed at 180 °C for 10 s with no observable residues. The energy barrier during leaching is calculated to be 113.9 kJ/mol. Noteworthy, the solubility of cobalt ions can be reversibly tuned by simply adding/evaporating deionized water, thus avoiding the addition of precipitant and enabling the easy recovery of the leaching solvent for realizing a closed-loop recycling process. The simultaneous realization of high efficiency, green and closed-loop process is expected to push the DES into practical application for recycling the electrodes of LIBs.
Author Hu, Tao
Jing, Siqi
Li, Taibai
Wang, Zhongjie
Xiong, Yige
Yan, Xiaohui
Ge, Xiang
Author_xml – sequence: 1
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  surname: Li
  fullname: Li, Taibai
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  givenname: Yige
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  orcidid: 0000-0001-7932-5606
  surname: Ge
  fullname: Ge, Xiang
  email: xge@gzu.edu.cn
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Snippet The recycling of LCO is realized in a closed-loop protocol, where the dissolution/extraction of the cobalt element involves no additional precipitates, thus...
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SubjectTerms Closed-loop
Deep eutectic solvent
High efficiency
Lithium-ion batteries recycle
Solvent recovery
Title Closed-loop cobalt recycling from spent lithium-ion batteries based on a deep eutectic solvent (DES) with easy solvent recovery
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