Polypropylene membranes prepared via non-solvent/thermally induced phase separation: Effect of non-solvent nature
The goal of this work was to investigate the effect of non-solvent nature on the formation of porous membranes via non-solvent/thermally induced phase separation (N-TIPS). The hot solution of polypropylene (PP) in a mixture of dioctyl phthalate (DOP) and dibutyl phthalate (DBP) at 210 °C was placed...
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| Published in | Journal of membrane science Vol. 703; p. 122839 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.06.2024
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0376-7388 1873-3123 |
| DOI | 10.1016/j.memsci.2024.122839 |
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| Abstract | The goal of this work was to investigate the effect of non-solvent nature on the formation of porous membranes via non-solvent/thermally induced phase separation (N-TIPS). The hot solution of polypropylene (PP) in a mixture of dioctyl phthalate (DOP) and dibutyl phthalate (DBP) at 210 °C was placed as a thin film on a polyethylene terephthalate (PET) substrate, and then precipitated by immersion in the non-solvent (water, iso-propanol, 1-hexanol, or 1-decanol) at room temperature. It was found that the non-solvent nature greatly affected the morphology of the thin skin layer of the membrane facing the precipitation bath, which can be attributed to non-solvent induced phase separation (NIPS). The affinity between the polymeric solution and corresponding non-solvent was evaluated by using Hansen solubility parameters of components taken at room temperature and extrapolated to the temperature of 210 °C. An increase in the affinity between the non-solvent and the polymer transformed the surface layer structure from almost monolithic to cellular (with different pore sizes and porosity) and to spherulitic types. The non-solvent nature played a less pronounced role in the formation of the porous structure of the membrane bulk and the back side of the membrane (facing the PET substrate). Since the morphology of the rest of the membrane was correlated with thermophysical properties of non-solvents, it was concluded that the membrane formation took place due to temperature induced phase separation (TIPS). In the case of water, which has the highest cooling rate, the polypropylene crystallized by forming a “smectic” structure, while the standard α-lamellar structure was observed for other non-solvents. To gain insight into the TIPS process, a model of unsteady one-dimensional heat transfer was applied to simulate the change in the temperature profile of the hot, thin film of polymeric solution placed in the corresponding non-solvent. The resulting membranes were mainly in the microfiltration range with a mean through pore size of 0.05–0.61 μm, and iso-propanol permeance of 2.1–8.4 m3 m−2∙h−1∙bar−1. The rejection of 500 nm polystyrene microspheres was in the range of 45–98 %. The tensile strength was in the range of 2.9–3.2 MPa, and elongation at break was 30–190 % with respect to the non-solvent used.
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•Membranes from hot polypropylene solution were cast by precipitation in different non-solvents.•Effect of non-solvent nature in N-TIPS process was highlighted.•Membrane morphology, mechanical properties and pore size were subject of non-solvent nature.•Change of temperature profile of polymeric films during N-TIPS process was simulated. |
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| AbstractList | The goal of this work was to investigate the effect of non-solvent nature on the formation of porous membranes via non-solvent/thermally induced phase separation (N-TIPS). The hot solution of polypropylene (PP) in a mixture of dioctyl phthalate (DOP) and dibutyl phthalate (DBP) at 210 °C was placed as a thin film on a polyethylene terephthalate (PET) substrate, and then precipitated by immersion in the non-solvent (water, iso-propanol, 1-hexanol, or 1-decanol) at room temperature. It was found that the non-solvent nature greatly affected the morphology of the thin skin layer of the membrane facing the precipitation bath, which can be attributed to non-solvent induced phase separation (NIPS). The affinity between the polymeric solution and corresponding non-solvent was evaluated by using Hansen solubility parameters of components taken at room temperature and extrapolated to the temperature of 210 °C. An increase in the affinity between the non-solvent and the polymer transformed the surface layer structure from almost monolithic to cellular (with different pore sizes and porosity) and to spherulitic types. The non-solvent nature played a less pronounced role in the formation of the porous structure of the membrane bulk and the back side of the membrane (facing the PET substrate). Since the morphology of the rest of the membrane was correlated with thermophysical properties of non-solvents, it was concluded that the membrane formation took place due to temperature induced phase separation (TIPS). In the case of water, which has the highest cooling rate, the polypropylene crystallized by forming a “smectic” structure, while the standard α-lamellar structure was observed for other non-solvents. To gain insight into the TIPS process, a model of unsteady one-dimensional heat transfer was applied to simulate the change in the temperature profile of the hot, thin film of polymeric solution placed in the corresponding non-solvent. The resulting membranes were mainly in the microfiltration range with a mean through pore size of 0.05–0.61 μm, and iso-propanol permeance of 2.1–8.4 m3 m−2∙h−1∙bar−1. The rejection of 500 nm polystyrene microspheres was in the range of 45–98 %. The tensile strength was in the range of 2.9–3.2 MPa, and elongation at break was 30–190 % with respect to the non-solvent used.
[Display omitted]
•Membranes from hot polypropylene solution were cast by precipitation in different non-solvents.•Effect of non-solvent nature in N-TIPS process was highlighted.•Membrane morphology, mechanical properties and pore size were subject of non-solvent nature.•Change of temperature profile of polymeric films during N-TIPS process was simulated. |
| ArticleNumber | 122839 |
| Author | Volkov, Alexey Anokhina, Tatiana Pochivalov, Konstantin Lebedeva, Tatyana Yushkin, Alexey Shalygin, Maxim Yurov, Mikhail Basko, Andrey Lavrentyev, Viktor |
| Author_xml | – sequence: 1 givenname: Konstantin orcidid: 0000-0002-4570-0284 surname: Pochivalov fullname: Pochivalov, Konstantin organization: G.A. Krestov Institute of Solution Chemistry, Russian Academy of Sciences, Akademicheskaya ul. 1, Ivanovo, 153045, Russia – sequence: 2 givenname: Andrey orcidid: 0000-0002-8772-5236 surname: Basko fullname: Basko, Andrey organization: G.A. Krestov Institute of Solution Chemistry, Russian Academy of Sciences, Akademicheskaya ul. 1, Ivanovo, 153045, Russia – sequence: 3 givenname: Mikhail surname: Yurov fullname: Yurov, Mikhail organization: G.A. Krestov Institute of Solution Chemistry, Russian Academy of Sciences, Akademicheskaya ul. 1, Ivanovo, 153045, Russia – sequence: 4 givenname: Tatyana orcidid: 0000-0003-0537-0927 surname: Lebedeva fullname: Lebedeva, Tatyana organization: G.A. Krestov Institute of Solution Chemistry, Russian Academy of Sciences, Akademicheskaya ul. 1, Ivanovo, 153045, Russia – sequence: 5 givenname: Maxim orcidid: 0000-0002-5139-2265 surname: Shalygin fullname: Shalygin, Maxim organization: A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia – sequence: 6 givenname: Viktor surname: Lavrentyev fullname: Lavrentyev, Viktor organization: Institute of Macromolecular Compounds of the Russian Academy of Sciences, 31 Bolshoy pr., 199004, St. Petersburg, Russia – sequence: 7 givenname: Alexey surname: Yushkin fullname: Yushkin, Alexey organization: A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia – sequence: 8 givenname: Tatiana surname: Anokhina fullname: Anokhina, Tatiana organization: A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia – sequence: 9 givenname: Alexey surname: Volkov fullname: Volkov, Alexey email: avolkov@ips.ac.ru organization: A.V. Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences, Leninskii pr. 29, Moscow, 119991, Russia |
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| Keywords | Polypropylene Phase diagram Morphology Non-solvent-thermally induced phase separation Membrane Membrane performance N-TIPS |
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| Title | Polypropylene membranes prepared via non-solvent/thermally induced phase separation: Effect of non-solvent nature |
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