The black and white coatings on Ti-6Al-4V alloy or pure titanium by plasma electrolytic oxidation in concentrated silicate electrolyte

[Display omitted] •PEO of Ti-6Al-4V alloy and pure titanium in concentrated silicate electrolyte.•Black and white coatings respectively are formed by varying the PEO time.•Black color is attributed to Ti2+ and Ti3+ in the coatings.•The white coating shows super hydrophilicity.•Coating formation mech...

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Published inApplied surface science Vol. 428; pp. 684 - 697
Main Authors Han, Jun-xiang, Cheng, Yu-lin, Tu, Wen-bin, Zhan, Ting-Yan, Cheng, Ying-liang
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.01.2018
Subjects
Black TiO2
Hydrophilicity
Plasma electrolytic oxidation
Ti-6Al-4V alloy
Black TiO2
Ti-6Al-4V alloy
Hydrophilicity
Plasma electrolytic oxidation
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Abstract [Display omitted] •PEO of Ti-6Al-4V alloy and pure titanium in concentrated silicate electrolyte.•Black and white coatings respectively are formed by varying the PEO time.•Black color is attributed to Ti2+ and Ti3+ in the coatings.•The white coating shows super hydrophilicity.•Coating formation mechanisms have been discussed. Black TiO2 has triggered scientific interest due to its unique properties such as enhanced solar-driven photocatalytic activity. In this paper, plasma electrolytic oxidation (PEO) treatment of Ti-6Al-4V alloy has been carried out in concentrated sodium silicate electrolyte. Silica-based black and white TiO2 coatings respectively have been obtained by controlling the oxidation time. The black coating, which was formed with a short treatment time, shows good corrosion resistance and the black appearance can be attributed to the presence of Ti2+ and Ti3+ in the coating. The lower valence titanium ions are absent in the white coatings and they also contain relatively higher Na content compared to the black coatings. The white coatings have great surface roughnesses and super hydrophilicity. The bonding strengths of the black and white coatings on the Ti-6Al-4V alloy are ∼14.4 and 4.3MPa, respectively. The vanadium contributes little to the black appearance of the coating on Ti6Al4V alloy, since the same phenomena occur for the PEO of a pure titanium substrate.
AbstractList [Display omitted] •PEO of Ti-6Al-4V alloy and pure titanium in concentrated silicate electrolyte.•Black and white coatings respectively are formed by varying the PEO time.•Black color is attributed to Ti2+ and Ti3+ in the coatings.•The white coating shows super hydrophilicity.•Coating formation mechanisms have been discussed. Black TiO2 has triggered scientific interest due to its unique properties such as enhanced solar-driven photocatalytic activity. In this paper, plasma electrolytic oxidation (PEO) treatment of Ti-6Al-4V alloy has been carried out in concentrated sodium silicate electrolyte. Silica-based black and white TiO2 coatings respectively have been obtained by controlling the oxidation time. The black coating, which was formed with a short treatment time, shows good corrosion resistance and the black appearance can be attributed to the presence of Ti2+ and Ti3+ in the coating. The lower valence titanium ions are absent in the white coatings and they also contain relatively higher Na content compared to the black coatings. The white coatings have great surface roughnesses and super hydrophilicity. The bonding strengths of the black and white coatings on the Ti-6Al-4V alloy are ∼14.4 and 4.3MPa, respectively. The vanadium contributes little to the black appearance of the coating on Ti6Al4V alloy, since the same phenomena occur for the PEO of a pure titanium substrate.
Author Tu, Wen-bin
Zhan, Ting-Yan
Cheng, Ying-liang
Han, Jun-xiang
Cheng, Yu-lin
Author_xml – sequence: 1
  givenname: Jun-xiang
  surname: Han
  fullname: Han, Jun-xiang
– sequence: 2
  givenname: Yu-lin
  surname: Cheng
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– sequence: 3
  givenname: Wen-bin
  surname: Tu
  fullname: Tu, Wen-bin
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  givenname: Ting-Yan
  surname: Zhan
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– sequence: 5
  givenname: Ying-liang
  surname: Cheng
  fullname: Cheng, Ying-liang
  email: chengyingliang@hnu.edu.cn, deepblacksea@163.com
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Keywords Black TiO2
Ti-6Al-4V alloy
Hydrophilicity
Plasma electrolytic oxidation
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Snippet [Display omitted] •PEO of Ti-6Al-4V alloy and pure titanium in concentrated silicate electrolyte.•Black and white coatings respectively are formed by varying...
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Publisher
StartPage 684
SubjectTerms Black TiO2
Hydrophilicity
Plasma electrolytic oxidation
Ti-6Al-4V alloy
Title The black and white coatings on Ti-6Al-4V alloy or pure titanium by plasma electrolytic oxidation in concentrated silicate electrolyte
URI https://dx.doi.org/10.1016/j.apsusc.2017.09.109
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