Modification of TiO2 nanotubes by WO3 species for improving their photocatalytic activity
•WO3/titania nanotubes are synthesized at low temperature (383K) by a novel approach.•WO3/titania nanotubes present enhanced photocatalytic activity.•The substitution of Ti4+ by W6+ does not occur in nanocomposites at 383K.•Diffuse reflectance spectra of WO3/TNTs exhibit a red shift due to WO3 conne...
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| Published in | Applied surface science Vol. 343; pp. 181 - 187 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.07.2015
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| Subjects | |
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| Abstract | •WO3/titania nanotubes are synthesized at low temperature (383K) by a novel approach.•WO3/titania nanotubes present enhanced photocatalytic activity.•The substitution of Ti4+ by W6+ does not occur in nanocomposites at 383K.•Diffuse reflectance spectra of WO3/TNTs exhibit a red shift due to WO3 connection.•The optimal degradation rate of MO could reach 95% within 2h irradiation.
WO3/TiO2 nanotubular composite was synthesized at low temperature (383K) by a novel approach. WO3 nanoparticles were loaded on anatase TiO2 nanotubes through the reaction between (NH4)6W7O24·6H2O and aqueous solution of HCl. The obtained products were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD) and UV–vis diffuse reflectance spectroscopy (UV-DRS). Degradation of methyl orange was employed to investigate the photocatalytic activity of the products. Results show that, among the samples with different concentrations of WO3, W10T with the atomic ratio W/Ti of 10% presents optimal degradation rate. This degradation rate is about 95% within 2h under UV light irradiation, which is much higher than that of pure TiO2 nanotubes. |
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| AbstractList | •WO3/titania nanotubes are synthesized at low temperature (383K) by a novel approach.•WO3/titania nanotubes present enhanced photocatalytic activity.•The substitution of Ti4+ by W6+ does not occur in nanocomposites at 383K.•Diffuse reflectance spectra of WO3/TNTs exhibit a red shift due to WO3 connection.•The optimal degradation rate of MO could reach 95% within 2h irradiation.
WO3/TiO2 nanotubular composite was synthesized at low temperature (383K) by a novel approach. WO3 nanoparticles were loaded on anatase TiO2 nanotubes through the reaction between (NH4)6W7O24·6H2O and aqueous solution of HCl. The obtained products were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD) and UV–vis diffuse reflectance spectroscopy (UV-DRS). Degradation of methyl orange was employed to investigate the photocatalytic activity of the products. Results show that, among the samples with different concentrations of WO3, W10T with the atomic ratio W/Ti of 10% presents optimal degradation rate. This degradation rate is about 95% within 2h under UV light irradiation, which is much higher than that of pure TiO2 nanotubes. WO3/TiO2 nanotubular composite was synthesized at low temperature (383K) by a novel approach. WO3 nanoparticles were loaded on anatase TiO2 nanotubes through the reaction between (NH4)6W7O24.6H2O and aqueous solution of HCl. The obtained products were characterized by transmission electron microscopy (TEM), X-ray diffraction (XRD) and UV-vis diffuse reflectance spectroscopy (UV-DRS). Degradation of methyl orange was employed to investigate the photocatalytic activity of the products. Results show that, among the samples with different concentrations of WO3, W10T with the atomic ratio W/Ti of 10% presents optimal degradation rate. This degradation rate is about 95% within 2h under UV light irradiation, which is much higher than that of pure TiO2 nanotubes. |
| Author | Su, Ge Gao, Rongjie Dong, Bohua Liu, Wei Sun, Hui Song, Liang Cao, Lixin |
| Author_xml | – sequence: 1 givenname: Hui surname: Sun fullname: Sun, Hui email: sunhuichn@hotmail.com – sequence: 2 givenname: Bohua surname: Dong fullname: Dong, Bohua email: dongbohua@ouc.edu.cn – sequence: 3 givenname: Ge surname: Su fullname: Su, Ge email: gesu@ouc.edu.cn – sequence: 4 givenname: Rongjie surname: Gao fullname: Gao, Rongjie email: dmh206@ouc.edu.cn – sequence: 5 givenname: Wei surname: Liu fullname: Liu, Wei email: weiliu@ouc.edu.cn – sequence: 6 givenname: Liang surname: Song fullname: Song, Liang email: songliang@qibebt.ac.cn – sequence: 7 givenname: Lixin surname: Cao fullname: Cao, Lixin email: caolixin@mail.ouc.edu.cn |
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| Snippet | •WO3/titania nanotubes are synthesized at low temperature (383K) by a novel approach.•WO3/titania nanotubes present enhanced photocatalytic activity.•The... WO3/TiO2 nanotubular composite was synthesized at low temperature (383K) by a novel approach. WO3 nanoparticles were loaded on anatase TiO2 nanotubes through... |
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| SubjectTerms | Ammonium paratungstate Degradation Hydrothermal Nanostructure Nanotubes Photocatalysis Photocatalytic activity Reflectance Titanium Titanium dioxide Tungsten oxides WO3/TiO2 nanotubes |
| Title | Modification of TiO2 nanotubes by WO3 species for improving their photocatalytic activity |
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