Analysis of 500-ng/l levels of bromate in drinking water by direct-injection suppressed ion chromatography coupled with a single, pneumatically delivered post-column reagent
In July 1997, the US Environmental Protection Agency (EPA) began sampling and analyzing drinking water matrices from US municipalities serving populations greater than 100 000 for low-level bromate (>0.20 μg/l) in support of the Information Collection Rule (ICR) using the selective anion concentr...
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Published in | Journal of Chromatography A Vol. 850; no. 1; pp. 119 - 129 |
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Main Authors | , , , |
Format | Journal Article Conference Proceeding |
Language | English |
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Elsevier B.V
30.07.1999
Elsevier |
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Abstract | In July 1997, the US Environmental Protection Agency (EPA) began sampling and analyzing drinking water matrices from US municipalities serving populations greater than 100 000 for low-level bromate (>0.20 μg/l) in support of the Information Collection Rule (ICR) using the selective anion concentration (SAC) method. In September 1997, EPA published Method 300.1 which lowered the Method 300.0 bromate method detection limit (MDL) from 20.0 to 1.4 μg/l. This paper describes the research conducted at the EPA’s Technical Support Center laboratory investigating a single post-column reagent,
o-dianisidine (ODA), which has been successfully coupled to EPA Method 300.1 to extend the MDL for bromate. Initial studies indicate that this method offers a MDL which approaches the EPA’s SAC method with the added benefit of increased specificity, shortened analysis time and reduced sample preparation. The method provides excellent ruggedness and acceptable precision and accuracy with a bromate MDL in reagent water of 0.1 μg/l, and a method reporting limit of 0.50 μg/l. |
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AbstractList | In July 1997, the US Environmental Protection Agency (EPA) began sampling and analyzing drinking water matrices from US municipalities serving populations greater than 100,000 for low-level bromate (> 0.20 microgram/l) in support of the Information Collection Rule (ICR) using the selective anion concentration (SAC) method. In September 1997, EPA published Method 300.1 which lowered the Method 300.0 bromate method detection limit (MDL) from 20.0 to 1.4 micrograms/l. This paper describes the research conducted at the EPA's Technical Support Center laboratory investigating a single post-column reagent, o-dianisidine (ODA), which has been successfully coupled to EPA Method 300.1 to extend the MDL for bromate. Initial studies indicate that this method offers a MDL which approaches the EPA's SAC method with the added benefit of increased specificity, shortened analysis time and reduced sample preparation. The method provides excellent ruggedness and acceptable precision and accuracy with a bromate MDL in reagent water of 0.1 microgram/l, and a method reporting limit of 0.50 microgram/l. In July 1997, the US Environmental Protection Agency (EPA) began sampling and analyzing drinking water matrices from US municipalities serving populations greater than 100,000 for low-level bromate (> 0.20 microgram/l) in support of the Information Collection Rule (ICR) using the selective anion concentration (SAC) method. In September 1997, EPA published Method 300.1 which lowered the Method 300.0 bromate method detection limit (MDL) from 20.0 to 1.4 micrograms/l. This paper describes the research conducted at the EPA's Technical Support Center laboratory investigating a single post-column reagent, o-dianisidine (ODA), which has been successfully coupled to EPA Method 300.1 to extend the MDL for bromate. Initial studies indicate that this method offers a MDL which approaches the EPA's SAC method with the added benefit of increased specificity, shortened analysis time and reduced sample preparation. The method provides excellent ruggedness and acceptable precision and accuracy with a bromate MDL in reagent water of 0.1 microgram/l, and a method reporting limit of 0.50 microgram/l. In July 1997, the US Environmental Protection Agency (EPA) began sampling and analyzing drinking water matrices from US municipalities serving populations greater than 100 000 for low-level bromate (>0.20 μg/l) in support of the Information Collection Rule (ICR) using the selective anion concentration (SAC) method. In September 1997, EPA published Method 300.1 which lowered the Method 300.0 bromate method detection limit (MDL) from 20.0 to 1.4 μg/l. This paper describes the research conducted at the EPA’s Technical Support Center laboratory investigating a single post-column reagent, o-dianisidine (ODA), which has been successfully coupled to EPA Method 300.1 to extend the MDL for bromate. Initial studies indicate that this method offers a MDL which approaches the EPA’s SAC method with the added benefit of increased specificity, shortened analysis time and reduced sample preparation. The method provides excellent ruggedness and acceptable precision and accuracy with a bromate MDL in reagent water of 0.1 μg/l, and a method reporting limit of 0.50 μg/l. |
Author | Wagner, Herbert P Hautman, Daniel P Munch, David J Pepich, Barry V |
Author_xml | – sequence: 1 givenname: Herbert P surname: Wagner fullname: Wagner, Herbert P organization: ICF Kaiser Environmental and Facilities Management Group, 26 W. Martin Luther King Drive, Cincinnati, OH 45219, USA – sequence: 2 givenname: Barry V surname: Pepich fullname: Pepich, Barry V organization: ICF Kaiser Environmental and Facilities Management Group, 26 W. Martin Luther King Drive, Cincinnati, OH 45219, USA – sequence: 3 givenname: Daniel P surname: Hautman fullname: Hautman, Daniel P organization: US Environmental Protection Agency, Office of Ground Water and Drinking Water, 26 W. Martin Luther King Drive, Cincinnati, OH 45268, USA – sequence: 4 givenname: David J surname: Munch fullname: Munch, David J organization: US Environmental Protection Agency, Office of Ground Water and Drinking Water, 26 W. Martin Luther King Drive, Cincinnati, OH 45268, USA |
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Keywords | Dianisidine Derivatization, LC Water analysis Bromate Inorganic anions Drinking water treatment Drinking water Chemical analysis Bromates Interference Disinfection Derivatization Postcolumn Carcinogen Ozonization Ion chromatography Inorganic anion Sample preparation By product Quantitative analysis Ultraviolet visible spectrometry |
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SubjectTerms | Analytical chemistry Applied sciences Biological and medical sciences Borates - analysis Bromate Bromides - chemistry Carcinogenesis, carcinogens and anticarcinogens Chemical agents Chemistry Chlorides - chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Ion Exchange - instrumentation Chromatography, Ion Exchange - methods Dianisidine Dianisidine - chemistry Drinking water and swimming-pool water. Desalination Exact sciences and technology Indicators and Reagents Inorganic anions Medical sciences Nitric Acid - chemistry Other chromatographic methods Pollution Potassium Compounds - chemistry Quality Control Software Temperature Tumors Water - chemistry Water treatment and pollution |
Title | Analysis of 500-ng/l levels of bromate in drinking water by direct-injection suppressed ion chromatography coupled with a single, pneumatically delivered post-column reagent |
URI | https://dx.doi.org/10.1016/S0021-9673(99)00031-X https://www.ncbi.nlm.nih.gov/pubmed/10457472 https://search.proquest.com/docview/69988501 |
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