Dislocation structure evolution during room temperature dwell loading of a Ti-6Al-4 V alloy

• Published in: Materials characterization Vol. 209; p. 113757
• Main Authors: Cizek, Pavel, Kada, Sitarama R., Wang, Jun, Armstrong, Nicholas, Antoniou, Ross A., Slater, Sonya, Lynch, Peter A.
• Format: Journal Article
• Language: English
• Published: Elsevier Inc 01.03.2024
• Subjects: Characterization; Electron microscopy; Plasticity; Titanium alloys; Characterization; Titanium alloys; Electron microscopy; Plasticity
• DOI: 10.1016/j.matchar.2024.113757
• ISSN: 1044-5803

The current work examines the evolution of the dislocation structure, within both the α and β phases, of a Ti-6Al-4 V alloy subjected to room temperature dwell loading performed at about 96% of the macroscopic yield stress level for several durations, as part of a synchrotron in-situ deformation experiment. The obtained findings represent a vital contribution to creating a scientific basis for improving lifing predictions for aero-propulsion components. The dislocation configuration, type and density were examined post-mortem using transmission electron microscopy (TEM). Despite the relatively low applied stress level, well-developed dislocation structures were already formed within the α phase at a dwell duration of 10 min and changed only modestly up to 60 min. The plastic deformation of the above phase took place solely via dislocation slip. To facilitate a comparison between different dwell durations, the TEM investigation focused on the regions oriented for the prismatic glide that represented the main deformation mode due to the starting crystallographic texture. After deformation, the regions oriented for the prismatic slip contained planar slip bands largely consisting of dislocations of a screw type. There was rather limited interaction between different bands, as the dislocation arrays passed through the slip band intersections with only minor difficulty. The screw-type dislocations seemed to preferentially form during straining. Dislocation Burgers vectors experimentally determined within the β phase occasionally departed from the Schmid rule and such dislocations typically showed a prevalent screw component. Some deformation banding and {112} 〈111〉 − type mechanical twin formation were locally detected within the β phase. •Dislocation structure within the β phase developed faster during dwell holding.•The α and β phase dislocations largely possessed a dominant screw component.•Screw dislocations within the α phase were preferentially created during straining.•The studied α prismatic slip dislocation arrays were planar and interacted weekly.•The Burgers vectors within the β phase did not strictly follow the Schmid rule.