Fabrication of acrylamide decorated superhydrophilic and underwater superoleophobic poly(vinylidene fluoride) membranes for oil/water emulsion separation

•The water flux of PVDF/Al2O3 hybrid membrane was greatly improved.•The "needle-shaped" PAM on the membrane surface increases roughness.•The modified membrane has superhydrophilicity and underwater superoleophobicity.•The flux recovery rate of PVDF/Al2O3/PAM membrane is exceeded 83%. Here...

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Published inJournal of the Taiwan Institute of Chemical Engineers Vol. 95; pp. 300 - 307
Main Authors Liu, Siwei, Zhou, Zhiping, Zhou, Shi, Cui, Jiuyun, Wang, Qingqing, Zhang, Yufeng, Lang, Jihui, Yan, Yongsheng
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.02.2019
Subjects
High flux
Oil/water separation
PVDF membrane
Superhydrophilic
Underwater superoleophobic
High flux
Underwater superoleophobic
Oil/water separation
PVDF membrane
Superhydrophilic
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Abstract •The water flux of PVDF/Al2O3 hybrid membrane was greatly improved.•The "needle-shaped" PAM on the membrane surface increases roughness.•The modified membrane has superhydrophilicity and underwater superoleophobicity.•The flux recovery rate of PVDF/Al2O3/PAM membrane is exceeded 83%. Here we have successfully fabricated the superhydrophilic and underwater superoleophobic PVDF/Al2O3/PAM membranes by constructed "needle-shaped" PAM on the PVDF/Al2O3 hybrid membranes surface through ATRP technology. The modified membranes were characterized by the Fourier-transform infrared (FT-IR), X-ray diffraction (XRD) and X-ray photoelectron spectra (XPS) that the AIP has been hydrolyzed to Al2O3 and AM has successfully polymerized on the membrane surface. When the PVDF/Al2O3/PAM membranes were applied in oil/water emulsion separation, the separation efficiencies were more than 99.1% and the maximum flux of the emulsion was 5874L/ m/2/h/bar. In the anti-fouling performance experiment, the flux recovery ration (FRR) of the PVDF/Al2O3/PAM membranes could still reach 83.46% after eight cycles. Therefore, the PVDF/Al2O3/PAM membranes have high separation efficiency and high flux performance for separating oil-water emulsions, and steadily anti-oil performance is suitable for practical applications. [Display omitted] Schematic illustration of preparation of the PVDF/Al2O3/PAM membrane, underwater-oil CA on the surface of different membranes, and optical microscopy images of the emulsion before and after filtration.
AbstractList •The water flux of PVDF/Al2O3 hybrid membrane was greatly improved.•The "needle-shaped" PAM on the membrane surface increases roughness.•The modified membrane has superhydrophilicity and underwater superoleophobicity.•The flux recovery rate of PVDF/Al2O3/PAM membrane is exceeded 83%. Here we have successfully fabricated the superhydrophilic and underwater superoleophobic PVDF/Al2O3/PAM membranes by constructed "needle-shaped" PAM on the PVDF/Al2O3 hybrid membranes surface through ATRP technology. The modified membranes were characterized by the Fourier-transform infrared (FT-IR), X-ray diffraction (XRD) and X-ray photoelectron spectra (XPS) that the AIP has been hydrolyzed to Al2O3 and AM has successfully polymerized on the membrane surface. When the PVDF/Al2O3/PAM membranes were applied in oil/water emulsion separation, the separation efficiencies were more than 99.1% and the maximum flux of the emulsion was 5874L/ m/2/h/bar. In the anti-fouling performance experiment, the flux recovery ration (FRR) of the PVDF/Al2O3/PAM membranes could still reach 83.46% after eight cycles. Therefore, the PVDF/Al2O3/PAM membranes have high separation efficiency and high flux performance for separating oil-water emulsions, and steadily anti-oil performance is suitable for practical applications. [Display omitted] Schematic illustration of preparation of the PVDF/Al2O3/PAM membrane, underwater-oil CA on the surface of different membranes, and optical microscopy images of the emulsion before and after filtration.
Author Liu, Siwei
Lang, Jihui
Zhang, Yufeng
Zhou, Shi
Yan, Yongsheng
Zhou, Zhiping
Wang, Qingqing
Cui, Jiuyun
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Keywords High flux
Underwater superoleophobic
Oil/water separation
PVDF membrane
Superhydrophilic
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Snippet •The water flux of PVDF/Al2O3 hybrid membrane was greatly improved.•The "needle-shaped" PAM on the membrane surface increases roughness.•The modified membrane...
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SubjectTerms High flux
Oil/water separation
PVDF membrane
Superhydrophilic
Underwater superoleophobic
Title Fabrication of acrylamide decorated superhydrophilic and underwater superoleophobic poly(vinylidene fluoride) membranes for oil/water emulsion separation
URI https://dx.doi.org/10.1016/j.jtice.2018.07.015
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