Selective and continuous ion recovery using flow electrode capacitive deionization with polymer multilayers functionalized ion exchange membrane
Flow electrode capacitive deionization (FCDI) is a newly developed salt removal technology that overcomes the limitations of conventional CDI by eliminating the need for a discharging process, thus achieving much higher desalination capacity and a continuous desalination operation. In this study, we...
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Published in | Desalination Vol. 558; p. 116626 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
15.07.2023
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Abstract | Flow electrode capacitive deionization (FCDI) is a newly developed salt removal technology that overcomes the limitations of conventional CDI by eliminating the need for a discharging process, thus achieving much higher desalination capacity and a continuous desalination operation. In this study, we aimed to achieve selective and continuous sodium recovery from Na+/Ca2+ mixtures through FCDI by utilizing polymer multilayer functionalized cation-exchange membranes (CEM). A layer-by-layer method was used to deposit polymer multilayers consisting of PAH (poly allylamine hydrochloride) and PSS (poly styrene sulfonate) on the CEM. Changes in the concentration of feed electrolyte, number of coated polymer layers, and type of outermost layer were investigated in terms of their effect on the selective ion separation. The functionalized CEM switches from a divalent ion affinity to a monovalent ion affinity due to their different ion sizes and charge densities. As the number of polymer layers increased, the selectivity of Na+/Ca2+ increased, reaching up to 3.26 from 0.16 for pristine CEM. We believe that our approach can provide insight into the selective recovery of valuable materials including lithium-ion battery recycling, the recovery of noble metals, and the separation of toxic ions using the FCDI system.
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•Selective ion recovery was realized by FCDI using a functionalized membrane.•PAH/PSS polymer multilayers were successfully deposited onto an ion exchange membrane.•The multilayer coating changed the affinity of the FCDI system from divalent to monovalent.•Na/Ca selectivity increased from 0.16 to 3.26 as a result of multilayer coating. |
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AbstractList | Flow electrode capacitive deionization (FCDI) is a newly developed salt removal technology that overcomes the limitations of conventional CDI by eliminating the need for a discharging process, thus achieving much higher desalination capacity and a continuous desalination operation. In this study, we aimed to achieve selective and continuous sodium recovery from Na+/Ca2+ mixtures through FCDI by utilizing polymer multilayer functionalized cation-exchange membranes (CEM). A layer-by-layer method was used to deposit polymer multilayers consisting of PAH (poly allylamine hydrochloride) and PSS (poly styrene sulfonate) on the CEM. Changes in the concentration of feed electrolyte, number of coated polymer layers, and type of outermost layer were investigated in terms of their effect on the selective ion separation. The functionalized CEM switches from a divalent ion affinity to a monovalent ion affinity due to their different ion sizes and charge densities. As the number of polymer layers increased, the selectivity of Na+/Ca2+ increased, reaching up to 3.26 from 0.16 for pristine CEM. We believe that our approach can provide insight into the selective recovery of valuable materials including lithium-ion battery recycling, the recovery of noble metals, and the separation of toxic ions using the FCDI system.
[Display omitted]
•Selective ion recovery was realized by FCDI using a functionalized membrane.•PAH/PSS polymer multilayers were successfully deposited onto an ion exchange membrane.•The multilayer coating changed the affinity of the FCDI system from divalent to monovalent.•Na/Ca selectivity increased from 0.16 to 3.26 as a result of multilayer coating. |
ArticleNumber | 116626 |
Author | Kim, Youna Kang, Hong Suk Hong, Jinkee Jung, Hye Bin Huynh, Van Phung Tran, Nguyen Anh Thu Cho, Younghuyn Yoo, Chung-Yul Khoi, Tran Minh |
Author_xml | – sequence: 1 givenname: Tran Minh surname: Khoi fullname: Khoi, Tran Minh organization: Department of Energy Systems, Soonchunhyang University, Asan 31538, Republic of Korea – sequence: 2 givenname: Nguyen Anh Thu surname: Tran fullname: Tran, Nguyen Anh Thu organization: Department of Energy Systems, Soonchunhyang University, Asan 31538, Republic of Korea – sequence: 3 givenname: Hye Bin surname: Jung fullname: Jung, Hye Bin organization: Department of Energy Systems, Soonchunhyang University, Asan 31538, Republic of Korea – sequence: 4 givenname: Van Phung surname: Huynh fullname: Huynh, Van Phung organization: Department of Energy Systems, Soonchunhyang University, Asan 31538, Republic of Korea – sequence: 5 givenname: Youna surname: Kim fullname: Kim, Youna organization: Department of Chemical & Biomolecular Engineering, Yonsei University, Seoul 03722, Republic of Korea – sequence: 6 givenname: Jinkee surname: Hong fullname: Hong, Jinkee organization: Department of Chemical & Biomolecular Engineering, Yonsei University, Seoul 03722, Republic of Korea – sequence: 7 givenname: Chung-Yul surname: Yoo fullname: Yoo, Chung-Yul email: chungyulyoo@mokpo.ac.kr organization: Department of Chemistry, Mokpo National University, 1666 Yeongsan-ro, Cheonggye-myeon, Muan-gun, Jeollanamdo 58554, Republic of Korea – sequence: 8 givenname: Hong Suk surname: Kang fullname: Kang, Hong Suk email: hskang@inha.ac.kr organization: Department of Polymer Science and Engineering and Program in Environmental and Polymer Engineering, Inha University, Incheon 22212, Republic of Korea – sequence: 9 givenname: Younghuyn surname: Cho fullname: Cho, Younghuyn email: yhcho@sch.ac.kr organization: Department of Energy Systems, Soonchunhyang University, Asan 31538, Republic of Korea |
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Keywords | Selective ion recovery Layer-by-layer deposition Flow electrode capacitive deionization Desalination Polymer multilayers |
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Snippet | Flow electrode capacitive deionization (FCDI) is a newly developed salt removal technology that overcomes the limitations of conventional CDI by eliminating... |
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SubjectTerms | Desalination Flow electrode capacitive deionization Layer-by-layer deposition Polymer multilayers Selective ion recovery |
Title | Selective and continuous ion recovery using flow electrode capacitive deionization with polymer multilayers functionalized ion exchange membrane |
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