Fabrication of PbFe12O19 nanoparticles and study of their structural, magnetic and dielectric properties

In this study, M-type Lead hexaferrite (PbFe12O19) nanoparticles were prepared by a sol–gel method and the prepared powders were annealed at 700–1000°C for 1, 1.5, 2, 2.5 and 3h. The Lead hexaferrite powders were characterized using thermogravimetry-differential thermal analysis, X-ray diffraction,...

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Published inJournal of magnetism and magnetic materials Vol. 399; pp. 130 - 142
Main Authors Mousavi Ghahfarokhi, S.E., Rostami, Z.A., Kazeminezhad, I.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.02.2016
Subjects
Annealing temperature
Annealing time
Dielectic properties
Lead hexaferrite nanoparticles
Magnetic properties
Structure properties
Annealing temperature
Structure properties
Lead hexaferrite nanoparticles
Dielectic properties
Annealing time
Magnetic properties
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Abstract In this study, M-type Lead hexaferrite (PbFe12O19) nanoparticles were prepared by a sol–gel method and the prepared powders were annealed at 700–1000°C for 1, 1.5, 2, 2.5 and 3h. The Lead hexaferrite powders were characterized using thermogravimetry-differential thermal analysis, X-ray diffraction, scanning electron microscopy, LCR meter, vibrating sample magnetometer, and Fourier transforms infrared spectroscopy. The size of the nanoparticles was increased with the annealing temparature. The results reveal that the best annealing temperature and annealing time for preparing PbFe12O19 nanoparticles at 800°C and 3h are obtained. The infrared spectra measured in range of 4000–400cm−1 exhibit stretching modes of metal ions in tetrahedral site at 580–550cm−1 and octahedral site at 470–430cm−1. The variation in ac conductivity (σac) with frequency shows that the electrical conductivity in these ferrites is mainly attributed to the electron hopping mechanism. [Display omitted] •We synthesize M-type Lead hexaferrite (PbFe12O19) by sol–gel method..•We study the role of annealing temperature and annealing time on the morphology, size, structure, magnetic and dielectric properties of PbFe12O10 nanoparticles.•The results of dielectric measurement of all samples show that with increasing frequency, dielectric constant, dielectric loss, and electrical ac conductivity decreases.
AbstractList In this study, M-type Lead hexaferrite (PbFe12O19) nanoparticles were prepared by a sol–gel method and the prepared powders were annealed at 700–1000°C for 1, 1.5, 2, 2.5 and 3h. The Lead hexaferrite powders were characterized using thermogravimetry-differential thermal analysis, X-ray diffraction, scanning electron microscopy, LCR meter, vibrating sample magnetometer, and Fourier transforms infrared spectroscopy. The size of the nanoparticles was increased with the annealing temparature. The results reveal that the best annealing temperature and annealing time for preparing PbFe12O19 nanoparticles at 800°C and 3h are obtained. The infrared spectra measured in range of 4000–400cm−1 exhibit stretching modes of metal ions in tetrahedral site at 580–550cm−1 and octahedral site at 470–430cm−1. The variation in ac conductivity (σac) with frequency shows that the electrical conductivity in these ferrites is mainly attributed to the electron hopping mechanism. [Display omitted] •We synthesize M-type Lead hexaferrite (PbFe12O19) by sol–gel method..•We study the role of annealing temperature and annealing time on the morphology, size, structure, magnetic and dielectric properties of PbFe12O10 nanoparticles.•The results of dielectric measurement of all samples show that with increasing frequency, dielectric constant, dielectric loss, and electrical ac conductivity decreases.
Author Rostami, Z.A.
Mousavi Ghahfarokhi, S.E.
Kazeminezhad, I.
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  email: I.kazeminezhad@scu.ac.ir
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Keywords Annealing temperature
Structure properties
Lead hexaferrite nanoparticles
Dielectic properties
Annealing time
Magnetic properties
Language English
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Snippet In this study, M-type Lead hexaferrite (PbFe12O19) nanoparticles were prepared by a sol–gel method and the prepared powders were annealed at 700–1000°C for 1,...
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elsevier
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StartPage 130
SubjectTerms Annealing temperature
Annealing time
Dielectic properties
Lead hexaferrite nanoparticles
Magnetic properties
Structure properties
Title Fabrication of PbFe12O19 nanoparticles and study of their structural, magnetic and dielectric properties
URI https://dx.doi.org/10.1016/j.jmmm.2015.09.063
Volume 399
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