Green production of silica hydroxyl riched palygorskite by shear-assisted supercritical CO2 separation process for dye adsorption and heavy oil viscosity reduction

A green shear-assisted rapid depressurization process was developed to produce highly-dispersed palygorskite (Pal) nanorods with abundant silica hydroxyl (Si-OH) groups by using supercritical CO2 (ScCO2) treatment. The disentangled Pal (DPal) nanorods prepared by ScCO2 were obtained with small parti...

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Published inApplied clay science Vol. 212; p. 106207
Main Authors Li, Dingyao, Li, Yun, Yang, Fan, Tian, Xiaojuan, Che, Sai, Wang, Yifan, Bao, Weijie, Lv, Guangwei, Xu, Chong, Sun, Yankun, Yan, Xingru, Deng, Bijian, Lu, Yi, Li, Yongfeng
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.10.2021
Subjects
Adsorption
Palygorskite
Silica hydroxyl
Supercritical CO2
Viscosity reduction
Viscosity reduction
Adsorption
Palygorskite
Supercritical CO2
Silica hydroxyl
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Abstract A green shear-assisted rapid depressurization process was developed to produce highly-dispersed palygorskite (Pal) nanorods with abundant silica hydroxyl (Si-OH) groups by using supercritical CO2 (ScCO2) treatment. The disentangled Pal (DPal) nanorods prepared by ScCO2 were obtained with small particle sizes and high dispersity, and confirmed by electron microscopy and particle size analysis. Higher zeta potential and smaller contact angle were achieved for DPal due to the efficient exposure of Si-OH groups, consistent with the better rheological property as well as the higher adsorption of methylene blue (88%) and rhodamine B (86%). The nano viscosity reducer synthesized by DPal achieved a high viscosity reduction rate of 95% with Liaohe heavy oil, attributed to the higher degree of modification due to the increased Si-OH groups and the stronger aggregation effect on wax crystal caused by the nano viscosity reducer. The disentangled and modified Pal demonstrated great potential in dye adsorption and heavy oil viscosity reduction applications. The rod-shaped palygorskite is disentangled by the shear-assisted ScCO2 separation process. The obtained nanorods shows preserved crystal structure and high disagreegation degree. The disentangled palygorskite presents excellent adsorption capacity, and the further synthsized nano visocosity reducer shows a high viscosity reduction rate with Liaohe crude olil. [Display omitted] •Shear-assisted ScCO2 separation method produces vertical and horizontal forces.•The disentangled palygorskite achieves the effective exposure of Si-OH groups.•The disentangled palygorskite possesses the excellent adsorption for dyes.•The prepared nano viscosity reducer obtains a viscosity reduction rate of 95%.
AbstractList A green shear-assisted rapid depressurization process was developed to produce highly-dispersed palygorskite (Pal) nanorods with abundant silica hydroxyl (Si-OH) groups by using supercritical CO2 (ScCO2) treatment. The disentangled Pal (DPal) nanorods prepared by ScCO2 were obtained with small particle sizes and high dispersity, and confirmed by electron microscopy and particle size analysis. Higher zeta potential and smaller contact angle were achieved for DPal due to the efficient exposure of Si-OH groups, consistent with the better rheological property as well as the higher adsorption of methylene blue (88%) and rhodamine B (86%). The nano viscosity reducer synthesized by DPal achieved a high viscosity reduction rate of 95% with Liaohe heavy oil, attributed to the higher degree of modification due to the increased Si-OH groups and the stronger aggregation effect on wax crystal caused by the nano viscosity reducer. The disentangled and modified Pal demonstrated great potential in dye adsorption and heavy oil viscosity reduction applications. The rod-shaped palygorskite is disentangled by the shear-assisted ScCO2 separation process. The obtained nanorods shows preserved crystal structure and high disagreegation degree. The disentangled palygorskite presents excellent adsorption capacity, and the further synthsized nano visocosity reducer shows a high viscosity reduction rate with Liaohe crude olil. [Display omitted] •Shear-assisted ScCO2 separation method produces vertical and horizontal forces.•The disentangled palygorskite achieves the effective exposure of Si-OH groups.•The disentangled palygorskite possesses the excellent adsorption for dyes.•The prepared nano viscosity reducer obtains a viscosity reduction rate of 95%.
ArticleNumber 106207
Author Tian, Xiaojuan
Li, Yun
Bao, Weijie
Che, Sai
Lv, Guangwei
Xu, Chong
Yang, Fan
Deng, Bijian
Li, Dingyao
Lu, Yi
Yan, Xingru
Li, Yongfeng
Sun, Yankun
Wang, Yifan
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Keywords Viscosity reduction
Adsorption
Palygorskite
Supercritical CO2
Silica hydroxyl
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Snippet A green shear-assisted rapid depressurization process was developed to produce highly-dispersed palygorskite (Pal) nanorods with abundant silica hydroxyl...
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elsevier
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Publisher
StartPage 106207
SubjectTerms Adsorption
Palygorskite
Silica hydroxyl
Supercritical CO2
Viscosity reduction
Title Green production of silica hydroxyl riched palygorskite by shear-assisted supercritical CO2 separation process for dye adsorption and heavy oil viscosity reduction
URI https://dx.doi.org/10.1016/j.clay.2021.106207
Volume 212
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