Comparative study of in-situ formation process of Mg-Al layered double hydroxides though two pathways to remove Cr(VI) and As(V) from wastewater
The method of direct synthesis of layered double hydroxide (LDHs) in wastewater has attracted wide attention, but the formation process and removal mechanism are still unclear. In this study, two different paths of alkali solution (NaOH) dropped to salt solution (Mg2+/Al3+) (A-S process) and salt so...
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Published in | Journal of environmental chemical engineering Vol. 11; no. 5; p. 111043 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.10.2023
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Abstract | The method of direct synthesis of layered double hydroxide (LDHs) in wastewater has attracted wide attention, but the formation process and removal mechanism are still unclear. In this study, two different paths of alkali solution (NaOH) dropped to salt solution (Mg2+/Al3+) (A-S process) and salt solution dropped to alkali solution (S-A process) were proposed to directly synthesize LDHs in wastewater and remove contaminants Cr(VI)/As(V) simultaneously. In A-S process, the formation of LDHs could be divided into three stages: initial formation of amorphous Al(OH)3, crystal phase transformation, and the complete formation of LDHs crystal. There was a gradual incorporation of Mg into Al(OH)3, and the removal of Cr(VI)/As(V) significantly increased upon the formation of LDHs structure. However, in S-A process, the formation of LDHs primarily involved crystal structure optimization. The layered structure was constantly growing and optimizing, accompanied by the removal of Cr(VI)/As(V). The Competition removal experiment of Cr(VI)/As(V) indicated that As(V) preferentially possess active sites and occupied more high-energy sites analyzed by molecular simulation and site energy distribution theory. The experimental investigation of co-existing ions, pH and recycle experiment for practical performance were also examined and demonstrated a high stability and a good recyclability.
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LDHs directly form in wastewater and remove Cr(VI)/As(V) synchronously.Two distinct paths of LDHs formation process are comparatively investigated.Synchrotron radiation FTIR is used to analyze crystal phase transition process.Different paths of LDHs formation produce discrepant charge density.The preferential removal of As(V) is analyzed by molecular simulation. |
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AbstractList | The method of direct synthesis of layered double hydroxide (LDHs) in wastewater has attracted wide attention, but the formation process and removal mechanism are still unclear. In this study, two different paths of alkali solution (NaOH) dropped to salt solution (Mg2+/Al3+) (A-S process) and salt solution dropped to alkali solution (S-A process) were proposed to directly synthesize LDHs in wastewater and remove contaminants Cr(VI)/As(V) simultaneously. In A-S process, the formation of LDHs could be divided into three stages: initial formation of amorphous Al(OH)3, crystal phase transformation, and the complete formation of LDHs crystal. There was a gradual incorporation of Mg into Al(OH)3, and the removal of Cr(VI)/As(V) significantly increased upon the formation of LDHs structure. However, in S-A process, the formation of LDHs primarily involved crystal structure optimization. The layered structure was constantly growing and optimizing, accompanied by the removal of Cr(VI)/As(V). The Competition removal experiment of Cr(VI)/As(V) indicated that As(V) preferentially possess active sites and occupied more high-energy sites analyzed by molecular simulation and site energy distribution theory. The experimental investigation of co-existing ions, pH and recycle experiment for practical performance were also examined and demonstrated a high stability and a good recyclability.
[Display omitted]
LDHs directly form in wastewater and remove Cr(VI)/As(V) synchronously.Two distinct paths of LDHs formation process are comparatively investigated.Synchrotron radiation FTIR is used to analyze crystal phase transition process.Different paths of LDHs formation produce discrepant charge density.The preferential removal of As(V) is analyzed by molecular simulation. |
ArticleNumber | 111043 |
Author | Zhang, Zihan Wang, Yu Kong, Fanping Xie, Yuan Huang, Hanhan Meng, Zilin Liu, Huiqiang Ma, Zequn |
Author_xml | – sequence: 1 givenname: Yuan surname: Xie fullname: Xie, Yuan organization: School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo, PR China – sequence: 2 givenname: Hanhan surname: Huang fullname: Huang, Hanhan organization: School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo, PR China – sequence: 3 givenname: Zihan surname: Zhang fullname: Zhang, Zihan organization: School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo, PR China – sequence: 4 givenname: Yu surname: Wang fullname: Wang, Yu organization: School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo, PR China – sequence: 5 givenname: Fanping surname: Kong fullname: Kong, Fanping organization: School of Agricultural Engineering and Food Science, Shandong University of Technology, Zibo, PR China – sequence: 6 givenname: Zequn surname: Ma fullname: Ma, Zequn organization: School of Materials Science and Engineering, Suzhou University of Science and Technology, Suzhou, PR China – sequence: 7 givenname: Huiqiang surname: Liu fullname: Liu, Huiqiang email: liuhq@sdut.edu.cn organization: School of Physics and Optoelectronic Engineering, Shandong University of Technology, Zibo, PR China – sequence: 8 givenname: Zilin surname: Meng fullname: Meng, Zilin email: mzl@sdut.edu.cn organization: School of Resources and Environmental Engineering, Shandong University of Technology, Zibo, PR China |
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Keywords | As(V) Cr(VI) Layered double hydroxide Formation mechanism |
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