Pilot test of Mn-Fe/Al2O3 catalytic ozonation in tertiary wastewater treatment
Heterogeneous catalytic ozonation has received increasing popularity in wastewater treatment across China. However, some challenges, such as metal leaching from catalysts, still exist. Meanwhile, it is lesser known about its removal efficiency of dissolved organic carbon and impact on biological tox...
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Published in | Journal of environmental chemical engineering Vol. 12; no. 2; p. 111937 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.04.2024
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Abstract | Heterogeneous catalytic ozonation has received increasing popularity in wastewater treatment across China. However, some challenges, such as metal leaching from catalysts, still exist. Meanwhile, it is lesser known about its removal efficiency of dissolved organic carbon and impact on biological toxicity in pilot-scale applications. Here we synthesized an Al-based catalyst (Mn-Fe/Al2O3) for catalytic ozonation in pilot-scale. Results of characterization show that Mn and Fe were effectively supported on porous alumina and formed chemical bonds. The catalytic ozonation process could generate hydroxyl radical, superoxide radical and singlet oxygen for the deep degradation of dissolved organic carbon. Its chemical oxygen demand removal efficiency (average removal of 14.5 mg/L) could meet the requirement of Discharge Standard of Pollutants for Municipal Wastewater Treatment Plant (GB 18918-2002) in China with acceptable metal leaching. The process also effectively removed dissolved organic carbon, especially the hydrophobic fractions (99 % removal). In toxicogenomics assay, the total transcriptional effect level index value for the effluent (1.40) was ≤ 1.50, indicating there was no obvious toxic effect for ecosystem. Based on economical estimation, the operational cost of the catalytic ozonation was 0.09 $/m3, much less than previous reported cases. This study provides convincing evidence for the effectiveness of Mn-Fe/Al2O3 catalytic ozonation in future wastewater treatment.
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•An Al-based catalyst was synthesized for catalytic ozonation in pilot-scale.•Mn-Fe/Al2O3 could generate reactive oxygen species to degrade organics.•Mn and Fe forming chemical bonds with porous alumina reduced metal leaching.•Toxicogenomics assay showed no obvious toxic effect via catalytic ozonation.•Operational cost of catalytic ozonation was less than previous reported cases. |
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AbstractList | Heterogeneous catalytic ozonation has received increasing popularity in wastewater treatment across China. However, some challenges, such as metal leaching from catalysts, still exist. Meanwhile, it is lesser known about its removal efficiency of dissolved organic carbon and impact on biological toxicity in pilot-scale applications. Here we synthesized an Al-based catalyst (Mn-Fe/Al2O3) for catalytic ozonation in pilot-scale. Results of characterization show that Mn and Fe were effectively supported on porous alumina and formed chemical bonds. The catalytic ozonation process could generate hydroxyl radical, superoxide radical and singlet oxygen for the deep degradation of dissolved organic carbon. Its chemical oxygen demand removal efficiency (average removal of 14.5 mg/L) could meet the requirement of Discharge Standard of Pollutants for Municipal Wastewater Treatment Plant (GB 18918-2002) in China with acceptable metal leaching. The process also effectively removed dissolved organic carbon, especially the hydrophobic fractions (99 % removal). In toxicogenomics assay, the total transcriptional effect level index value for the effluent (1.40) was ≤ 1.50, indicating there was no obvious toxic effect for ecosystem. Based on economical estimation, the operational cost of the catalytic ozonation was 0.09 $/m3, much less than previous reported cases. This study provides convincing evidence for the effectiveness of Mn-Fe/Al2O3 catalytic ozonation in future wastewater treatment.
[Display omitted]
•An Al-based catalyst was synthesized for catalytic ozonation in pilot-scale.•Mn-Fe/Al2O3 could generate reactive oxygen species to degrade organics.•Mn and Fe forming chemical bonds with porous alumina reduced metal leaching.•Toxicogenomics assay showed no obvious toxic effect via catalytic ozonation.•Operational cost of catalytic ozonation was less than previous reported cases. |
ArticleNumber | 111937 |
Author | Pan, Jian Niu, Xi-Zhi Yang, Heyun Wang, Haiqiang Guan, Baohong Zheng, Xing |
Author_xml | – sequence: 1 givenname: Jian surname: Pan fullname: Pan, Jian organization: College of Environmental Resources Science, Zhejiang University, Hangzhou 310058, China – sequence: 2 givenname: Xi-Zhi surname: Niu fullname: Niu, Xi-Zhi organization: Environmental Technology Innovation Center of Jiande, Hangzhou 311607, China – sequence: 3 givenname: Heyun surname: Yang fullname: Yang, Heyun organization: Xi’an University of Technology, Xi’an 710000, China – sequence: 4 givenname: Xing surname: Zheng fullname: Zheng, Xing organization: School of Environmental and Natural Resources, Zhejiang University of Science & Technology, Hangzhou 310023, China – sequence: 5 givenname: Baohong surname: Guan fullname: Guan, Baohong email: guanbaohong@zju.edu.cn organization: College of Environmental Resources Science, Zhejiang University, Hangzhou 310058, China – sequence: 6 givenname: Haiqiang surname: Wang fullname: Wang, Haiqiang email: haiqiangwang@zju.edu.cn organization: College of Environmental Resources Science, Zhejiang University, Hangzhou 310058, China |
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Keywords | Dissolved organic carbon Metal leaching Economical estimation Catalytic ozonation Toxicogenomics assay |
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Title | Pilot test of Mn-Fe/Al2O3 catalytic ozonation in tertiary wastewater treatment |
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