New iodoargentates with azole molecules: Syntheses, structural characterization and photoluminescence properties

In this article, two organic bases (dtb ​= ​1,4-di(1H-1,2,4-triazol-1-yl)benzene; mimb ​= ​1,2-bis((2-methyl-1H-imidazole-1-yl)methyl)benzen) were employed to solvethermally react with AgI in an strong acidic environment, creating two new hybrid haloargentates [pbmt]0.5[AgI2] 1 (pbmt2+ ​= ​1,1'...

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Published inJournal of solid state chemistry Vol. 306; p. 122748
Main Authors Li, Chun-Hong, Yu, Jie-Hui, Xu, Ji-Qing
Format Journal Article
LanguageEnglish
Published Elsevier Inc 01.02.2022
Subjects
Fluorescent photo(thermo)chromism
In situ N-alkylation
Iodoargentate
Photoluminescence
Iodoargentate
Fluorescent photo(thermo)chromism
In situ N-alkylation
Photoluminescence
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Abstract In this article, two organic bases (dtb ​= ​1,4-di(1H-1,2,4-triazol-1-yl)benzene; mimb ​= ​1,2-bis((2-methyl-1H-imidazole-1-yl)methyl)benzen) were employed to solvethermally react with AgI in an strong acidic environment, creating two new hybrid haloargentates [pbmt]0.5[AgI2] 1 (pbmt2+ ​= ​1,1'-(1,4-phenylene)bis(4-methyl-1H-1,2,4-triazol-4-ium)) and [H2(mimb)]0.5[Ag2I3] 2. Note that pbmt2+ in 1 originated from the in situ N-alkylation of dtb with CH3OH. X-ray single-crystal diffraction analysis reveals that (i) 1 exhibits 1-D chain structure, which can be described as an infinite extension of AgI4 tetrahedra via sharing edge; (ii) in 2, Ag+ and I− aggregate to form a 3-D iodoargentate with open-framework structure. The photoluminescence analysis reveals that at room temperature, 1 emits yellow light, while at low temperature, it just occasionally emits yellow light, and in most cases it emits yellow-green light. Whether at room temperature or low temperature, 2 always emits yellow light. It means that 1 possesses the fluorescent photo(thermo)chromic properties, whereas 2 does not have these properties. The related mechanism was also discussed. Structures of two new azole-based hybrid iodoargentates (1 and 2) are reported. 1 is found to possess fluorescent photo(thermo)chromic properties. [Display omitted] •Azole molecules and their in-situ N-alkylation have employed in the construction of hybrid materials.•The photoluminescence behavior of two hybrids at different excitation wavelengths and low temperature was studied.•Iodoargentate possesses the fluorescent photo(thermo)chromic properties.
AbstractList In this article, two organic bases (dtb ​= ​1,4-di(1H-1,2,4-triazol-1-yl)benzene; mimb ​= ​1,2-bis((2-methyl-1H-imidazole-1-yl)methyl)benzen) were employed to solvethermally react with AgI in an strong acidic environment, creating two new hybrid haloargentates [pbmt]0.5[AgI2] 1 (pbmt2+ ​= ​1,1'-(1,4-phenylene)bis(4-methyl-1H-1,2,4-triazol-4-ium)) and [H2(mimb)]0.5[Ag2I3] 2. Note that pbmt2+ in 1 originated from the in situ N-alkylation of dtb with CH3OH. X-ray single-crystal diffraction analysis reveals that (i) 1 exhibits 1-D chain structure, which can be described as an infinite extension of AgI4 tetrahedra via sharing edge; (ii) in 2, Ag+ and I− aggregate to form a 3-D iodoargentate with open-framework structure. The photoluminescence analysis reveals that at room temperature, 1 emits yellow light, while at low temperature, it just occasionally emits yellow light, and in most cases it emits yellow-green light. Whether at room temperature or low temperature, 2 always emits yellow light. It means that 1 possesses the fluorescent photo(thermo)chromic properties, whereas 2 does not have these properties. The related mechanism was also discussed. Structures of two new azole-based hybrid iodoargentates (1 and 2) are reported. 1 is found to possess fluorescent photo(thermo)chromic properties. [Display omitted] •Azole molecules and their in-situ N-alkylation have employed in the construction of hybrid materials.•The photoluminescence behavior of two hybrids at different excitation wavelengths and low temperature was studied.•Iodoargentate possesses the fluorescent photo(thermo)chromic properties.
ArticleNumber 122748
Author Li, Chun-Hong
Yu, Jie-Hui
Xu, Ji-Qing
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Keywords Iodoargentate
Fluorescent photo(thermo)chromism
In situ N-alkylation
Photoluminescence
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Snippet In this article, two organic bases (dtb ​= ​1,4-di(1H-1,2,4-triazol-1-yl)benzene; mimb ​= ​1,2-bis((2-methyl-1H-imidazole-1-yl)methyl)benzen) were employed to...
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SubjectTerms Fluorescent photo(thermo)chromism
In situ N-alkylation
Iodoargentate
Photoluminescence
Title New iodoargentates with azole molecules: Syntheses, structural characterization and photoluminescence properties
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