Preparation and photoluminescence enhancement of Li＋ and Eu3＋ co-doped YPO4 hollow microspheres
Li＋ and Eu3＋ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene （PS） as template. Techniques of X-ray diffraction （XRD）, scanning electron microscopy （SEM）, as well as transmission electron microscopy （TEM） were employed to characterize...
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| Published in | Journal of rare earths Vol. 31; no. 5; pp. 449 - 455 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.05.2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60302-0 |
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| Abstract | Li＋ and Eu3＋ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene （PS） as template. Techniques of X-ray diffraction （XRD）, scanning electron microscopy （SEM）, as well as transmission electron microscopy （TEM） were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence （PL） characterization of the Li＋ and Eu3＋ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li＋ and Eu3＋ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li＋ ions into the YPOa：Eu3＋ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li＋ and 5%Eu3＋ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4：5%Eu3＋. |
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| AbstractList | Li+ and Eu3+ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene (PS) as template. Techniques of X-ray diffraction (XRD), scanning electron microscopy (SEM), as well as transmission electron microscopy (TEM) were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence (PL) characterization of the Li+ and Eu3+ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li+ and Eu3+ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li+ ions into the YPO4:Eu3+ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li+ and 5%Eu3+ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4:5%Eu3+.
PL intensity of the 5D0→7F1 and 5D0→7F2 transitions plotted as a function of Li+ concentration in the YPO4:5%Eu3+, x%Li+ hollow microsphere Li＋ and Eu3＋ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene （PS） as template. Techniques of X-ray diffraction （XRD）, scanning electron microscopy （SEM）, as well as transmission electron microscopy （TEM） were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence （PL） characterization of the Li＋ and Eu3＋ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li＋ and Eu3＋ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li＋ ions into the YPOa：Eu3＋ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li＋ and 5%Eu3＋ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4：5%Eu3＋. Li+ and Eu3+ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene (PS) as template. Techniques of X-ray diffraction (XRD), scanning electron microscopy (SEM), as well as transmission electron microscopy (TEM) were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence (PL) characterization of the Li+ and Eu3+ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li+ and Eu3+ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li+ ions into the YPO4:Eu3+ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li+ and 5%Eu3+ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4:5%Eu3+. |
| Author | 张立新 酒红芳 付跃华 孙益新 王瑗钟 |
| AuthorAffiliation | Chemical Engineering and Environment Institute, North University of China, Taiyuan 030051, China College of Science, North University of China, Taiyuan 030051, China |
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| Copyright | 2013 The Chinese Society of Rare Earths |
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| Keywords | lithium photoluminescence hollow microspheres sacrificial template europium yttrium orthophospha rare earths |
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| Notes | 11-2788/TF Li＋ and Eu3＋ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene （PS） as template. Techniques of X-ray diffraction （XRD）, scanning electron microscopy （SEM）, as well as transmission electron microscopy （TEM） were employed to characterize the as-synthesized sample. Furthermore, the photoluminescence （PL） characterization of the Li＋ and Eu3＋ co-doped YPO4 microsphere was carried out and the effects of the doping concentration of Li＋ and Eu3＋ active center concentration as well as calcination temperature on the PL properties were studied in detail. The results showed that the incorporation of Li＋ ions into the YPOa：Eu3＋ lattice could induce a remarkable improvement of the PL intensity. The highest emission intensity was observed with the compound of 5%Li＋ and 5%Eu3＋ co-doped YPO4, whose brightness was increased by a factor of more than 2.2 in comparison with that of the YPO4：5%Eu3＋. ZHANG Lixin , JIU Hongfang, FU Yuehua, SUN Yixin , WANG Yuanzhong（1. Chemical Engineering and Environment Institute, North University of China, Taiyuan 030051, China; 2. College of Science, North University of China, Taiyuan 030051, China） yttrium orthophospha; sacrificial template; europium; lithium; photoluminescence; hollow microspheres; rare earths ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| Snippet | Li＋ and Eu3＋ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene （PS） as template. Techniques of... Li+ and Eu3+ co-doped YPO4 hollow microspheres were successfully synthesized by a sacrificial template method using polystyrene (PS) as template. Techniques of... |
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| SubjectTerms | Diffraction europium hollow microspheres lithium photoluminescence rare earths sacrificial template X-射线衍射 YPO4 yttrium orthophospha 光致发光 共掺杂 制备 扫描电子显微镜 空心微球 透射电子显微镜 |
| Title | Preparation and photoluminescence enhancement of Li＋ and Eu3＋ co-doped YPO4 hollow microspheres |
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