THE HIGHLY UNSATURATED ALCOHOLS IN SPERM BLUBBER OIL

The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was separated and then debrominated to regenerate the highly unsaturated alcohols. These were converted into acetates, and the latter were fractionated. An...

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Published inBulletin of the Chemical Society of Japan Vol. 11; no. 1; pp. 29 - 34
Main Authors Toyama, Yoshiyuki, Akiyama, Goroku
Format Journal Article
LanguageEnglish
Published Tokyo The Chemical Society of Japan 01.01.1936
Chemical Society of Japan
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Abstract The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was separated and then debrominated to regenerate the highly unsaturated alcohols. These were converted into acetates, and the latter were fractionated. An examination of the resulting fractions showed that the highly unsaturated alcohols of sperm blubber oil contained two individual alcohols C20H34O and C22H36O as chief components.
AbstractList Abstract The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was separated and then debrominated to regenerate the highly unsaturated alcohols. These were converted into acetates, and the latter were fractionated. An examination of the resulting fractions showed that the highly unsaturated alcohols of sperm blubber oil contained two individual alcohols C20H34O and C22H36O as chief components.
The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was separated and then debrominated to regenerate the highly unsaturated alcohols. These were converted into acetates, and the latter were fractionated. An examination of the resulting fractions showed that the highly unsaturated alcohols of sperm blubber oil contained two individual alcohols C20H34O and C22H36O as chief components.
Author Toyama, Yoshiyuki
Akiyama, Goroku
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10.1246/bcsj.10.296
10.1246/bcsj.10.441
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References 12) Adam and Dyer, J. Chem. Soc., 127 (1925), 70.
9) J. Soc. Chem. Ind., Japan, 28 (1925), 390.
3) J. Soc. Chem. Ind., 48 (1929), 365 T.
7) Toyama and Tsuchiya, Bull. Chem. Soc. Jpn., 10 (1935), 441.
8) Derived from Catadontidae.
10) This value is thought to be a little too high.
5) Toyama and Tsuchiya, Bull. Chem. Soc. Jpn., 10 (193, 573
4) Compt. rend., 185 (1927), 279.
11) For the elementary analyses we are indebted to Mr. Tsuchiya.
6) Toyama and Tsuchiya, Bull. Chem. Soc. Jpn., 10 (1935), 296.
13) Bleyberg and Ulrich, Ber., 64 (1931), 2504.
2) Bull. Chem. Soc. Jpn., 10 (1935), 579.
1) Toyama, J. Soc. Chem. Ind., Japan, 30 (1927), 527.
Toyama and Akiyama, Bull. Chem. Soc. Jpn., 10 (1935), 579.
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Snippet The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was separated...
Abstract The high boiling fraction of the unsaponifiable matter of sperm blubber oil was brominated in ethereal solution, and the ether insoluble bromide was...
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Title THE HIGHLY UNSATURATED ALCOHOLS IN SPERM BLUBBER OIL
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