Eco-friendly synthesis of porous and charged polyethersulfone membrane for improved protein separation efficiency

•A new sustainable honeycomb-structured PES-PVA porous membrane was synthesized.•Increased surface charge and hydrophilicity were responsible for improving protein separation.•BSA formed an electrostatic bond with PES/PVA, leading to a synergistic effect in fouling.•The water flux and protein reject...

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Published inResults in engineering Vol. 25; p. 104422
Main Authors Talukder, Md Eman, Pervez, Md. Nahid, Song, Hongchen, Buonerba, Antonio, Stylios, George K., Naddeo, Vincenzo, Kujawski, Wojciech, Figoli, Alberto
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.03.2025
Elsevier
Subjects
Antifouling properties
Green solvent
PES
Porous membrane
Protein separation
Protein separation
Antifouling properties
Green solvent
Porous membrane
PES
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Abstract •A new sustainable honeycomb-structured PES-PVA porous membrane was synthesized.•Increased surface charge and hydrophilicity were responsible for improving protein separation.•BSA formed an electrostatic bond with PES/PVA, leading to a synergistic effect in fouling.•The water flux and protein rejection rates (99%) were higher for the PES-PVA membrane.•Polarclean® was used as a solvent for fabricating PES/PVA membranes. This research article aims to develop a novel, sustainable, porous charged membrane with excellent antifouling performance. It focuses on creating a porous polyethersulfone/ polyvinyl alcohol (PES-PVA) negative charged membrane with a porous surface structure, employing polyvinylpyrrolidone (PVP) and a green solvent (PolarClean) to improve the wettability of the membrane. The characteristics of the composite membranes, such as morphology, mechanical properties, porosity, pore size, and water permeability, were scrutinized. The PES-PVP blended membrane exhibited a significantly higher water flux of 542.2 ± 5.4 L m−2 h−1 bar−1 relative to the pure PES membrane, which had a flux of 289.4 ± 3.4 L m−2 h−1 bar−1. PEG molecular weight cut-offs (MWCOs) and rejection rates were 50 - 500 kDa and 89 - 99 %, respectively. BSA is repulsed to the PES/PVA membrane surface, which highly rejects proteins. Additionally, using lower molecular weight and PVA concentration could yield membranes with increased protein flux and enhanced protein rejection (99 %) along with strong fouling resistance (99.9 %), surpassing the performance of blended PES membranes and other commercial membranes (CMs).
AbstractList •A new sustainable honeycomb-structured PES-PVA porous membrane was synthesized.•Increased surface charge and hydrophilicity were responsible for improving protein separation.•BSA formed an electrostatic bond with PES/PVA, leading to a synergistic effect in fouling.•The water flux and protein rejection rates (99%) were higher for the PES-PVA membrane.•Polarclean® was used as a solvent for fabricating PES/PVA membranes. This research article aims to develop a novel, sustainable, porous charged membrane with excellent antifouling performance. It focuses on creating a porous polyethersulfone/ polyvinyl alcohol (PES-PVA) negative charged membrane with a porous surface structure, employing polyvinylpyrrolidone (PVP) and a green solvent (PolarClean) to improve the wettability of the membrane. The characteristics of the composite membranes, such as morphology, mechanical properties, porosity, pore size, and water permeability, were scrutinized. The PES-PVP blended membrane exhibited a significantly higher water flux of 542.2 ± 5.4 L m−2 h−1 bar−1 relative to the pure PES membrane, which had a flux of 289.4 ± 3.4 L m−2 h−1 bar−1. PEG molecular weight cut-offs (MWCOs) and rejection rates were 50 - 500 kDa and 89 - 99 %, respectively. BSA is repulsed to the PES/PVA membrane surface, which highly rejects proteins. Additionally, using lower molecular weight and PVA concentration could yield membranes with increased protein flux and enhanced protein rejection (99 %) along with strong fouling resistance (99.9 %), surpassing the performance of blended PES membranes and other commercial membranes (CMs).
This research article aims to develop a novel, sustainable, porous charged membrane with excellent antifouling performance. It focuses on creating a porous polyethersulfone/ polyvinyl alcohol (PES-PVA) negative charged membrane with a porous surface structure, employing polyvinylpyrrolidone (PVP) and a green solvent (PolarClean) to improve the wettability of the membrane. The characteristics of the composite membranes, such as morphology, mechanical properties, porosity, pore size, and water permeability, were scrutinized. The PES-PVP blended membrane exhibited a significantly higher water flux of 542.2 ± 5.4 L m−2 h−1 bar−1 relative to the pure PES membrane, which had a flux of 289.4 ± 3.4 L m−2 h−1 bar−1. PEG molecular weight cut-offs (MWCOs) and rejection rates were 50 - 500 kDa and 89 - 99 %, respectively. BSA is repulsed to the PES/PVA membrane surface, which highly rejects proteins. Additionally, using lower molecular weight and PVA concentration could yield membranes with increased protein flux and enhanced protein rejection (99 %) along with strong fouling resistance (99.9 %), surpassing the performance of blended PES membranes and other commercial membranes (CMs).
ArticleNumber 104422
Author Song, Hongchen
Pervez, Md. Nahid
Talukder, Md Eman
Buonerba, Antonio
Stylios, George K.
Naddeo, Vincenzo
Kujawski, Wojciech
Figoli, Alberto
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Antifouling properties
Green solvent
Porous membrane
PES
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SSID ssj0002810137
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Snippet •A new sustainable honeycomb-structured PES-PVA porous membrane was synthesized.•Increased surface charge and hydrophilicity were responsible for improving...
This research article aims to develop a novel, sustainable, porous charged membrane with excellent antifouling performance. It focuses on creating a porous...
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elsevier
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StartPage 104422
SubjectTerms Antifouling properties
Green solvent
PES
Porous membrane
Protein separation
Title Eco-friendly synthesis of porous and charged polyethersulfone membrane for improved protein separation efficiency
URI https://dx.doi.org/10.1016/j.rineng.2025.104422
https://doaj.org/article/52eaca090a7d452d9b230b4d219a4068
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