Visible-light-driven activation of peroxymonosulfate for accelerating ciprofloxacin degradation using CeO2/Co3O4 p-n heterojunction photocatalysts
[Display omitted] •Novel highly efficient visible-light-driven photocatalytic system Co3O4/CeO2/PMS is prepared.•87.8% of CIP could be removed within 50 min visible illumination.•The addition of PMS produced the synergetic effect in Co3O4/CeO2 photocatalytic system.•A plausible degradation pathway f...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 391; p. 123612 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.07.2020
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Novel highly efficient visible-light-driven photocatalytic system Co3O4/CeO2/PMS is prepared.•87.8% of CIP could be removed within 50 min visible illumination.•The addition of PMS produced the synergetic effect in Co3O4/CeO2 photocatalytic system.•A plausible degradation pathway for CIP was proposed.•The in-depth mechanisms insight of charge separation.
The development of simple and effective approaches for the synthesis of bimetallic oxide heterojunction photocatalyst which are used to activate peroxymonosulfate (PMS) under visible-light-driven is highly feasible but remains a great challenge. In this work, the Co3O4/CeO2 composite was prepared by a facile chemical reaction, followed by annealing in a muffle furnace and then applied to activate PMS for ciprofloxacin (CIP) degradation. Various characterizations confirmed the formation of p-n heterojunction between Co3O4 and CeO2. Meanwhile, the 5 wt% Co3O4/CeO2/PMS composite showed highest degradation rate of CIP (87.8%) under visible light irradiation. The obtained Co3O4/CeO2/PMS system still exhibited a good catalytic performance in presence of different anion. Besides, the active radical h+, OH, O2−, and SO4− are involved in CIP degradation. The excellent degradation performance can be interpreted as the synergistic effect between Co3O4/CeO2 heterojunction photocatalyst and PMS activation. Moreover, the energy band structure and valence band deviation of Co3O4/CeO2 p-n heterogeneous junction were confirmed. This work would give a reference for combining the photocatalyst and activation of PMS under visible light for further removal of pollutants. |
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| AbstractList | [Display omitted]
•Novel highly efficient visible-light-driven photocatalytic system Co3O4/CeO2/PMS is prepared.•87.8% of CIP could be removed within 50 min visible illumination.•The addition of PMS produced the synergetic effect in Co3O4/CeO2 photocatalytic system.•A plausible degradation pathway for CIP was proposed.•The in-depth mechanisms insight of charge separation.
The development of simple and effective approaches for the synthesis of bimetallic oxide heterojunction photocatalyst which are used to activate peroxymonosulfate (PMS) under visible-light-driven is highly feasible but remains a great challenge. In this work, the Co3O4/CeO2 composite was prepared by a facile chemical reaction, followed by annealing in a muffle furnace and then applied to activate PMS for ciprofloxacin (CIP) degradation. Various characterizations confirmed the formation of p-n heterojunction between Co3O4 and CeO2. Meanwhile, the 5 wt% Co3O4/CeO2/PMS composite showed highest degradation rate of CIP (87.8%) under visible light irradiation. The obtained Co3O4/CeO2/PMS system still exhibited a good catalytic performance in presence of different anion. Besides, the active radical h+, OH, O2−, and SO4− are involved in CIP degradation. The excellent degradation performance can be interpreted as the synergistic effect between Co3O4/CeO2 heterojunction photocatalyst and PMS activation. Moreover, the energy band structure and valence band deviation of Co3O4/CeO2 p-n heterogeneous junction were confirmed. This work would give a reference for combining the photocatalyst and activation of PMS under visible light for further removal of pollutants. |
| ArticleNumber | 123612 |
| Author | Wen, Xiao-Ju Mu, Qi-Ming Shen, Chun-Hui Fei, Zheng-Hao Liu, Zong-Tang |
| Author_xml | – sequence: 1 givenname: Chun-Hui surname: Shen fullname: Shen, Chun-Hui organization: School of Chemistry and Environmental Engineering, Yancheng Teachers University, Yancheng, Jiangsu Province 224051, China – sequence: 2 givenname: Xiao-Ju orcidid: 0000-0002-6450-7244 surname: Wen fullname: Wen, Xiao-Ju email: wenxiaoju1990@126.com organization: School of Chemistry and Environmental Engineering, Yancheng Teachers University, Yancheng, Jiangsu Province 224051, China – sequence: 3 givenname: Zheng-Hao surname: Fei fullname: Fei, Zheng-Hao email: feizhenghao@163.com organization: School of Chemistry and Environmental Engineering, Yancheng Teachers University, Yancheng, Jiangsu Province 224051, China – sequence: 4 givenname: Zong-Tang surname: Liu fullname: Liu, Zong-Tang organization: School of Chemistry and Environmental Engineering, Yancheng Teachers University, Yancheng, Jiangsu Province 224051, China – sequence: 5 givenname: Qi-Ming surname: Mu fullname: Mu, Qi-Ming organization: School of Chemistry and Environmental Engineering, Yancheng Teachers University, Yancheng, Jiangsu Province 224051, China |
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•Novel highly efficient visible-light-driven photocatalytic system Co3O4/CeO2/PMS is prepared.•87.8% of CIP could be removed within 50 min... |
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| Title | Visible-light-driven activation of peroxymonosulfate for accelerating ciprofloxacin degradation using CeO2/Co3O4 p-n heterojunction photocatalysts |
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