Crystallinity and rheology of HDPE/PA12 blends compatibilized with HDPE‐alt‐MAH
This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and injected into a mold with 75/25, 50/50, and 25/75 HDPE/PA ratios. The Fourier‐transform infrared spectroscopy (FTIR) analysis showed that no...
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| Published in | Polymers for advanced technologies Vol. 34; no. 1; pp. 145 - 154 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Chichester, UK
John Wiley & Sons, Ltd
01.01.2023
Wiley Subscription Services, Inc |
| Subjects | |
| Online Access | Get full text |
| ISSN | 1042-7147 1099-1581 |
| DOI | 10.1002/pat.5873 |
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| Abstract | This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and injected into a mold with 75/25, 50/50, and 25/75 HDPE/PA ratios. The Fourier‐transform infrared spectroscopy (FTIR) analysis showed that no oxidation reaction occurred in the high‐temperature processing and that stronger interactions between the components of the blends occurred in the polyamide's functional groups. The x‐ray diffraction (XRD) analysis showed that the crystallinity degree of the blends and the mean crystallite sizes decreased with the addition of PA12 for both blends. The HDPE's lattice parameters were consistent with the values in the literature, whereas for the PA12, it was not possible to fit its lattice parameters. The rheology analysis evaluated the relationship between the shear stress and viscosity and found that the HDPE/PA 75/25 blend was the most pseudoplastic, presenting the best processability under high shear rates. |
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| AbstractList | This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and injected into a mold with 75/25, 50/50, and 25/75 HDPE/PA ratios. The Fourier‐transform infrared spectroscopy (FTIR) analysis showed that no oxidation reaction occurred in the high‐temperature processing and that stronger interactions between the components of the blends occurred in the polyamide's functional groups. The x‐ray diffraction (XRD) analysis showed that the crystallinity degree of the blends and the mean crystallite sizes decreased with the addition of PA12 for both blends. The HDPE's lattice parameters were consistent with the values in the literature, whereas for the PA12, it was not possible to fit its lattice parameters. The rheology analysis evaluated the relationship between the shear stress and viscosity and found that the HDPE/PA 75/25 blend was the most pseudoplastic, presenting the best processability under high shear rates. This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and injected into a mold with 75/25, 50/50, and 25/75 HDPE/PA ratios. The Fourier‐transform infrared spectroscopy (FTIR) analysis showed that no oxidation reaction occurred in the high‐temperature processing and that stronger interactions between the components of the blends occurred in the polyamide's functional groups. The x‐ray diffraction (XRD) analysis showed that the crystallinity degree of the blends and the mean crystallite sizes decreased with the addition of PA12 for both blends. The HDPE's lattice parameters were consistent with the values in the literature, whereas for the PA12, it was not possible to fit its lattice parameters. The rheology analysis evaluated the relationship between the shear stress and viscosity and found that the HDPE/PA 75/25 blend was the most pseudoplastic, presenting the best processability under high shear rates. |
| Author | Almeida Santos da Silva, Geovane Avillez, Roberto Ribeiro Letichevsky, Sonia d'Almeida, José Roberto Moraes |
| Author_xml | – sequence: 1 givenname: Geovane orcidid: 0000-0002-3365-9640 surname: Almeida Santos da Silva fullname: Almeida Santos da Silva, Geovane email: almeida_geovane@hotmail.com organization: Pontifícia Universidade Católica do Rio de Janeiro – sequence: 2 givenname: José Roberto Moraes orcidid: 0000-0002-0026-1863 surname: d'Almeida fullname: d'Almeida, José Roberto Moraes organization: Pontifícia Universidade Católica do Rio de Janeiro – sequence: 3 givenname: Sonia orcidid: 0000-0003-1419-7935 surname: Letichevsky fullname: Letichevsky, Sonia organization: Pontifícia Universidade Católica do Rio de Janeiro – sequence: 4 givenname: Roberto Ribeiro surname: Avillez fullname: Avillez, Roberto Ribeiro organization: Pontifícia Universidade Católica do Rio de Janeiro |
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| Snippet | This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and... This work studies the crystallinity and rheology of HDPE/PA12 blends compatibilized with 2 wt% of HDPE‐alt‐MAH. Specimens of HDPE/PA12 blends were extruded and... |
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| SubjectTerms | blends Crystallinity Crystallites Extrusion molding Functional groups Infrared analysis Lattice parameters Oxidation Polyamide resins polyamides Polymer blends Pseudoplasticity Rheological properties Rheology Shear stress spectroscopy |
| Title | Crystallinity and rheology of HDPE/PA12 blends compatibilized with HDPE‐alt‐MAH |
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