3D surface characterization of polymer-oxide nanocomposite coating using nanoscale stereometric approach for enhanced functionality
This study investigates the influence of varying nanorods (NR) filler concentrations (0, 5, 10, 20, and 30 wt%) on the surface morphology of nanocomposite coating composed of a poly(methyl methacrylate) matrix containing elongated titania nanorods, applied via spin-coating. Detailed analyses of 3-D...
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| Published in | Colloids and surfaces. A, Physicochemical and engineering aspects Vol. 711; p. 136360 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
20.04.2025
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| Abstract | This study investigates the influence of varying nanorods (NR) filler concentrations (0, 5, 10, 20, and 30 wt%) on the surface morphology of nanocomposite coating composed of a poly(methyl methacrylate) matrix containing elongated titania nanorods, applied via spin-coating. Detailed analyses of 3-D topographic AFM images, contour line plots, Abbott-Firestone curves, furrow depth, texture direction, power spectral density (PSD), and ISO 25178–2:2012 statistical surface parameters were conducted. Results revealed a significant increase in surface roughness and complexity with increasing NR content, peaking at 20 wt% (P20). P20 demonstrated the highest roughness, optimal texture alignment, and functional properties, while further increases in NR content (P30) led to surface smoothing due to filler agglomeration. These findings highlight the critical role of NR concentration in tailoring the surface properties of nanocomposite films for enhanced performance.
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•Optimized 20 wt% nanorods yield peak surface roughness and functionality.•High nanorod concentrations smooth surfaces and reduce coating performance•AFM and stereometric analysis reveals nanoscale surface evolution with nanorod content.•Enhanced roughness improves adhesion and functional surface properties.•Fractal analysis highlights surface complexity with varying nanorod concentrations. |
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| AbstractList | This study investigates the influence of varying nanorods (NR) filler concentrations (0, 5, 10, 20, and 30 wt%) on the surface morphology of nanocomposite coating composed of a poly(methyl methacrylate) matrix containing elongated titania nanorods, applied via spin-coating. Detailed analyses of 3-D topographic AFM images, contour line plots, Abbott-Firestone curves, furrow depth, texture direction, power spectral density (PSD), and ISO 25178–2:2012 statistical surface parameters were conducted. Results revealed a significant increase in surface roughness and complexity with increasing NR content, peaking at 20 wt% (P20). P20 demonstrated the highest roughness, optimal texture alignment, and functional properties, while further increases in NR content (P30) led to surface smoothing due to filler agglomeration. These findings highlight the critical role of NR concentration in tailoring the surface properties of nanocomposite films for enhanced performance. This study investigates the influence of varying nanorods (NR) filler concentrations (0, 5, 10, 20, and 30 wt%) on the surface morphology of nanocomposite coating composed of a poly(methyl methacrylate) matrix containing elongated titania nanorods, applied via spin-coating. Detailed analyses of 3-D topographic AFM images, contour line plots, Abbott-Firestone curves, furrow depth, texture direction, power spectral density (PSD), and ISO 25178–2:2012 statistical surface parameters were conducted. Results revealed a significant increase in surface roughness and complexity with increasing NR content, peaking at 20 wt% (P20). P20 demonstrated the highest roughness, optimal texture alignment, and functional properties, while further increases in NR content (P30) led to surface smoothing due to filler agglomeration. These findings highlight the critical role of NR concentration in tailoring the surface properties of nanocomposite films for enhanced performance. [Display omitted] •Optimized 20 wt% nanorods yield peak surface roughness and functionality.•High nanorod concentrations smooth surfaces and reduce coating performance•AFM and stereometric analysis reveals nanoscale surface evolution with nanorod content.•Enhanced roughness improves adhesion and functional surface properties.•Fractal analysis highlights surface complexity with varying nanorod concentrations. |
| ArticleNumber | 136360 |
| Author | Ţălu, Ştefan Patra, Niranjan |
| Author_xml | – sequence: 1 givenname: Ştefan surname: Ţălu fullname: Ţălu, Ştefan email: stefan.talu@auto.utcluj.ro organization: The Technical University of Cluj-Napoca, The Directorate of Research, Development and Innovation Management (DMCDI), Constantin Daicoviciu Street, no. 15, Cluj-Napoca, Cluj County 400020, Romania – sequence: 2 givenname: Niranjan orcidid: 0000-0003-3941-5345 surname: Patra fullname: Patra, Niranjan email: patraji@gmail.com, drpatra.niranjan@gmail.com organization: Department of Chemistry, Koneru Lakshmaiah Education Foundation, Greenfield, Vaddeswaram, Andhra Pradesh 522502, India |
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| Cites_doi | 10.1080/02670844.2019.1710937 10.1016/j.jiec.2016.08.003 10.1016/j.jallcom.2018.06.213 10.1007/s11082-017-1079-3 10.1007/s10854-017-7422-4 10.1016/j.cplett.2019.01.042 10.1016/j.rinp.2023.106209 10.1007/s13391-015-4280-1 10.1016/j.jelechem.2018.10.037 10.1080/1023666X.2014.955400 10.1016/j.porgcoat.2015.07.024 |
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| Keywords | Atomic force microscopy Titania nanorods Polymer-oxide nanocomposites Spin-coated coating Surface micromorphology |
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| SubjectTerms | Atomic force microscopy furrows nanocomposites nanorods Polymer-oxide nanocomposites roughness Spin-coated coating Surface micromorphology surface roughness texture Titania nanorods titanium dioxide |
| Title | 3D surface characterization of polymer-oxide nanocomposite coating using nanoscale stereometric approach for enhanced functionality |
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