Facile and scalable preparation of 2D-MoS2/graphene oxide composite for supercapacitor
Due to both hydrophilic oxygen–containing groups and hydrophobic unoxidized aromatic rings, graphene oxide (GO) exhibits amphiphilic properties, similar to common surfactants. Here, hydrophobic bulk molybdenum disulfide (MoS 2 ) was successfully exfoliated in GO aqueous dispersion under the conditio...
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| Published in | Ionics Vol. 28; no. 11; pp. 5223 - 5232 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Berlin/Heidelberg
Springer Berlin Heidelberg
01.11.2022
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0947-7047 1862-0760 |
| DOI | 10.1007/s11581-022-04719-9 |
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| Abstract | Due to both hydrophilic oxygen–containing groups and hydrophobic unoxidized aromatic rings, graphene oxide (GO) exhibits amphiphilic properties, similar to common surfactants. Here, hydrophobic bulk molybdenum disulfide (MoS
2
) was successfully exfoliated in GO aqueous dispersion under the condition of high shear force. The amphiphilic GO nanosheets play an importance role in exfoliation of bulk MoS
2
and inhibiting agglomeration of two-dimensional (2D) MoS
2
. The stacking supramolecular interaction and hydrophobic force enable rapid formation of 2D-MoS
2
/GO composite. Meanwhile, the strong electrostatic repulsion make composite uniformly dispersed in water. The exfoliation conditions were optimum that include pH value, exfoliation time, GO concentration, oxidation level of GO, and size of bulk MoS
2
. The average length and thickness of optimum 2D-MoS
2
nanosheets are 161.3 nm and below 10 nm, respectively. The contents of 2D-MoS
2
in composites are up to 4.87%. The structure characterization and quenched fluorescence also demonstrated that 2D-MoS
2
is adhered to the surface of GO and dispersing in water. The 2D-MoS
2
/rGO film prepared from prepared dispersion shows an outstanding volume specific capacitance and cycle stability in supercapacitor. Overall, this work provides a facile and scalable technology for preparing 2D-MoS
2
/GO composite without any additives, which can be used for supercapacitor electrode. |
|---|---|
| AbstractList | Due to both hydrophilic oxygen–containing groups and hydrophobic unoxidized aromatic rings, graphene oxide (GO) exhibits amphiphilic properties, similar to common surfactants. Here, hydrophobic bulk molybdenum disulfide (MoS
2
) was successfully exfoliated in GO aqueous dispersion under the condition of high shear force. The amphiphilic GO nanosheets play an importance role in exfoliation of bulk MoS
2
and inhibiting agglomeration of two-dimensional (2D) MoS
2
. The stacking supramolecular interaction and hydrophobic force enable rapid formation of 2D-MoS
2
/GO composite. Meanwhile, the strong electrostatic repulsion make composite uniformly dispersed in water. The exfoliation conditions were optimum that include pH value, exfoliation time, GO concentration, oxidation level of GO, and size of bulk MoS
2
. The average length and thickness of optimum 2D-MoS
2
nanosheets are 161.3 nm and below 10 nm, respectively. The contents of 2D-MoS
2
in composites are up to 4.87%. The structure characterization and quenched fluorescence also demonstrated that 2D-MoS
2
is adhered to the surface of GO and dispersing in water. The 2D-MoS
2
/rGO film prepared from prepared dispersion shows an outstanding volume specific capacitance and cycle stability in supercapacitor. Overall, this work provides a facile and scalable technology for preparing 2D-MoS
2
/GO composite without any additives, which can be used for supercapacitor electrode. |
| Author | Wu, Wei Meng, Hong Yin, Xianglu Teng, Aijun Zeng, Zehua |
| Author_xml | – sequence: 1 givenname: Xianglu surname: Yin fullname: Yin, Xianglu organization: Ansteel Beijing Research Institute Co., LTD, College of Chemical Engineering, Beijing University of Chemical Technology – sequence: 2 givenname: Aijun surname: Teng fullname: Teng, Aijun organization: Ansteel Beijing Research Institute Co., LTD – sequence: 3 givenname: Zehua surname: Zeng fullname: Zeng, Zehua organization: Ansteel Beijing Research Institute Co., LTD – sequence: 4 givenname: Hong surname: Meng fullname: Meng, Hong organization: College of Chemical Engineering, Beijing University of Chemical Technology – sequence: 5 givenname: Wei surname: Wu fullname: Wu, Wei email: wuwei@mail.buct.edu.cn organization: College of Chemical Engineering, Beijing University of Chemical Technology |
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| Cites_doi | 10.1002/anie.201105364 10.1021/nn405938z 10.1016/j.apsusc.2017.06.303 10.1021/ja404523s 10.1021/nl403036h 10.1002/adma.201000732 10.1021/nl201874w 10.1039/C4CE00200H 10.1016/j.ensm.2018.05.013 10.3389/fmats.2020.580424 10.1038/nmat3439 10.1021/nl301335q 10.1016/j.electacta.2013.07.094 10.1021/acs.nanolett.7b03968 10.1002/adma.201205157 10.1021/nl404396p 10.1021/ar4002312 10.1016/j.colsurfa.2017.07.074 10.1016/j.carbon.2011.09.008 10.1021/acsami.9b00192 10.1021/cm5044864 10.1103/PhysRevB.82.125403 10.1126/science.1200770 10.1038/nmat3944 10.1021/jp103745g 10.1039/C7NR01501A 10.1039/c2jm30587a 10.1021/jacs.6b08096 10.1002/chem.201001771 10.1021/nn203715c 10.1016/j.ijhydene.2013.08.112 10.1002/smll.201102654 10.1021/acsami.7b10967 10.1016/j.jcis.2015.01.058 10.1039/C5CC02066B 10.1002/adma.201501888 10.1126/science.1194975 10.1126/science.1102896 |
| ContentType | Journal Article |
| Copyright | The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
| Copyright_xml | – notice: The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2022. Springer Nature or its licensor holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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| Keywords | Supercapacitor Graphene oxide Molybdenum disulfide Exfoliation |
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| Title | Facile and scalable preparation of 2D-MoS2/graphene oxide composite for supercapacitor |
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