Effect of Thermal Treatment on the Photocatalytic Activity in Visible Light of TiO2-W Flame Spray Synthesised Nanopowders

Effect of W doping as well as a thermal treatment on the structural and photocatalytic properties of TiO 2 produced by flame spray synthesis (FSS) were the subject of investigation. Structural properties were studied by means of X-ray diffraction (XRD), BET adsorption isotherm and transmission elect...

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Published inTopics in catalysis Vol. 52; no. 8; pp. 1051 - 1059
Main Authors Michalow, Katarzyna A., Heel, Andre, Vital, Andri, Amberg, Martin, Fortunato, Giuseppino, Kowalski, Kazimierz, Graule, Thomas J., Rekas, Mieczyslaw
Format Journal Article
LanguageEnglish
Published Boston Springer US 01.07.2009
Subjects
Catalysis
Characterization and Evaluation of Materials
Chemistry
Chemistry and Materials Science
Industrial Chemistry/Chemical Engineering
Original Paper
Pharmacy
Physical Chemistry
Nanoparticles
TiO
Visible light absorption
Flame spray synthesis (FSS)
Photocatalysis
Doping
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Abstract Effect of W doping as well as a thermal treatment on the structural and photocatalytic properties of TiO 2 produced by flame spray synthesis (FSS) were the subject of investigation. Structural properties were studied by means of X-ray diffraction (XRD), BET adsorption isotherm and transmission electron microscopy (TEM). The surface condition was investigated by X-ray photoelectron spectroscopy (XPS) and differential scanning calorimetry (DSC) and differential thermal and thermogravimetric analysis (DTA-TGA). The photocatalytic properties were studied by optical measurements and photodecomposition of methylene blue under visible irradiation. It was found that the photoactivity in the visible region was enhanced significantly by the W-doping as well as by additional thermal treatment of those nanopowders. The obtained TiO 2 -W nanopowders exhibited higher performance under visible light than P25.
AbstractList Effect of W doping as well as a thermal treatment on the structural and photocatalytic properties of TiO 2 produced by flame spray synthesis (FSS) were the subject of investigation. Structural properties were studied by means of X-ray diffraction (XRD), BET adsorption isotherm and transmission electron microscopy (TEM). The surface condition was investigated by X-ray photoelectron spectroscopy (XPS) and differential scanning calorimetry (DSC) and differential thermal and thermogravimetric analysis (DTA-TGA). The photocatalytic properties were studied by optical measurements and photodecomposition of methylene blue under visible irradiation. It was found that the photoactivity in the visible region was enhanced significantly by the W-doping as well as by additional thermal treatment of those nanopowders. The obtained TiO 2 -W nanopowders exhibited higher performance under visible light than P25.
Author Rekas, Mieczyslaw
Michalow, Katarzyna A.
Fortunato, Giuseppino
Amberg, Martin
Heel, Andre
Vital, Andri
Graule, Thomas J.
Kowalski, Kazimierz
Author_xml – sequence: 1
  givenname: Katarzyna A.
  surname: Michalow
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  givenname: Andre
  surname: Heel
  fullname: Heel, Andre
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  surname: Vital
  fullname: Vital, Andri
  organization: High Performance Ceramics, Empa, Swiss Federal Laboratories for Materials Testing and Research
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  surname: Amberg
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  organization: Laboratory for Advanced Fibers, Empa, Swiss Federal Laboratories for Materials Testing and Research
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  givenname: Giuseppino
  surname: Fortunato
  fullname: Fortunato, Giuseppino
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  givenname: Kazimierz
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  fullname: Kowalski, Kazimierz
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  givenname: Thomas J.
  surname: Graule
  fullname: Graule, Thomas J.
  organization: High Performance Ceramics, Empa, Swiss Federal Laboratories for Materials Testing and Research
– sequence: 8
  givenname: Mieczyslaw
  surname: Rekas
  fullname: Rekas, Mieczyslaw
  email: rekas@agh.edu.pl
  organization: Faculty of Material Science and Ceramic, AGH University of Science and Technology
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Keywords Nanoparticles
TiO
Visible light absorption
Flame spray synthesis (FSS)
Photocatalysis
Doping
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Snippet Effect of W doping as well as a thermal treatment on the structural and photocatalytic properties of TiO 2 produced by flame spray synthesis (FSS) were the...
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SubjectTerms Catalysis
Characterization and Evaluation of Materials
Chemistry
Chemistry and Materials Science
Industrial Chemistry/Chemical Engineering
Original Paper
Pharmacy
Physical Chemistry
Title Effect of Thermal Treatment on the Photocatalytic Activity in Visible Light of TiO2-W Flame Spray Synthesised Nanopowders
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