Fabrication of a super-hydrophobic and high-roughness terrace-effect membrane for enhanced flux and fouling resistance
The current study reported a novel terrace effect on the membrane surface, which is a straightforward and practical approach to enhancing membrane performance characterized by high roughness, thermal stability, and extended durability. We prepared pure PVDF and terraced PVDF membrane using several m...
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| Published in | Desalination and water treatment Vol. 322; p. 101153 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Inc
01.04.2025
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The current study reported a novel terrace effect on the membrane surface, which is a straightforward and practical approach to enhancing membrane performance characterized by high roughness, thermal stability, and extended durability. We prepared pure PVDF and terraced PVDF membrane using several membrane fabrication methods, Delayed non-solvent Induced Phase Separation (D-NIPS) and Thermally Induced Phase Separation (TIPS), along with Vapor-Induced Phase Separation (VIPS) processes with solvent/water mix vapor flow. These methods were complemented by adjusting the coagulation bath composition and temperature, followed by surface fluorination and surfactant sodium dodecyl sulfate (SDS) to reduce the membrane's surface energy and the surface tension of the feed saltwater. The resulting super-hydrophobic pure PVDF, terraced effect porous PVDF membranes, terraced effect PVDF-FS membranes with high roughness 72 ± 4.3 nm, 360 ± 20 nm, 401 ± 24 nm, and a water contact angle (WCA) of 109 ± 1.1°, 138 ± 1.5°, 147 ± 2.9°. Our results demonstrated that membranes with terrace effect super-hydrophobic surfaces achieved a high flux of 9.6 Lm−2h−1 for pure PVDF, and 25.2 Lm−2h−1 for terrace effect porous PVDF, offering a significant advantage for MD treatment.
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•Designed a new surface structure on the membrane surface.•Terrace-effect porous membrane with high roughness and superhydrophobicity properties.•New structure improved the flux and fouling resistance of membrane.•Terrace-effect MD membrane retard membrane scaling. |
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| AbstractList | The current study reported a novel terrace effect on the membrane surface, which is a straightforward and practical approach to enhancing membrane performance characterized by high roughness, thermal stability, and extended durability. We prepared pure PVDF and terraced PVDF membrane using several membrane fabrication methods, Delayed non-solvent Induced Phase Separation (D-NIPS) and Thermally Induced Phase Separation (TIPS), along with Vapor-Induced Phase Separation (VIPS) processes with solvent/water mix vapor flow. These methods were complemented by adjusting the coagulation bath composition and temperature, followed by surface fluorination and surfactant sodium dodecyl sulfate (SDS) to reduce the membrane's surface energy and the surface tension of the feed saltwater. The resulting super-hydrophobic pure PVDF, terraced effect porous PVDF membranes, terraced effect PVDF-FS membranes with high roughness 72 ± 4.3 nm, 360 ± 20 nm, 401 ± 24 nm, and a water contact angle (WCA) of 109 ± 1.1°, 138 ± 1.5°, 147 ± 2.9°. Our results demonstrated that membranes with terrace effect super-hydrophobic surfaces achieved a high flux of 9.6 Lm−2h−1 for pure PVDF, and 25.2 Lm−2h−1 for terrace effect porous PVDF, offering a significant advantage for MD treatment. The current study reported a novel terrace effect on the membrane surface, which is a straightforward and practical approach to enhancing membrane performance characterized by high roughness, thermal stability, and extended durability. We prepared pure PVDF and terraced PVDF membrane using several membrane fabrication methods, Delayed non-solvent Induced Phase Separation (D-NIPS) and Thermally Induced Phase Separation (TIPS), along with Vapor-Induced Phase Separation (VIPS) processes with solvent/water mix vapor flow. These methods were complemented by adjusting the coagulation bath composition and temperature, followed by surface fluorination and surfactant sodium dodecyl sulfate (SDS) to reduce the membrane's surface energy and the surface tension of the feed saltwater. The resulting super-hydrophobic pure PVDF, terraced effect porous PVDF membranes, terraced effect PVDF-FS membranes with high roughness 72 ± 4.3 nm, 360 ± 20 nm, 401 ± 24 nm, and a water contact angle (WCA) of 109 ± 1.1°, 138 ± 1.5°, 147 ± 2.9°. Our results demonstrated that membranes with terrace effect super-hydrophobic surfaces achieved a high flux of 9.6 Lm−2h−1 for pure PVDF, and 25.2 Lm−2h−1 for terrace effect porous PVDF, offering a significant advantage for MD treatment. [Display omitted] •Designed a new surface structure on the membrane surface.•Terrace-effect porous membrane with high roughness and superhydrophobicity properties.•New structure improved the flux and fouling resistance of membrane.•Terrace-effect MD membrane retard membrane scaling. |
| ArticleNumber | 101153 |
| Author | Kujawski, Wojciech Naddeo, Vincenzo Pervez, Md. Nahid Talukder, Md Eman Figoli, Alberto Talukder, Md. Romon |
| Author_xml | – sequence: 1 givenname: Md Eman surname: Talukder fullname: Talukder, Md Eman email: emant92@gmail.com organization: Faculty of Chemistry, Department of Physical Chemistry and Physical Chemistry of Polymers, Nicolaus Copernicus University, Toruń 87-100, Poland – sequence: 2 givenname: Md. Romon surname: Talukder fullname: Talukder, Md. Romon organization: Department of Chemistry, Government Saadat College, Tangail, Dhaka 1903, Bangladesh – sequence: 3 givenname: Md. Nahid surname: Pervez fullname: Pervez, Md. Nahid organization: Sanitary Environmental Engineering Division (SEED), Department of Civil Engineering, University of Salerno, Fisciano 84084, Italy – sequence: 4 givenname: Wojciech surname: Kujawski fullname: Kujawski, Wojciech organization: Faculty of Chemistry, Department of Physical Chemistry and Physical Chemistry of Polymers, Nicolaus Copernicus University, Toruń 87-100, Poland – sequence: 5 givenname: Alberto surname: Figoli fullname: Figoli, Alberto organization: Institute on Membrane Technology, via pietro Bucci, Rende, Cosenza 87036, Italy – sequence: 6 givenname: Vincenzo orcidid: 0000-0002-3395-3276 surname: Naddeo fullname: Naddeo, Vincenzo email: vnaddeo@unisa.it organization: Sanitary Environmental Engineering Division (SEED), Department of Civil Engineering, University of Salerno, Fisciano 84084, Italy |
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| Keywords | Surface modification High roughness Rice terrace cultivation Super-hydrophobic Terrace effect Membrane distillation |
| Language | English |
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| Title | Fabrication of a super-hydrophobic and high-roughness terrace-effect membrane for enhanced flux and fouling resistance |
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