A study of complex phosphovanadomolybdates [PVxMo12−xO40]−(3+x) by reversed-phase HPLC and capillary zone electrophoresis
A fundamental possibility of using ion-pair reversed-phased HPLC and capillary zone electrophoresis ( CZE ) for the study of polyoxometalate ( POM ) solutions has been demonstrated on an example of phosphovanadomolybdates of the composition [PV x Mo 12 − x O 40 ] −(3 + x ) , where x = 1–3 and the po...
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| Published in | Journal of analytical chemistry (New York, N.Y.) Vol. 70; no. 6; pp. 757 - 764 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
01.06.2015
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| Subjects | |
| Online Access | Get full text |
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| Abstract | A fundamental possibility of using ion-pair reversed-phased HPLC and capillary zone electrophoresis (
CZE
) for the study of polyoxometalate (
POM
) solutions has been demonstrated on an example of phosphovanadomolybdates of the composition [PV
x
Mo
12 −
x
O
40
]
−(3 +
x
)
, where
x
= 1–3 and the possibility of the separation of the products of their synthesis has been shown. It has been found that the modification of the inner surface of a capillary by alkyl groups C
1
and C
8
results in an increase in the resolution of analytical signals in CZE. It has been shown that the results obtained by HPLC and CZE are in a good agreement and can be confirmed by the data of
51
V NMR spectrometry. |
|---|---|
| AbstractList | A fundamental possibility of using ion-pair reversed-phased HPLC and capillary zone electrophoresis (
CZE
) for the study of polyoxometalate (
POM
) solutions has been demonstrated on an example of phosphovanadomolybdates of the composition [PV
x
Mo
12 −
x
O
40
]
−(3 +
x
)
, where
x
= 1–3 and the possibility of the separation of the products of their synthesis has been shown. It has been found that the modification of the inner surface of a capillary by alkyl groups C
1
and C
8
results in an increase in the resolution of analytical signals in CZE. It has been shown that the results obtained by HPLC and CZE are in a good agreement and can be confirmed by the data of
51
V NMR spectrometry. |
| Author | Shuvaeva, O. V. Zhdanov, A. A. |
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| Keywords | capillary zone electrophoresis polyoxometalates phosphomolybdates HPLC |
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| Snippet | A fundamental possibility of using ion-pair reversed-phased HPLC and capillary zone electrophoresis (
CZE
) for the study of polyoxometalate (
POM
) solutions... |
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| SubjectTerms | Analytical Chemistry Chemistry Chemistry and Materials Science |
| Title | A study of complex phosphovanadomolybdates [PVxMo12−xO40]−(3+x) by reversed-phase HPLC and capillary zone electrophoresis |
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