Depth-Sensing Indentation on REBa2Cu3O7−δ Single Crystals Obtained from Xenotime Mineral
A natural mixture of heavy rare-earth oxides extracted from xenotime mineral have been used to prepare large single crystals of the high-temperature REBa 2 Cu 3 O 7−δ superconductor, grown using the CuO–BaO self-flux method. Its mechanical properties along the ab -plane were characterized using inst...
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Published in | Brazilian journal of physics Vol. 42; no. 5-6; pp. 330 - 339 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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Springer-Verlag
01.12.2012
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Abstract | A natural mixture of heavy rare-earth oxides extracted from xenotime mineral have been used to prepare large single crystals of the high-temperature REBa
2
Cu
3
O
7−δ
superconductor, grown using the CuO–BaO self-flux method. Its mechanical properties along the
ab
-plane were characterized using instrumented indentation. Hardness and elastic moduli were measured by the Oliver and Pharr method, which yielded 7.4 ± 0.2 GPa and the range 135–175 GPa at small depths, respectively. Increased loads promote the nucleation of lateral cracks, which reduce hardness and measured elastic modulus, as indicated by instrumented indentation at higher loads. The indentation fracture toughness, estimated by measuring the radial crack length from cube corner indentations at various loads, was found to be 0.8 ± 0.2 MPa m
1/2
. The observed slip systems of REBa
2
Cu
3
O
7−δ
single crystals were [100](001) and [010](001), the same as for YBa
2
Cu
3
O
7−δ
single crystals. The initial stages of deformation and fracture in the indentation process were investigated. The hardness and elastic modulus are not strongly modified by the crystallographic orientation in the
ab
-plane. This was interpreted in terms of resolved shear stresses in the active slip systems. Evidence of cracking along the {100} and {110} planes on the
ab
-plane was observed. In conclusion, the mechanical properties of REBa
2
Cu
3
O
7−δ
single crystals prepared from xenotime are equivalent to those of YBa
2
Cu
3
O
7−δ
single crystals from conventional rare-earth oxides. |
---|---|
AbstractList | A natural mixture of heavy rare-earth oxides extracted from xenotime mineral have been used to prepare large single crystals of the high-temperature REBa
2
Cu
3
O
7−δ
superconductor, grown using the CuO–BaO self-flux method. Its mechanical properties along the
ab
-plane were characterized using instrumented indentation. Hardness and elastic moduli were measured by the Oliver and Pharr method, which yielded 7.4 ± 0.2 GPa and the range 135–175 GPa at small depths, respectively. Increased loads promote the nucleation of lateral cracks, which reduce hardness and measured elastic modulus, as indicated by instrumented indentation at higher loads. The indentation fracture toughness, estimated by measuring the radial crack length from cube corner indentations at various loads, was found to be 0.8 ± 0.2 MPa m
1/2
. The observed slip systems of REBa
2
Cu
3
O
7−δ
single crystals were [100](001) and [010](001), the same as for YBa
2
Cu
3
O
7−δ
single crystals. The initial stages of deformation and fracture in the indentation process were investigated. The hardness and elastic modulus are not strongly modified by the crystallographic orientation in the
ab
-plane. This was interpreted in terms of resolved shear stresses in the active slip systems. Evidence of cracking along the {100} and {110} planes on the
ab
-plane was observed. In conclusion, the mechanical properties of REBa
2
Cu
3
O
7−δ
single crystals prepared from xenotime are equivalent to those of YBa
2
Cu
3
O
7−δ
single crystals from conventional rare-earth oxides. |
Author | Serbena, Francisco Carlos Jurelo, Alcione Roberto Mikowski, Alexandre Júnior, Pedro Rodrigues Lepienski, Carlos Maurício Foerster, Carlos Eugênio Carubelli, Célia Regina |
Author_xml | – sequence: 1 givenname: Francisco Carlos surname: Serbena fullname: Serbena, Francisco Carlos email: fserbena@uepg.br organization: Departamento de Física, Universidade Estadual de Ponta Grossa – sequence: 2 givenname: Carlos Eugênio surname: Foerster fullname: Foerster, Carlos Eugênio organization: Departamento de Física, Universidade Estadual de Ponta Grossa – sequence: 3 givenname: Alcione Roberto surname: Jurelo fullname: Jurelo, Alcione Roberto organization: Departamento de Física, Universidade Estadual de Ponta Grossa – sequence: 4 givenname: Alexandre surname: Mikowski fullname: Mikowski, Alexandre organization: Centro de Engenharia da Mobilidade, Universidade Federal de Santa Catarina – sequence: 5 givenname: Pedro Rodrigues surname: Júnior fullname: Júnior, Pedro Rodrigues organization: Departamento de Física, Universidade Estadual de Ponta Grossa – sequence: 6 givenname: Célia Regina surname: Carubelli fullname: Carubelli, Célia Regina organization: Departamento de Química, Universidade Estadual de Ponta Grossa – sequence: 7 givenname: Carlos Maurício surname: Lepienski fullname: Lepienski, Carlos Maurício organization: Departamento de Física, Universidade Federal do Paraná |
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Keywords | Mechanical properties High-temperature superconductors Single crystal Xenotime |
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Snippet | A natural mixture of heavy rare-earth oxides extracted from xenotime mineral have been used to prepare large single crystals of the high-temperature REBa
2
Cu... |
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SubjectTerms | Condensed Matter Physics Physics and Astronomy |
Title | Depth-Sensing Indentation on REBa2Cu3O7−δ Single Crystals Obtained from Xenotime Mineral |
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