New azo Dyes Based on 1,3-dihydroxynitrobenzene and 2,4,6-trihydroxynitrobenzene for Polycaproamide Fibers
Syntheses of 16 previously undescribed mono- and bis-azo compounds in 70-95% yields via azo coupling of 1,3-dihydroxynitrobenzene and 2,4,6-trihydroxynitrobenzene with structurally varied aryldiazonium salts are reported. The synthesized mono- and bis-azo compounds were tested as acid and disperse d...
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| Published in | Fibre chemistry Vol. 53; no. 6; pp. 446 - 450 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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01.03.2022
Springer Springer Nature B.V |
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| Abstract | Syntheses of 16 previously undescribed mono- and bis-azo compounds in 70-95% yields via azo coupling of 1,3-dihydroxynitrobenzene and 2,4,6-trihydroxynitrobenzene with structurally varied aryldiazonium salts are reported. The synthesized mono- and bis-azo compounds were tested as acid and disperse dyes for polycaproamide fiber. Results of stability tests of the color fastness to washing (GOST 9733.4-–83) and perspiration (GOST 9733.6–83) indicated that the dyes had good operational properties. Conclusions were made about the dependence of the dye stability on the structures of the tested azo compounds. |
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| AbstractList | Syntheses of 16 previously undescribed mono- and bis-azo compounds in 70-95% yields via azo coupling of 1,3-dihydroxynitrobenzene and 2,4,6-trihydroxynitrobenzene with structurally varied aryldiazonium salts are reported. The synthesized mono- and bis-azo compounds were tested as acid and disperse dyes for polycaproamide fiber. Results of stability tests of the color fastness to washing (GOST 9733.4-–83) and perspiration (GOST 9733.6–83) indicated that the dyes had good operational properties. Conclusions were made about the dependence of the dye stability on the structures of the tested azo compounds. |
| Audience | Academic |
| Author | Meleshenkova, V. V. Shukurov, R. O. Kuznetsov, D. N. |
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| References | S. A. Shevelev, A. Kh. Shakhnes, and S. S. Vorob’ev, RU Pat. 2,292,329, “Method for preparing 2,4,6-trihydroxybenzene,” Jan. 27, 2007. K. I. Kobrakov, V. I. Ushkarov, et al., RU Pat. No. 2,415,892, “Method of producing mono- or disazo [sic] dyes based on methylphloroglucinol,” Apr. 10, 2011. I. A. Shchurova, S. V. Sysolyatin, et al., Yuzhno-sib. Nauchn. Vestn., 28, No. 4, 214-218 (2019); DOI: https://doi.org/10.25699/SSSB.2019.28.46376. A. I. Alafinov, K. I. Kobrakov, et al., Butlerov. Soobshch., 33, No. 3, 93-99 (2013); DOI: jbc-01/13-33-3-93. V. I. Ushkarov, K. I. Kobrakov, et al., Theor. Found. Chem. Eng., 41, 671-674 (2007); DOI: https://doi.org/10.1134/S0040579507050375. UshkarovVIKobrakovKIFibre Chem.20063831881901:CAS:528:DC%2BD28XhtFShtLrL10.1007/s10692-006-0067-3 Acute Rat Toxicity Prediction; http://way2drug.com/gusar/acutoxpredict.html (accessed May 15, 2020). VI Ushkarov (10327_CR5) 2006; 38 10327_CR6 10327_CR7 10327_CR2 10327_CR1 10327_CR4 10327_CR3 |
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| SubjectTerms | Azo compounds Chemistry Chemistry and Materials Science Color fastness Coupling (molecular) Dyes Organic Chemistry Perspiration Polymer Sciences Stability tests Structural stability Substitution reactions |
| Title | New azo Dyes Based on 1,3-dihydroxynitrobenzene and 2,4,6-trihydroxynitrobenzene for Polycaproamide Fibers |
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