Synthesis and Characterization of Spark Plasma Sintered FeAl and In situ FeAl–Al2O3 Composite

In the present work, nanocrystalline FeAl and FeAl–Al 2 O 3 composite were synthesized by high energy ball milling and subsequent compaction by spark plasma sintering. Microstructural changes during all stages of processing are studied using X-ray analysis. After 20 h of milling, the disordered FeAl...

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Published inTransactions of the Indian Institute of Metals Vol. 66; no. 4; pp. 419 - 424
Main Authors Chawake, Niraj, Paleti, Sri Harish Kumar, Murty, B. S., Kottada, Ravi S.
Format Journal Article
LanguageEnglish
Published India Springer-Verlag 01.08.2013
Subjects
Chemistry and Materials Science
Corrosion and Coatings
Materials Science
Metallic Materials
Technical Paper
Tribology
Iron aluminide
Spark plasma sintering
Reactive milling
Disordering
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Abstract In the present work, nanocrystalline FeAl and FeAl–Al 2 O 3 composite were synthesized by high energy ball milling and subsequent compaction by spark plasma sintering. Microstructural changes during all stages of processing are studied using X-ray analysis. After 20 h of milling, the disordered FeAl and some amount of Fe rich solid solution was obtained in both of these compositions. Subsequent heat treatment results in formation of ordered FeAl. However, disordering of FeAl was observed in both compositions after spark plasma sintering. Nanocrystallinity is retained in both the compositions even after sintering at high temperature of 1,000 °C. Very high hardness of ~575 HV 1 and ~600 HV 1 was exhibited by FeAl and FeAl–Al 2 O 3 composite.
AbstractList In the present work, nanocrystalline FeAl and FeAl–Al 2 O 3 composite were synthesized by high energy ball milling and subsequent compaction by spark plasma sintering. Microstructural changes during all stages of processing are studied using X-ray analysis. After 20 h of milling, the disordered FeAl and some amount of Fe rich solid solution was obtained in both of these compositions. Subsequent heat treatment results in formation of ordered FeAl. However, disordering of FeAl was observed in both compositions after spark plasma sintering. Nanocrystallinity is retained in both the compositions even after sintering at high temperature of 1,000 °C. Very high hardness of ~575 HV 1 and ~600 HV 1 was exhibited by FeAl and FeAl–Al 2 O 3 composite.
Author Kottada, Ravi S.
Paleti, Sri Harish Kumar
Murty, B. S.
Chawake, Niraj
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Keywords Iron aluminide
Spark plasma sintering
Reactive milling
Disordering
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  ident: 279_CR23
  publication-title: Intermetallics
  doi: 10.1016/S0966-9795(03)00027-X
  contributor:
    fullname: JL Jordan
– volume: 102
  start-page: 114913
  year: 2007
  ident: 279_CR13
  publication-title: J Appl Phys
  doi: 10.1063/1.2822189
  contributor:
    fullname: A Olevsky Eugene
SSID ssj0039233
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Snippet In the present work, nanocrystalline FeAl and FeAl–Al 2 O 3 composite were synthesized by high energy ball milling and subsequent compaction by spark plasma...
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SubjectTerms Chemistry and Materials Science
Corrosion and Coatings
Materials Science
Metallic Materials
Technical Paper
Tribology
Title Synthesis and Characterization of Spark Plasma Sintered FeAl and In situ FeAl–Al2O3 Composite
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