Peroxide-based route assisted with inverse microemulsion process to well-dispersed Bi4Ti3O12 nanocrystals

Well-dispersed bismuth titanate (BIT) nanocrystals with an average size ranged from 3 to 60 nm were synthesized via a peroxide-based route assisted with an inverse microemulsion process. The crystallite size and lattice parameter of BIT upon variable-temperature were determined by X-ray diffraction...

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Published inJournal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology Vol. 12; no. 5; pp. 1797 - 1805
Main Authors Hou, Jungang, Qu, Yuanfang, Krsmanovic, Dalibor, Kumar, R. V.
Format Journal Article
LanguageEnglish
Published Dordrecht Springer Netherlands 01.06.2010
Subjects
Characterization and Evaluation of Materials
Chemistry and Materials Science
Inorganic Chemistry
Lasers
Materials Science
Nanotechnology
Optical Devices
Optics
Photonics
Physical Chemistry
Research Paper
Bismuth titanate
Nanocrystals
Peroxide
Microemulsion
Crystallization
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Abstract Well-dispersed bismuth titanate (BIT) nanocrystals with an average size ranged from 3 to 60 nm were synthesized via a peroxide-based route assisted with an inverse microemulsion process. The crystallite size and lattice parameter of BIT upon variable-temperature were determined by X-ray diffraction (XRD). The particle size was confirmed by transmission electron microscopy (TEM). Thermal decomposition behaviour of Ti-peroxy and BIT gel and crystallization kinetics of BIT nanocrystals were investigated by differential scanning calorimetry/thermogravimetry (DSC/TG) and Fourier-Transform infrared spectroscopy (FTIR). Analysis of nonisothermal DSC data yielded a value of 220.84 ± 2.73 KJ/mol and 2.25 ± 0.26 for the activation energy of crystallization ( E a ) and the Avrami exponent ( n ), respectively.
AbstractList Well-dispersed bismuth titanate (BIT) nanocrystals with an average size ranged from 3 to 60 nm were synthesized via a peroxide-based route assisted with an inverse microemulsion process. The crystallite size and lattice parameter of BIT upon variable-temperature were determined by X-ray diffraction (XRD). The particle size was confirmed by transmission electron microscopy (TEM). Thermal decomposition behaviour of Ti-peroxy and BIT gel and crystallization kinetics of BIT nanocrystals were investigated by differential scanning calorimetry/thermogravimetry (DSC/TG) and Fourier-Transform infrared spectroscopy (FTIR). Analysis of nonisothermal DSC data yielded a value of 220.84 ± 2.73 KJ/mol and 2.25 ± 0.26 for the activation energy of crystallization ( E a ) and the Avrami exponent ( n ), respectively.
Author Krsmanovic, Dalibor
Qu, Yuanfang
Kumar, R. V.
Hou, Jungang
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  givenname: Jungang
  surname: Hou
  fullname: Hou, Jungang
  organization: Department of Materials Science and Metallurgy, University of Cambridge, Key Laboratory for Advanced Ceramic and Machining Technology of Ministry of Education, Tianjin University
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  givenname: Yuanfang
  surname: Qu
  fullname: Qu, Yuanfang
  organization: Key Laboratory for Advanced Ceramic and Machining Technology of Ministry of Education, Tianjin University
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  givenname: Dalibor
  surname: Krsmanovic
  fullname: Krsmanovic, Dalibor
  organization: Department of Materials Science and Metallurgy, University of Cambridge
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  surname: Kumar
  fullname: Kumar, R. V.
  email: rvk10@cam.ac.uk
  organization: Department of Materials Science and Metallurgy, University of Cambridge
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Issue 5
Keywords Bismuth titanate
Nanocrystals
Peroxide
Microemulsion
Crystallization
Language English
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Snippet Well-dispersed bismuth titanate (BIT) nanocrystals with an average size ranged from 3 to 60 nm were synthesized via a peroxide-based route assisted with an...
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StartPage 1797
SubjectTerms Characterization and Evaluation of Materials
Chemistry and Materials Science
Inorganic Chemistry
Lasers
Materials Science
Nanotechnology
Optical Devices
Optics
Photonics
Physical Chemistry
Research Paper
Title Peroxide-based route assisted with inverse microemulsion process to well-dispersed Bi4Ti3O12 nanocrystals
URI https://link.springer.com/article/10.1007/s11051-009-9737-4
Volume 12
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