A new insight on the diffusion growth mechanism of intermetallic compounds in Al-Er system
[Display omitted] •During annealing, the growth characteristics of Al-Er intermetallic compounds are accord with layer-terraced growth.•In Al-Er system, AlEr grows by consuming Er component, the growth of Al3Er proceeds by swallowing AlEr.•The pre-exponential factor and activation energy of the Al3E...
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Published in | Materials & design Vol. 224; p. 111341 |
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Main Authors | , , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.12.2022
Elsevier |
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Abstract | [Display omitted]
•During annealing, the growth characteristics of Al-Er intermetallic compounds are accord with layer-terraced growth.•In Al-Er system, AlEr grows by consuming Er component, the growth of Al3Er proceeds by swallowing AlEr.•The pre-exponential factor and activation energy of the Al3Er are 7.126 × 10−8 m2·s−1 and (88.4 ± 5.3) kJ·mol−1 respectively.•Al-Er diffusion couples were successfully prepared by casting cladding in the atmosphere.
The diffusion growth of intermetallic compounds in Al-Er alloys are closely related to the properties of the alloys. The current work aims at explaining the dominance of Al3Er in the Al-Er alloys precipitation phases and the interface thin layer phenomenon by diffusion couple technique, estimating the parabolic growth constant and diffusion activation energy of intermetallic compound in Al-Er diffusion couples to provide theoretical guidance for the design of new Al-Er alloys. In this work, Al-Er diffusion couples were successfully prepared by casting-cladding method in the atmosphere. The growth of Al-Er intermetallic compounds at diffusion couple interface during annealing were observed and recorded by High-Temperature Laser-Scanning Confocal Microscopy at 673, 698, 723 and 748 K respectively. The results show that the growth characteristics of Al-Er intermetallic compounds were accord with layer-terraced growth during annealing. The thickness of intermetallic compound was linear with the square root of time at experimental temperature. The intermetallic compound layer was composed of Al3Er and a very thin AlEr phase. The parabolic growth constants of Al3Er phase at 673, 698, 723 and 748 K were 1.017 × 10−14, 1.609 × 10−14, 3.111 × 10−14 and 4.76 × 10−14 respectively. The activation energy of Al3Er phase was (88.4 ± 5.3) kJ/mol and the pre-exponential factor was 7.126 × 10−8 m2/s. |
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AbstractList | [Display omitted]
•During annealing, the growth characteristics of Al-Er intermetallic compounds are accord with layer-terraced growth.•In Al-Er system, AlEr grows by consuming Er component, the growth of Al3Er proceeds by swallowing AlEr.•The pre-exponential factor and activation energy of the Al3Er are 7.126 × 10−8 m2·s−1 and (88.4 ± 5.3) kJ·mol−1 respectively.•Al-Er diffusion couples were successfully prepared by casting cladding in the atmosphere.
The diffusion growth of intermetallic compounds in Al-Er alloys are closely related to the properties of the alloys. The current work aims at explaining the dominance of Al3Er in the Al-Er alloys precipitation phases and the interface thin layer phenomenon by diffusion couple technique, estimating the parabolic growth constant and diffusion activation energy of intermetallic compound in Al-Er diffusion couples to provide theoretical guidance for the design of new Al-Er alloys. In this work, Al-Er diffusion couples were successfully prepared by casting-cladding method in the atmosphere. The growth of Al-Er intermetallic compounds at diffusion couple interface during annealing were observed and recorded by High-Temperature Laser-Scanning Confocal Microscopy at 673, 698, 723 and 748 K respectively. The results show that the growth characteristics of Al-Er intermetallic compounds were accord with layer-terraced growth during annealing. The thickness of intermetallic compound was linear with the square root of time at experimental temperature. The intermetallic compound layer was composed of Al3Er and a very thin AlEr phase. The parabolic growth constants of Al3Er phase at 673, 698, 723 and 748 K were 1.017 × 10−14, 1.609 × 10−14, 3.111 × 10−14 and 4.76 × 10−14 respectively. The activation energy of Al3Er phase was (88.4 ± 5.3) kJ/mol and the pre-exponential factor was 7.126 × 10−8 m2/s. The diffusion growth of intermetallic compounds in Al-Er alloys are closely related to the properties of the alloys. The current work aims at explaining the dominance of Al3Er in the Al-Er alloys precipitation phases and the interface thin layer phenomenon by diffusion couple technique, estimating the parabolic growth constant and diffusion activation energy of intermetallic compound in Al-Er diffusion couples to provide theoretical guidance for the design of new Al-Er alloys. In this work, Al-Er diffusion couples were successfully prepared by casting-cladding method in the atmosphere. The growth of Al-Er intermetallic compounds at diffusion couple interface during annealing were observed and recorded by High-Temperature Laser-Scanning Confocal Microscopy at 673, 698, 723 and 748 K respectively. The results show that the growth characteristics of Al-Er intermetallic compounds were accord with layer-terraced growth during annealing. The thickness of intermetallic compound was linear with the square root of time at experimental temperature. The intermetallic compound layer was composed of Al3Er and a very thin AlEr phase. The parabolic growth constants of Al3Er phase at 673, 698, 723 and 748 K were 1.017 × 10−14, 1.609 × 10−14, 3.111 × 10−14 and 4.76 × 10−14 respectively. The activation energy of Al3Er phase was (88.4 ± 5.3) kJ/mol and the pre-exponential factor was 7.126 × 10−8 m2/s. |
ArticleNumber | 111341 |
Author | Tan, Yapeng Tang, Zhichao Zhu, Weiqiang Cui, Jin Yu, Muzhi Xu, Tao Yang, Bo Xu, Zhengbing Zeng, Jianmin Yang, Haodong |
Author_xml | – sequence: 1 givenname: Zhichao surname: Tang fullname: Tang, Zhichao organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 2 givenname: Jin surname: Cui fullname: Cui, Jin organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 3 givenname: Muzhi surname: Yu fullname: Yu, Muzhi organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 4 givenname: Weiqiang surname: Zhu fullname: Zhu, Weiqiang organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 5 givenname: Zhengbing surname: Xu fullname: Xu, Zhengbing email: xuzhb@gxu.edu.cn organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 6 givenname: Jianmin surname: Zeng fullname: Zeng, Jianmin email: zjmg@gxu.edu.cn organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 7 givenname: Tao surname: Xu fullname: Xu, Tao organization: Anhui Antai New Style Packeting Materials Co., Ltd, Hefei 231203, China – sequence: 8 givenname: Haodong surname: Yang fullname: Yang, Haodong organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 9 givenname: Yapeng surname: Tan fullname: Tan, Yapeng organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China – sequence: 10 givenname: Bo surname: Yang fullname: Yang, Bo organization: Key Laboratory of Nonferrous Materials and New Processing Technology, School of Resources, Environment and Materials, Guangxi University, Nanning 530004, China |
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Keywords | High-Temperature Laser-Scanning Confocal Microscopy (HTLSCM) Intermetallic compound (IMC) Parabolic growth constant (PGC) Diffusion Casting-cladding method Activation energy |
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•During annealing, the growth characteristics of Al-Er intermetallic compounds are accord with layer-terraced growth.•In Al-Er system, AlEr... The diffusion growth of intermetallic compounds in Al-Er alloys are closely related to the properties of the alloys. The current work aims at explaining the... |
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SubjectTerms | Activation energy Casting-cladding method Diffusion High-Temperature Laser-Scanning Confocal Microscopy (HTLSCM) Intermetallic compound (IMC) Parabolic growth constant (PGC) |
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Title | A new insight on the diffusion growth mechanism of intermetallic compounds in Al-Er system |
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