Synthesis, crystal structure, Hirshfeld surface analyses and antibacterial activity of 2-fluorobenzylpyridinium tetrabromidocuprate(II)

In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy] 2 [CuBr 4 ], has been obtained by using a slow evaporation solution-growth method and was characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy...

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Published inMolecular Crystals and Liquid Crystals Vol. 769; no. 1; pp. 102 - 115
Main Authors Chen, Yan-Lin, Li, Xin-Ran, Li, Xiang-Ling, Hu, Bao-Yi, Jiang, Yan, Ni, Chun-Lin
Format Journal Article
LanguageEnglish
Published Philadelphia Taylor & Francis 02.01.2025
Taylor & Francis Ltd
Subjects
Antibacterial activities
Antiinfectives and antibacterials
Chemical bonds
Chemical synthesis
Crystal structure
Crystals
E coli
Evaporation
Hirshfeld surface analyses
Hydrogen bonding
Infrared analysis
Infrared spectroscopy
Optical properties
organic-inorganic hybrid
Semiconductor materials
Surface analysis (chemical)
tetrabromidocuprate salts(II)
X ray powder diffraction
X-ray diffraction
Online AccessGet full text
ISSN1542-1406
1563-5287
1527-1943
DOI10.1080/15421406.2024.2429177

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Abstract In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy] 2 [CuBr 4 ], has been obtained by using a slow evaporation solution-growth method and was characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy, UV-visible diffuse reflectance spectrum. The compound crystallizes in the monoclinic space group P2 1 /c, and the packing is governed by C − H···Br hydrogen bonding interactions, which was confirmed by the Hirshfeld surface analysis. The results of antimicrobial experiments showed that the compound possessed excellent antimicrobial activity against Staphylococcus aureus and Escherichia coli. RESEARCH HIGHLIGHTS An inorganic-organic hybrid salt [2FBzPy] 2 [CuBr 4 ] was synthesized and characterized. The main intermolecular interaction in [2FBzPy] 2 [CuBr 4 ] crystals have been studied and analyzed. The interactions between different molecules in[2FBzPy] 2 [CuBr 4 ] were examined by Hirshfeld surface analyses. [2FBzPy] 2 [CuBr 4 ] had an optical band gap of 1.69 eV, was a typical semiconductor material with good optical property. The as-synthesized salts exhibits good antibacterial activities against S. aureus and E. coli.
AbstractList In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy]2[CuBr4], has been obtained by using a slow evaporation solution-growth method and was characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy, UV–visible diffuse reflectance spectrum. The compound crystallizes in the monoclinic space group P21/c, and the packing is governed by C − H···Br hydrogen bonding interactions, which was confirmed by the Hirshfeld surface analysis. The results of antimicrobial experiments showed that the compound possessed excellent antimicrobial activity against Staphylococcus aureus and Escherichia coli.RESEARCH HIGHLIGHTSAn inorganic-organic hybrid salt [2FBzPy]2[CuBr4] was synthesized and characterized.The main intermolecular interaction in [2FBzPy]2[CuBr4] crystals have been studied and analyzed.The interactions between different molecules in[2FBzPy]2 [CuBr4] were examined by Hirshfeld surface analyses.[2FBzPy]2[CuBr4] had an optical band gap of 1.69 eV, was a typical semiconductor material with good optical property.The as-synthesized salts exhibits good antibacterial activities against S. aureus and E. coli.
In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy] 2 [CuBr 4 ], has been obtained by using a slow evaporation solution-growth method and was characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy, UV-visible diffuse reflectance spectrum. The compound crystallizes in the monoclinic space group P2 1 /c, and the packing is governed by C − H···Br hydrogen bonding interactions, which was confirmed by the Hirshfeld surface analysis. The results of antimicrobial experiments showed that the compound possessed excellent antimicrobial activity against Staphylococcus aureus and Escherichia coli. RESEARCH HIGHLIGHTS An inorganic-organic hybrid salt [2FBzPy] 2 [CuBr 4 ] was synthesized and characterized. The main intermolecular interaction in [2FBzPy] 2 [CuBr 4 ] crystals have been studied and analyzed. The interactions between different molecules in[2FBzPy] 2 [CuBr 4 ] were examined by Hirshfeld surface analyses. [2FBzPy] 2 [CuBr 4 ] had an optical band gap of 1.69 eV, was a typical semiconductor material with good optical property. The as-synthesized salts exhibits good antibacterial activities against S. aureus and E. coli.
Author Chen, Yan-Lin
Li, Xin-Ran
Hu, Bao-Yi
Jiang, Yan
Ni, Chun-Lin
Li, Xiang-Ling
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Snippet In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy] 2 [CuBr 4 ], has been obtained by using a...
In this article, novel organic-inorganic hybrid material, 2-fluorobenzylpyridinium tetrabromidocuprate(II) [2FBzPy]2[CuBr4], has been obtained by using a slow...
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SubjectTerms Antibacterial activities
Antiinfectives and antibacterials
Chemical bonds
Chemical synthesis
Crystal structure
Crystals
E coli
Evaporation
Hirshfeld surface analyses
Hydrogen bonding
Infrared analysis
Infrared spectroscopy
Optical properties
organic-inorganic hybrid
Semiconductor materials
Surface analysis (chemical)
tetrabromidocuprate salts(II)
X ray powder diffraction
X-ray diffraction
Title Synthesis, crystal structure, Hirshfeld surface analyses and antibacterial activity of 2-fluorobenzylpyridinium tetrabromidocuprate(II)
URI https://www.tandfonline.com/doi/abs/10.1080/15421406.2024.2429177
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Volume 769
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