ZnCl2 enabled synthesis of activated carbons from ion-exchange resin for efficient removal of Cu2+ ions from water via capacitive deionization
Capacitive deionization (CDI) is a promising method to remove metal contaminants in water. Herein, we report on the preparation of activated carbon from cation-exchange resin by introducing ZnCl2 via ion exchange followed by heat treatment and CO2 activation, which is evaluated for removal of Cu2+ i...
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| Published in | Chemosphere (Oxford) Vol. 264; p. 128557 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.02.2021
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| Abstract | Capacitive deionization (CDI) is a promising method to remove metal contaminants in water. Herein, we report on the preparation of activated carbon from cation-exchange resin by introducing ZnCl2 via ion exchange followed by heat treatment and CO2 activation, which is evaluated for removal of Cu2+ in water via CDI technology. The results have shown that both the heat treatment and the CO2 activation are helpful to tune the pore structure of the activated carbons in terms of ions adsorption and transportation. The activated carbon prepared by heat treatment at 600 °C and CO2 activation at 750 °C, named as AC-600-750, has the highest specific surface area of 1162 m2 g−1 and a specific capacitance of 247.4 F g−1 at 50 mV−1, with a Cu2+ adsorption capacity of 77.8 mg g−1 at 1.2 V in 50 mg L−1 CuCl2 solution that is much higher than that of the commercial activated carbon. The electrosorption of Cu2+ ions over activated carbon follows a monolayer adsorption scheme, of which the kinetic can be well explained by pseudo-first-order kinetic model. The resin-based activated carbons are of potential as an electrode material for efficient removal of heavy metal from contaminated water by CDI process.
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•Activated carbon from cation-exchange resin was prepared by ion exchange with ZnCl2.•Activated carbon showed high Cu2+ adsorption capacity of 77.8 mg g−1 by CDI process.•The electrosorption of Cu2+ followed pseudo-first order kinetic and Langmuir model. |
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| AbstractList | Capacitive deionization (CDI) is a promising method to remove metal contaminants in water. Herein, we report on the preparation of activated carbon from cation-exchange resin by introducing ZnCl2 via ion exchange followed by heat treatment and CO2 activation, which is evaluated for removal of Cu2+ in water via CDI technology. The results have shown that both the heat treatment and the CO2 activation are helpful to tune the pore structure of the activated carbons in terms of ions adsorption and transportation. The activated carbon prepared by heat treatment at 600 °C and CO2 activation at 750 °C, named as AC-600-750, has the highest specific surface area of 1162 m2 g−1 and a specific capacitance of 247.4 F g−1 at 50 mV−1, with a Cu2+ adsorption capacity of 77.8 mg g−1 at 1.2 V in 50 mg L−1 CuCl2 solution that is much higher than that of the commercial activated carbon. The electrosorption of Cu2+ ions over activated carbon follows a monolayer adsorption scheme, of which the kinetic can be well explained by pseudo-first-order kinetic model. The resin-based activated carbons are of potential as an electrode material for efficient removal of heavy metal from contaminated water by CDI process.
[Display omitted]
•Activated carbon from cation-exchange resin was prepared by ion exchange with ZnCl2.•Activated carbon showed high Cu2+ adsorption capacity of 77.8 mg g−1 by CDI process.•The electrosorption of Cu2+ followed pseudo-first order kinetic and Langmuir model. |
| ArticleNumber | 128557 |
| Author | Che, Lei Zhou, Jie Zhu, Pengfei Yan, Pengjie Wu, Shengji Wang, Hui Yang, Wei |
| Author_xml | – sequence: 1 givenname: Shengji surname: Wu fullname: Wu, Shengji organization: College of Engineering, Huzhou University, No. 759, East 2nd Road, 313000, Huzhou, China – sequence: 2 givenname: Pengjie surname: Yan fullname: Yan, Pengjie organization: College of Materials and Environmental Engineering, Hangzhou Dianzi University, Xiasha University Park, Hangzhou, 310018, China – sequence: 3 givenname: Wei surname: Yang fullname: Yang, Wei email: wei_yang15@hotmail.com organization: College of Engineering, Huzhou University, No. 759, East 2nd Road, 313000, Huzhou, China – sequence: 4 givenname: Jie orcidid: 0000-0003-2287-5396 surname: Zhou fullname: Zhou, Jie organization: College of Materials and Environmental Engineering, Hangzhou Dianzi University, Xiasha University Park, Hangzhou, 310018, China – sequence: 5 givenname: Hui orcidid: 0000-0002-5077-0615 surname: Wang fullname: Wang, Hui organization: College of Materials and Environmental Engineering, Hangzhou Dianzi University, Xiasha University Park, Hangzhou, 310018, China – sequence: 6 givenname: Lei surname: Che fullname: Che, Lei organization: College of Engineering, Huzhou University, No. 759, East 2nd Road, 313000, Huzhou, China – sequence: 7 givenname: Pengfei surname: Zhu fullname: Zhu, Pengfei organization: College of Engineering, Huzhou University, No. 759, East 2nd Road, 313000, Huzhou, China |
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| Keywords | Capacitive deionization Copper ions Electrosorption Ion exchange resin Activated carbon |
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| Title | ZnCl2 enabled synthesis of activated carbons from ion-exchange resin for efficient removal of Cu2+ ions from water via capacitive deionization |
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