Ultrafiltration membranes prepared via mixed solvent phase separation with enhanced performance for produced water treatment
Ultrafiltration (UF) is a promising membrane process to remove surfactant-stabilized oil emulsions from produced water (PW). However, UF membranes prepared by conventional methods have suffered from low permeate flux and are susceptible to fouling due to the sparsity of pores on the surface. In this...
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| Published in | Journal of membrane science Vol. 670; p. 121375 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.03.2023
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Ultrafiltration (UF) is a promising membrane process to remove surfactant-stabilized oil emulsions from produced water (PW). However, UF membranes prepared by conventional methods have suffered from low permeate flux and are susceptible to fouling due to the sparsity of pores on the surface. In this study, we used our recently developed mixed solvent phase separation (MSPS) method to fabricate a highly porous poly (vinylidene fluoride) (PVDF) ultrafiltration membrane for the treatment of produced water. The prepared MSPS PVDF membrane showed an asymmetric high-porous structure with a surface porosity of 23.66% and a narrow pore size distribution of 40 ± 19 nm. The MSPS PVDF membrane showed almost complete oil removal and high oily water permeance above 300 L m−2 h−1·bar−1 even after 72 h of continuous testing, which is an order of magnitude higher than the commercial PVDF membranes. In addition, the MSPS PVDF membrane showed excellent regeneration and recovery capabilities with a flux recovery ratio of 97% without any chemical cleaning, making the process economically and environmentally more viable. Moreover, we achieved optimal membrane performance without any further surface modification processes.
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•High-porous PVDF membranes with 23.7% surface porosity was prepared by MSPS method.•Ultrafiltration of produced water showed flux >300 LMH/Bar even after 75 h.•Excellent antifouling properties with >97% flux recovery and 99.99% TOC removal.•Easy flux recovery by a low-pressure DI water backwash without chemical additives. |
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| AbstractList | Ultrafiltration (UF) is a promising membrane process to remove surfactant-stabilized oil emulsions from produced water (PW). However, UF membranes prepared by conventional methods have suffered from low permeate flux and are susceptible to fouling due to the sparsity of pores on the surface. In this study, we used our recently developed mixed solvent phase separation (MSPS) method to fabricate a highly porous poly (vinylidene fluoride) (PVDF) ultrafiltration membrane for the treatment of produced water. The prepared MSPS PVDF membrane showed an asymmetric high-porous structure with a surface porosity of 23.66% and a narrow pore size distribution of 40 ± 19 nm. The MSPS PVDF membrane showed almost complete oil removal and high oily water permeance above 300 L m−2 h−1·bar−1 even after 72 h of continuous testing, which is an order of magnitude higher than the commercial PVDF membranes. In addition, the MSPS PVDF membrane showed excellent regeneration and recovery capabilities with a flux recovery ratio of 97% without any chemical cleaning, making the process economically and environmentally more viable. Moreover, we achieved optimal membrane performance without any further surface modification processes.
[Display omitted]
•High-porous PVDF membranes with 23.7% surface porosity was prepared by MSPS method.•Ultrafiltration of produced water showed flux >300 LMH/Bar even after 75 h.•Excellent antifouling properties with >97% flux recovery and 99.99% TOC removal.•Easy flux recovery by a low-pressure DI water backwash without chemical additives. |
| ArticleNumber | 121375 |
| Author | Liu, Xiaowei Cao, Li Lai, Zhiping Thankamony, Roshni L. Zhou, Zongyao Nuaimi, Reham A. |
| Author_xml | – sequence: 1 givenname: Reham A. surname: Nuaimi fullname: Nuaimi, Reham A. – sequence: 2 givenname: Roshni L. orcidid: 0000-0002-1175-7311 surname: Thankamony fullname: Thankamony, Roshni L. – sequence: 3 givenname: Xiaowei surname: Liu fullname: Liu, Xiaowei – sequence: 4 givenname: Li surname: Cao fullname: Cao, Li – sequence: 5 givenname: Zongyao surname: Zhou fullname: Zhou, Zongyao – sequence: 6 givenname: Zhiping orcidid: 0000-0001-9555-6009 surname: Lai fullname: Lai, Zhiping email: Zhiping.lai@kaust.edu.sa |
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| Keywords | Oil-water separation Mixed solvent phase separation PVDF membrane Ultrafiltration Produced water |
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| SubjectTerms | Mixed solvent phase separation Oil-water separation Produced water PVDF membrane Ultrafiltration |
| Title | Ultrafiltration membranes prepared via mixed solvent phase separation with enhanced performance for produced water treatment |
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