The FTIR studies of gels and thin films of Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems
[Display omitted] ► The bulk samples and thin films from Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems. ► Amorphous and homogenous materials up to 500°C. ► Al in octahedral coordination. ► Al in tetrahedral coordination when substitutes Si. In this work, samples in form of bulk ones and thin films were obt...
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Published in | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy Vol. 89; pp. 11 - 17 |
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Main Authors | , |
Format | Journal Article |
Language | English |
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England
Elsevier B.V
01.04.2012
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Abstract | [Display omitted]
► The bulk samples and thin films from Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems. ► Amorphous and homogenous materials up to 500°C. ► Al in octahedral coordination. ► Al in tetrahedral coordination when substitutes Si.
In this work, samples in form of bulk ones and thin films were obtained using the sol–gel method. The bulk samples were heated at different temperatures (500°C, 850°C and 1100°C) corresponding to the annealing process of coatings, deposited on different substrates by dipping and pulling out samples from the proper sol with the stable speed. Thin films of both Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems were deposited on carbon, steel and titanium substrates in two different ways: as single layers obtained from Al2O3 sol, TiO2 sol and Al2O3 sol or deposited as mixed coatings from Al2O3–TiO2 sol as well as Al2O3–TiO2–SiO2 one.
All bulk samples were studied by the FTIR spectroscopy and the X-ray diffractometry while thin films were also investigated by the electron microscopy.
In the IR spectra of Al2O3–TiO2 samples, as well as gels and coatings, bands due to the vibrations of AlO bonds of the octahedrally and tetrahedrally coordinated aluminum were observed.
The IR spectra of samples of Al2O3–TiO2–SiO2 system differ from that of Al2O3–TiO2 ones in presence of bands assigned to the SiO bond vibrations and in positions of bands due to AlO bond vibrations. In all spectra of bulk samples and coatings, the positions of TiO bond vibrations were ascribed basing on the IR spectra of the pure anatase and rutile. |
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AbstractList | [Display omitted]
► The bulk samples and thin films from Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems. ► Amorphous and homogenous materials up to 500°C. ► Al in octahedral coordination. ► Al in tetrahedral coordination when substitutes Si.
In this work, samples in form of bulk ones and thin films were obtained using the sol–gel method. The bulk samples were heated at different temperatures (500°C, 850°C and 1100°C) corresponding to the annealing process of coatings, deposited on different substrates by dipping and pulling out samples from the proper sol with the stable speed. Thin films of both Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems were deposited on carbon, steel and titanium substrates in two different ways: as single layers obtained from Al2O3 sol, TiO2 sol and Al2O3 sol or deposited as mixed coatings from Al2O3–TiO2 sol as well as Al2O3–TiO2–SiO2 one.
All bulk samples were studied by the FTIR spectroscopy and the X-ray diffractometry while thin films were also investigated by the electron microscopy.
In the IR spectra of Al2O3–TiO2 samples, as well as gels and coatings, bands due to the vibrations of AlO bonds of the octahedrally and tetrahedrally coordinated aluminum were observed.
The IR spectra of samples of Al2O3–TiO2–SiO2 system differ from that of Al2O3–TiO2 ones in presence of bands assigned to the SiO bond vibrations and in positions of bands due to AlO bond vibrations. In all spectra of bulk samples and coatings, the positions of TiO bond vibrations were ascribed basing on the IR spectra of the pure anatase and rutile. In this work, samples in form of bulk ones and thin films were obtained using the sol-gel method. The bulk samples were heated at different temperatures (500 °C, 850 °C and 1100 °C) corresponding to the annealing process of coatings, deposited on different substrates by dipping and pulling out samples from the proper sol with the stable speed. Thin films of both Al2O3-TiO2 and Al2O3-TiO2-SiO2 systems were deposited on carbon, steel and titanium substrates in two different ways: as single layers obtained from Al2O3 sol, TiO2 sol and Al2O3 sol or deposited as mixed coatings from Al2O3-TiO2 sol as well as Al2O3-TiO2-SiO2 one. All bulk samples were studied by the FTIR spectroscopy and the X-ray diffractometry while thin films were also investigated by the electron microscopy. In the IR spectra of Al2O3-TiO2 samples, as well as gels and coatings, bands due to the vibrations of AlO bonds of the octahedrally and tetrahedrally coordinated aluminum were observed. The IR spectra of samples of Al2O3-TiO2-SiO2 system differ from that of Al2O3-TiO2 ones in presence of bands assigned to the SiO bond vibrations and in positions of bands due to AlO bond vibrations. In all spectra of bulk samples and coatings, the positions of TiO bond vibrations were ascribed basing on the IR spectra of the pure anatase and rutile. |
Author | Długoń, Elżbieta Adamczyk, Anna |
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Cites_doi | 10.1016/S1466-6049(01)00189-1 10.1016/S0257-8972(97)00603-8 10.1016/j.surfcoat.2005.12.045 10.1111/j.1151-2916.1982.tb10490.x 10.1016/S0022-3093(05)80650-7 |
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Keywords | Thin films Sol–gel method FTIR spectroscopy |
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References | Stabel, Caballero, Espinos, Yubero, Justo, Gonzales-Elipe (bib0005) 1998; 100–101 Mozgawa, Król, Bajda (bib0035) 2009; 693–698 Muroya, Motoki, Shimanoe, Maeda, Haruta, Teraoka, Yamazoe (bib0010) 2006; 201 Yoldas (bib0020) 1975; 54 Padmaja, Anilkumar, Mukindan, Aruldhas, Warrier (bib0030) 2001; 3 Yoldas (bib0025) 1992; 65 Sakka, Kammiya (bib0015) 1992; 147 Mozgawa (10.1016/j.saa.2011.12.018_bib0035) 2009; 693–698 Muroya (10.1016/j.saa.2011.12.018_bib0010) 2006; 201 Stabel (10.1016/j.saa.2011.12.018_bib0005) 1998; 100–101 Yoldas (10.1016/j.saa.2011.12.018_bib0020) 1975; 54 Padmaja (10.1016/j.saa.2011.12.018_bib0030) 2001; 3 Sakka (10.1016/j.saa.2011.12.018_bib0015) 1992; 147 Yoldas (10.1016/j.saa.2011.12.018_bib0025) 1992; 65 |
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► The bulk samples and thin films from Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems. ► Amorphous and homogenous materials up to 500°C. ► Al in... In this work, samples in form of bulk ones and thin films were obtained using the sol-gel method. The bulk samples were heated at different temperatures (500... |
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SubjectTerms | Aluminum Oxide - chemistry FTIR spectroscopy Gels - chemistry Hot Temperature Silicon Dioxide - chemistry Sol–gel method Spectroscopy, Fourier Transform Infrared Thin films Titanium - chemistry |
Title | The FTIR studies of gels and thin films of Al2O3–TiO2 and Al2O3–TiO2–SiO2 systems |
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