A fluorescent hydrogen-bonded organic framework for highly selective sensing of mono-nitrophenol isomers in water
Hydrogen-bonded organic frameworks (HOFs) have great potential as sensing platforms for specific molecular recognition due to their designable structures, high solution processability, and easy regeneration. However, the exploration of fluorescent HOFs for chemical sensing in water remains a challen...
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Published in | Journal of materials chemistry. A, Materials for energy and sustainability Vol. 12; no. 1; pp. 153 - 161 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
Cambridge
Royal Society of Chemistry
19.12.2023
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Subjects | |
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Abstract | Hydrogen-bonded organic frameworks (HOFs) have great potential as sensing platforms for specific molecular recognition due to their designable structures, high solution processability, and easy regeneration. However, the exploration of fluorescent HOFs for chemical sensing in water remains a challenge due to the need to combine excellent photoluminescence performance, high water stability, and specific recognition sites simultaneously. Herein, we report an aggregation-induced emission (AIE) active HOF (termed HOF-TPE-CN) built from a cyano-decorated tetraphenylethylene linker for highly fluorescent sensing of mono-nitrophenol isomers. Owing to the effective AIE effect, HOF-TPE-CN shows a notable enhancement in fluorescence emission, wherein the quantum yield of HOF-TPE-CN was notably increased to 21% compared with that of the TPE-CN ligand in DMF solution (2.89%). Most importantly, this HOF exhibits highly efficient fluorescence quenching toward mono-nitrophenol isomers in water, with a remarkably low detection limit of 0.65 μM. Furthermore, HOF-TPE-CN is more responsive and selective toward mono-nitrophenols compared with a series of homologues. Theoretical calculations combined with X-ray photoelectron spectroscopy revealed that there exist multiple van der Waals and hydrogen-bonding interactions between the trapped nitrophenol molecules and the HOF framework, which form ground-state complexation, resulting in fluorescence quenching by efficient photo-induced electron transfer.
We designed and realized a water-stable and AIE-active HOF (HOF-TPE-CN) with notably enhanced fluorescence emission for achieving highly sensitive and selective sensing of mono-nitrophenols in water. |
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AbstractList | Hydrogen-bonded organic frameworks (HOFs) have great potential as sensing platforms for specific molecular recognition due to their designable structures, high solution processability, and easy regeneration. However, the exploration of fluorescent HOFs for chemical sensing in water remains a challenge due to the need to combine excellent photoluminescence performance, high water stability, and specific recognition sites simultaneously. Herein, we report an aggregation-induced emission (AIE) active HOF (termed HOF-TPE-CN) built from a cyano-decorated tetraphenylethylene linker for highly fluorescent sensing of mono-nitrophenol isomers. Owing to the effective AIE effect, HOF-TPE-CN shows a notable enhancement in fluorescence emission, wherein the quantum yield of HOF-TPE-CN was notably increased to 21% compared with that of the TPE-CN ligand in DMF solution (2.89%). Most importantly, this HOF exhibits highly efficient fluorescence quenching toward mono-nitrophenol isomers in water, with a remarkably low detection limit of 0.65 μM. Furthermore, HOF-TPE-CN is more responsive and selective toward mono-nitrophenols compared with a series of homologues. Theoretical calculations combined with X-ray photoelectron spectroscopy revealed that there exist multiple van der Waals and hydrogen-bonding interactions between the trapped nitrophenol molecules and the HOF framework, which form ground-state complexation, resulting in fluorescence quenching by efficient photo-induced electron transfer.
We designed and realized a water-stable and AIE-active HOF (HOF-TPE-CN) with notably enhanced fluorescence emission for achieving highly sensitive and selective sensing of mono-nitrophenols in water. Hydrogen-bonded organic frameworks (HOFs) have great potential as sensing platforms for specific molecular recognition due to their designable structures, high solution processability, and easy regeneration. However, the exploration of fluorescent HOFs for chemical sensing in water remains a challenge due to the need to combine excellent photoluminescence performance, high water stability, and specific recognition sites simultaneously. Herein, we report an aggregation-induced emission (AIE) active HOF (termed HOF-TPE-CN) built from a cyano-decorated tetraphenylethylene linker for highly fluorescent sensing of mono-nitrophenol isomers. Owing to the effective AIE effect, HOF-TPE-CN shows a notable enhancement in fluorescence emission, wherein the quantum yield of HOF-TPE-CN was notably increased to 21% compared with that of the TPE-CN ligand in DMF solution (2.89%). Most importantly, this HOF exhibits highly efficient fluorescence quenching toward mono-nitrophenol isomers in water, with a remarkably low detection limit of 0.65 μM. Furthermore, HOF-TPE-CN is more responsive and selective toward mono-nitrophenols compared with a series of homologues. Theoretical calculations combined with X-ray photoelectron spectroscopy revealed that there exist multiple van der Waals and hydrogen-bonding interactions between the trapped nitrophenol molecules and the HOF framework, which form ground-state complexation, resulting in fluorescence quenching by efficient photo-induced electron transfer. |
Author | Wang, Yu-Bo Qian, Guodong Jiang, Chenghao Li, Bin Lin, Yu-Xin Wang, Jia-Xin |
AuthorAffiliation | State Key Laboratory of Silicon and Advanced Semiconductor Materials Zhejiang University School of Materials Science and Engineering |
AuthorAffiliation_xml | – name: State Key Laboratory of Silicon and Advanced Semiconductor Materials – name: School of Materials Science and Engineering – name: Zhejiang University |
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Notes | Electronic supplementary information (ESI) available: Additional graphics (Fig. S1-S21), tables (Tables S1 and S2) and calculation methods. See DOI https://doi.org/10.1039/d3ta05309a |
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SubjectTerms | Chemical perception Chemoreception Electron transfer Emissions Fluorescence Hydrogen Hydrogen bonding Isomers Nitrophenol Photoelectron spectroscopy Photoelectrons Photoluminescence Photons Quenching Recognition Water stability X ray photoelectron spectroscopy |
Title | A fluorescent hydrogen-bonded organic framework for highly selective sensing of mono-nitrophenol isomers in water |
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