Influence of the ultrasonic-assisted synthesis on Al distribution in a MOR zeolite: from gel to resulting material
Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. The organization of Al atoms both in the synthesis gel and zeolite product was investigated. Although both methods of th...
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| Published in | New journal of chemistry Vol. 45; no. 41; pp. 19294 - 1933 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Royal Society of Chemistry
25.10.2021
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| Abstract | Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. The organization of Al atoms both in the synthesis gel and zeolite product was investigated. Although both methods of the gel activation resulted in a similar transformation of Al and Si source according to NMR spectroscopy, stirring provided a significantly higher fraction of AlSiAl sequences in the gel compared to the ultrasonic pretreatment. These sequences were transferred to the zeolite product and were more populated in the conventionally prepared mordenite. Al atoms of AlSiAl sequences face different channels and mainly behave as single Al atoms, but they can also form Al pairs or close unpaired Al atoms, observed for the first time for mordenite.
Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. |
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| AbstractList | Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. The organization of Al atoms both in the synthesis gel and zeolite product was investigated. Although both methods of the gel activation resulted in a similar transformation of Al and Si source according to NMR spectroscopy, stirring provided a significantly higher fraction of AlSiAl sequences in the gel compared to the ultrasonic pretreatment. These sequences were transferred to the zeolite product and were more populated in the conventionally prepared mordenite. Al atoms of AlSiAl sequences face different channels and mainly behave as single Al atoms, but they can also form Al pairs or close unpaired Al atoms, observed for the first time for mordenite. Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. The organization of Al atoms both in the synthesis gel and zeolite product was investigated. Although both methods of the gel activation resulted in a similar transformation of Al and Si source according to NMR spectroscopy, stirring provided a significantly higher fraction of AlSiAl sequences in the gel compared to the ultrasonic pretreatment. These sequences were transferred to the zeolite product and were more populated in the conventionally prepared mordenite. Al atoms of AlSiAl sequences face different channels and mainly behave as single Al atoms, but they can also form Al pairs or close unpaired Al atoms, observed for the first time for mordenite. Two Al-rich mordenite samples were prepared by the same synthesis procedure except for the activation of the gel for which classical stirring and ultrasonic pretreatment was used. |
| Author | Tabor, Edyta Brus, Jiri Klein, Petr Kornas, Agnieszka Dedecek, Jiri Mlekodaj, Kinga Urbanova, Martina Pashkova, Veronika Brabec, Libor Olszowka, Joanna E |
| AuthorAffiliation | v.v.i. Heyrovského nám. 1888 v.v.i. Dolejškova 2155/3 J. Heyrovský Institute of Physical Chemistry of the CAS Institute of Macromolecular Chemistry of the CAS |
| AuthorAffiliation_xml | – name: Institute of Macromolecular Chemistry of the CAS – name: J. Heyrovský Institute of Physical Chemistry of the CAS – name: v.v.i. Dolejškova 2155/3 – name: v.v.i. Heyrovského nám. 1888 |
| Author_xml | – sequence: 1 givenname: Joanna E surname: Olszowka fullname: Olszowka, Joanna E – sequence: 2 givenname: Veronika surname: Pashkova fullname: Pashkova, Veronika – sequence: 3 givenname: Agnieszka surname: Kornas fullname: Kornas, Agnieszka – sequence: 4 givenname: Jiri surname: Dedecek fullname: Dedecek, Jiri – sequence: 5 givenname: Jiri surname: Brus fullname: Brus, Jiri – sequence: 6 givenname: Martina surname: Urbanova fullname: Urbanova, Martina – sequence: 7 givenname: Edyta surname: Tabor fullname: Tabor, Edyta – sequence: 8 givenname: Petr surname: Klein fullname: Klein, Petr – sequence: 9 givenname: Libor surname: Brabec fullname: Brabec, Libor – sequence: 10 givenname: Kinga surname: Mlekodaj fullname: Mlekodaj, Kinga |
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| Cites_doi | 10.1021/jp053217u 10.3390/catal9030248 10.1016/j.micromeso.2014.09.056 10.1021/acs.jpcc.9b03620 10.1016/0144-2449(85)90078-8 10.1016/j.micromeso.2014.02.039 10.1016/j.jmr.2009.07.009 10.1021/acs.jpcc.5b03289 10.1021/acsomega.0c05655 10.3390/cryst8010020 10.1021/cr4001513 10.1135/cccc20010685 10.1016/j.jcat.2010.03.013 10.1002/mrc.984 10.1016/j.ssnmr.2016.12.013 10.1006/jmre.1999.1717 10.1016/S1387-1811(01)00307-9 10.1016/j.jcat.2014.06.024 10.1080/01614940.2012.632662 10.1016/j.micromeso.2011.05.004 10.1016/S0167-2991(01)80259-7 10.1021/acscatal.7b01273 10.1021/acsami.0c12293 10.1016/j.cplett.2006.09.081 10.1016/S0926-2040(00)00061-8 10.1246/cl.1983.1547 10.1021/acs.cgd.8b00402 10.1016/j.apcata.2010.06.026 10.1038/s42004-020-0268-3 10.1016/S0021-9517(02)93697-3 10.1007/s11244-009-9271-8 10.1007/s10934-012-9598-6 10.1021/cm2032515 10.1021/cm301629a 10.1016/j.jcat.2015.10.010 10.1039/B203966B 10.1016/j.jcat.2016.09.025 10.1039/C9CY00929A 10.1016/j.jcat.2004.08.001 10.1002/cssc.201801959 10.1016/j.ultsonch.2019.04.020 10.1021/acscatal.6b01771 10.1021/acs.jpcc.8b07343 10.1039/C5CC02670A 10.1021/acs.chemmater.6b00181 |
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| Notes | COO 27 acetonitrile adsorption. See DOI 29 Electronic supplementary information (ESI) available: SEM images of mordenites prepared by US assisted synthesis (MOR-U), and by a standard approach (MOR-R) 10.1039/d1nj00685a Al DQ coherence followed for recoupling periods ranging from 200 to 2000 μs; concentration of SiOHAl calculated based on the intensity of the band at 3613 cm Si MAS NMR spectrum of MOR-U (a), and MOR-R (b); comparison of 1 Al DQF MAS NMR spectra of Al(CH 3 the build-up of Al MAS NMR and on FTIR spectra of evacuated H-forms of MOR-R and MOR-U, and after d |
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| SubjectTerms | Aluminum NMR spectroscopy Pretreatment Silicon Stirring Synthesis Zeolites |
| Title | Influence of the ultrasonic-assisted synthesis on Al distribution in a MOR zeolite: from gel to resulting material |
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