Rational design and microwave-assisted synthesis of a novel terthiophene derivative for facile preparation of binder-free polymer/metal oxide-based binary composite electrodes with high electrochemical performance

In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically desi...

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Published inNew journal of chemistry Vol. 46; no. 13; pp. 6134 - 6149
Main Authors Yi it, Deniz, Güllü, Mustafa
Format Journal Article
LanguageEnglish
Published CAMBRIDGE Royal Soc Chemistry 28.03.2022
Royal Society of Chemistry
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Abstract In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically designed to fabricate homogeneous and chemically stable redox-active composite electrodes for pseudocapacitor applications. Poly(3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (PSDOGA) was electrochemically deposited on stainless steel substrates and modified with TiO 2 and V 2 O 5 particles via a simple, efficient and low-cost process without any polymeric binder. Cyclic voltammetry (CV), galvanostatic charge/discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques were used to study the pseudocapacitive properties of PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composites in both three-electrode and two-electrode cell configurations. PSDOGA/TiO 2 and PSDOGA/V 2 O 5 composites delivered high specific capacitances of 396.4 Fg −1 and 444.5 Fg −1 , respectively, at 2.5 mA cm −2 current density in single electrode measurements. Symmetrical supercapacitor devices assembled by using PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composite electrodes exhibited satisfactory energy (78 W h kg −1 and 94.8 W h kg −1 ) and power (700 W kg −1 and 736 W kg −1 ) densities with good charge/discharge characteristics at a large operating voltage of 1.85 V. Furthermore, symmetric type supercapacitor cells achieved an excellent capacitance retention of 87% and 90% for 12 500 consecutive galvanic charge/discharge cycles at a constant current density of 2.5 mA cm −2 . The experimental results revealed that the cooperation between conducting polymer film and metal oxide particles not only greatly enhanced the capacitive performances, but also improved the long-term charge/discharge stability of the redox-active electrode materials. A simple and effective approach was reported for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials.
AbstractList In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically designed to fabricate homogeneous and chemically stable redox-active composite electrodes for pseudocapacitor applications. Poly(3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (PSDOGA) was electrochemically deposited on stainless steel substrates and modified with TiO 2 and V 2 O 5 particles via a simple, efficient and low-cost process without any polymeric binder. Cyclic voltammetry (CV), galvanostatic charge/discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques were used to study the pseudocapacitive properties of PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composites in both three-electrode and two-electrode cell configurations. PSDOGA/TiO 2 and PSDOGA/V 2 O 5 composites delivered high specific capacitances of 396.4 Fg −1 and 444.5 Fg −1 , respectively, at 2.5 mA cm −2 current density in single electrode measurements. Symmetrical supercapacitor devices assembled by using PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composite electrodes exhibited satisfactory energy (78 W h kg −1 and 94.8 W h kg −1 ) and power (700 W kg −1 and 736 W kg −1 ) densities with good charge/discharge characteristics at a large operating voltage of 1.85 V. Furthermore, symmetric type supercapacitor cells achieved an excellent capacitance retention of 87% and 90% for 12 500 consecutive galvanic charge/discharge cycles at a constant current density of 2.5 mA cm −2 . The experimental results revealed that the cooperation between conducting polymer film and metal oxide particles not only greatly enhanced the capacitive performances, but also improved the long-term charge/discharge stability of the redox-active electrode materials. A simple and effective approach was reported for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials.
In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically designed to fabricate homogeneous and chemically stable redox-active composite electrodes for pseudocapacitor applications. Poly(3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (PSDOGA) was electrochemically deposited on stainless steel substrates and modified with TiO 2 and V 2 O 5 particles via a simple, efficient and low-cost process without any polymeric binder. Cyclic voltammetry (CV), galvanostatic charge/discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques were used to study the pseudocapacitive properties of PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composites in both three-electrode and two-electrode cell configurations. PSDOGA/TiO 2 and PSDOGA/V 2 O 5 composites delivered high specific capacitances of 396.4 Fg −1 and 444.5 Fg −1 , respectively, at 2.5 mA cm −2 current density in single electrode measurements. Symmetrical supercapacitor devices assembled by using PSDOGA/TiO 2 and PSDOGA/V 2 O 5 binder-free binary composite electrodes exhibited satisfactory energy (78 W h kg −1 and 94.8 W h kg −1 ) and power (700 W kg −1 and 736 W kg −1 ) densities with good charge/discharge characteristics at a large operating voltage of 1.85 V. Furthermore, symmetric type supercapacitor cells achieved an excellent capacitance retention of 87% and 90% for 12 500 consecutive galvanic charge/discharge cycles at a constant current density of 2.5 mA cm −2 . The experimental results revealed that the cooperation between conducting polymer film and metal oxide particles not only greatly enhanced the capacitive performances, but also improved the long-term charge/discharge stability of the redox-active electrode materials.
In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2 ':5 ',2 ''-terthiophen-3 '-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically designed to fabricate homogeneous and chemically stable redox-active composite electrodes for pseudocapacitor applications. Poly(3-[(2,2 ':5 ',2 ''-terthiophen-3 '-yl)]-2-cyanoacrylic acid) (PSDOGA) was electrochemically deposited on stainless steel substrates and modified with TiO2 and V2O5 particles via a simple, efficient and low-cost process without any polymeric binder. Cyclic voltammetry (CV), galvanostatic charge/discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques were used to study the pseudocapacitive properties of PSDOGA/TiO2 and PSDOGA/V2O5 binder-free binary composites in both three-electrode and two-electrode cell configurations. PSDOGA/TiO2 and PSDOGA/V2O5 composites delivered high specific capacitances of 396.4 Fg(-1) and 444.5 Fg(-1), respectively, at 2.5 mA cm(-2) current density in single electrode measurements. Symmetrical supercapacitor devices assembled by using PSDOGA/TiO2 and PSDOGA/V2O5 binder-free binary composite electrodes exhibited satisfactory energy (78 W h kg(-1) and 94.8 W h kg(-1)) and power (700 W kg(-1) and 736 W kg(-1)) densities with good charge/discharge characteristics at a large operating voltage of 1.85 V. Furthermore, symmetric type supercapacitor cells achieved an excellent capacitance retention of 87% and 90% for 12 500 consecutive galvanic charge/discharge cycles at a constant current density of 2.5 mA cm(-2). The experimental results revealed that the cooperation between conducting polymer film and metal oxide particles not only greatly enhanced the capacitive performances, but also improved the long-term charge/discharge stability of the redox-active electrode materials.
In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode materials. The novel electropolymerizable thiophene monomer, 3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (SDOGA), was specifically designed to fabricate homogeneous and chemically stable redox-active composite electrodes for pseudocapacitor applications. Poly(3-[(2,2′:5′,2′′-terthiophen-3′-yl)]-2-cyanoacrylic acid) (PSDOGA) was electrochemically deposited on stainless steel substrates and modified with TiO2 and V2O5 particles via a simple, efficient and low-cost process without any polymeric binder. Cyclic voltammetry (CV), galvanostatic charge/discharge (GCD) and electrochemical impedance spectroscopy (EIS) techniques were used to study the pseudocapacitive properties of PSDOGA/TiO2 and PSDOGA/V2O5 binder-free binary composites in both three-electrode and two-electrode cell configurations. PSDOGA/TiO2 and PSDOGA/V2O5 composites delivered high specific capacitances of 396.4 Fg−1 and 444.5 Fg−1, respectively, at 2.5 mA cm−2 current density in single electrode measurements. Symmetrical supercapacitor devices assembled by using PSDOGA/TiO2 and PSDOGA/V2O5 binder-free binary composite electrodes exhibited satisfactory energy (78 W h kg−1 and 94.8 W h kg−1) and power (700 W kg−1 and 736 W kg−1) densities with good charge/discharge characteristics at a large operating voltage of 1.85 V. Furthermore, symmetric type supercapacitor cells achieved an excellent capacitance retention of 87% and 90% for 12 500 consecutive galvanic charge/discharge cycles at a constant current density of 2.5 mA cm−2. The experimental results revealed that the cooperation between conducting polymer film and metal oxide particles not only greatly enhanced the capacitive performances, but also improved the long-term charge/discharge stability of the redox-active electrode materials.
Author Güllü, Mustafa
Yi it, Deniz
AuthorAffiliation Department of Chemistry
Sö ütözü
Lokman Hekim University
Department of Basic Pharmaceutical Sciences
Faculty of Pharmacy
Faculty of Science
Ankara University
Besevler
AuthorAffiliation_xml – name: Department of Chemistry
– name: Lokman Hekim University
– name: Ankara University
– name: Sö ütözü
– name: Besevler
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– name: Faculty of Science
Author_xml – sequence: 1
  givenname: Deniz
  surname: Yi it
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  givenname: Mustafa
  surname: Güllü
  fullname: Güllü, Mustafa
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CitedBy_id crossref_primary_10_1002_ente_202301076
crossref_primary_10_1016_j_est_2023_107477
crossref_primary_10_1016_j_envres_2023_115285
crossref_primary_10_1039_D3NJ03557C
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Keywords SUPERCAPACITOR ELECTRODES
POLYPYRROLE
V2O5
POLYTHIOPHENE
ACTIVE MATERIALS
NANOSTRUCTURES
REDOX SUPERCAPACITORS
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Electronic supplementary information (ESI) available. See DOI
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Snippet In this study, a simple and effective method was presented for the preparation of binder-free conducting polymer/metal oxide binary composite electrode...
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SubjectTerms Charge density
Chemistry
Chemistry, Multidisciplinary
Composite materials
Conducting polymers
Current density
Discharge
Electrochemical analysis
Electrochemical impedance spectroscopy
Electrode materials
Electrodes
Metal oxides
Physical Sciences
Polymer films
Polymers
Science & Technology
Stainless steels
Substrates
Supercapacitors
Titanium dioxide
Vanadium pentoxide
Title Rational design and microwave-assisted synthesis of a novel terthiophene derivative for facile preparation of binder-free polymer/metal oxide-based binary composite electrodes with high electrochemical performance
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