Structural, magnetic and magnetoelectric studies of BaTiO3:Co nanocomposite films formed by ion-beam methods

Thin-film samples of ferroelectric barium titanate (BaTiO3) with cobalt nanoparticles were obtained by using either ion implantation or ion beam sputtering deposition (IBSD) techniques. The samples were characterized using X-ray diffraction, transmission electron microscopy, magnetometry and ferroma...

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Published inNuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms Vol. 331; pp. 163 - 167
Main Authors Khalitov, N.I., Valeev, V.F., Faizrakhmanov, I.A., Khaibullin, R.I., Gorbatova, P.A., Parfenov, V.V., Prikhodko, K.E., Roddatis, V.V., Presniakov, M.Yu, Maksutoglu, M., Mikailzade, F.A.
Format Journal Article
LanguageEnglish
Published 15.07.2014
Subjects
Annealing
Barium titanates
Cobalt
Ion beam sputtering
Ion beams
Ion implantation
Nanoparticles
Nanostructure
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Abstract Thin-film samples of ferroelectric barium titanate (BaTiO3) with cobalt nanoparticles were obtained by using either ion implantation or ion beam sputtering deposition (IBSD) techniques. The samples were characterized using X-ray diffraction, transmission electron microscopy, magnetometry and ferromagnetic resonance to investigate the efficiency of above ion-beam methods in the synthesis of magnetoelectric nanocomposite materials. Our structural studies show that high-fluence implantation with Co+ ions results in the formation of cobalt nanoparticles with mean size of 5nm in thin surface layer of monocrystalline plate of BaTiO3. On the other hand, larger nanoparticles of cobalt with sizes from 5 up to 40nm are formed in polycrystalline BaTiO3 matrix only after high-temperature annealing of BaTiO3_Co composite film prepared by IBSD method. Both types of thin-film nanocomposite samples have similar magnetic hysteresis curves in the sample plane. However Co-implanted BaTiO3 reveals strong uniaxial magnetic anisotropy for out-of-plane orientation, while BaTiO3_Co nanocomposite film demonstrates almost isotropic magnetic response. Strong magnetoelectric effect are observed in Co-implanted BaTiO3, and no magnetoelectric coupling are detected in BaTiO3_Co nanocomposite film formed by IBSD with subsequent high-temperature annealing.
AbstractList Thin-film samples of ferroelectric barium titanate (BaTiO3) with cobalt nanoparticles were obtained by using either ion implantation or ion beam sputtering deposition (IBSD) techniques. The samples were characterized using X-ray diffraction, transmission electron microscopy, magnetometry and ferromagnetic resonance to investigate the efficiency of above ion-beam methods in the synthesis of magnetoelectric nanocomposite materials. Our structural studies show that high-fluence implantation with Co+ ions results in the formation of cobalt nanoparticles with mean size of 5nm in thin surface layer of monocrystalline plate of BaTiO3. On the other hand, larger nanoparticles of cobalt with sizes from 5 up to 40nm are formed in polycrystalline BaTiO3 matrix only after high-temperature annealing of BaTiO3_Co composite film prepared by IBSD method. Both types of thin-film nanocomposite samples have similar magnetic hysteresis curves in the sample plane. However Co-implanted BaTiO3 reveals strong uniaxial magnetic anisotropy for out-of-plane orientation, while BaTiO3_Co nanocomposite film demonstrates almost isotropic magnetic response. Strong magnetoelectric effect are observed in Co-implanted BaTiO3, and no magnetoelectric coupling are detected in BaTiO3_Co nanocomposite film formed by IBSD with subsequent high-temperature annealing.
Author Gorbatova, P.A.
Prikhodko, K.E.
Mikailzade, F.A.
Presniakov, M.Yu
Parfenov, V.V.
Khalitov, N.I.
Khaibullin, R.I.
Roddatis, V.V.
Faizrakhmanov, I.A.
Maksutoglu, M.
Valeev, V.F.
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SubjectTerms Annealing
Barium titanates
Cobalt
Ion beam sputtering
Ion beams
Ion implantation
Nanoparticles
Nanostructure
Title Structural, magnetic and magnetoelectric studies of BaTiO3:Co nanocomposite films formed by ion-beam methods
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