Structural and optical properties of Er3+-doped willemite glass-ceramics from waste materials
The production of Er3+-doped willemite glass-ceramic using waste soda lime silica (SLS) glass was reported in this study. The precursor glass and glass-ceramics were prepared using conventional melt-quenching technique with empirical formula (Er2O3)x[(ZnO)0.5(SLS)0.5]1-x where x=1wt.% and sintered a...
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Published in | Optik (Stuttgart) Vol. 127; no. 24; pp. 11698 - 11705 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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Elsevier GmbH
01.12.2016
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Abstract | The production of Er3+-doped willemite glass-ceramic using waste soda lime silica (SLS) glass was reported in this study. The precursor glass and glass-ceramics were prepared using conventional melt-quenching technique with empirical formula (Er2O3)x[(ZnO)0.5(SLS)0.5]1-x where x=1wt.% and sintered at various temperatures. The trend of density and the linear shrinkage of the glass-ceramic samples were increased with the progression of sintering temperature. The crystallization behaviour and surface morphology of the glass-ceramics was studied using X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). It was revealed that at a lower sintering temperature (700°C), the stable state of α-willemite (α-Zn2SiO4) phase was formed. Fourier transform infrared (FTIR) spectroscopy reveals that the presence of different functional groups in the samples. Three transition states of excitation were shown in UV–visible (UV–vis) spectra which arise from the ground state 4I15/2 to the excited states 4F7/2, 2H11/2, 4F9/2. Broad green emission at 557nm under excitation 385nm was obtained. These spectra reveal that the luminescence of the samples was increased with the progression of sintering temperature due to the presence of Er3+ ions into the willemite crystal. Such luminescence of glass and glass-ceramics are expected to have potential applications in optoelectronic devices. |
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AbstractList | The production of Er3+-doped willemite glass-ceramic using waste soda lime silica (SLS) glass was reported in this study. The precursor glass and glass-ceramics were prepared using conventional melt-quenching technique with empirical formula (Er2O3)x[(ZnO)0.5(SLS)0.5]1-x where x=1wt.% and sintered at various temperatures. The trend of density and the linear shrinkage of the glass-ceramic samples were increased with the progression of sintering temperature. The crystallization behaviour and surface morphology of the glass-ceramics was studied using X-ray diffraction (XRD) and field emission scanning electron microscopy (FESEM). It was revealed that at a lower sintering temperature (700°C), the stable state of α-willemite (α-Zn2SiO4) phase was formed. Fourier transform infrared (FTIR) spectroscopy reveals that the presence of different functional groups in the samples. Three transition states of excitation were shown in UV–visible (UV–vis) spectra which arise from the ground state 4I15/2 to the excited states 4F7/2, 2H11/2, 4F9/2. Broad green emission at 557nm under excitation 385nm was obtained. These spectra reveal that the luminescence of the samples was increased with the progression of sintering temperature due to the presence of Er3+ ions into the willemite crystal. Such luminescence of glass and glass-ceramics are expected to have potential applications in optoelectronic devices. |
Author | Effendy, Nuraidayani Zaid, Mohd Hafiz Mohd Abdul Wahab, Zaidan Mohamed Kamari, Halimah Hj. Ab Aziz, Sidek Matori, Khamirul Amin |
Author_xml | – sequence: 1 givenname: Nuraidayani surname: Effendy fullname: Effendy, Nuraidayani email: aidayanieffendy@gmail.com organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia – sequence: 2 givenname: Zaidan surname: Abdul Wahab fullname: Abdul Wahab, Zaidan organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia – sequence: 3 givenname: Halimah surname: Mohamed Kamari fullname: Mohamed Kamari, Halimah email: halimahmk@upm.edu.my organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia – sequence: 4 givenname: Khamirul Amin surname: Matori fullname: Matori, Khamirul Amin organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia – sequence: 5 givenname: Sidek surname: Hj. Ab Aziz fullname: Hj. Ab Aziz, Sidek organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia – sequence: 6 givenname: Mohd Hafiz Mohd surname: Zaid fullname: Zaid, Mohd Hafiz Mohd organization: Department of Physics, Faculty of Science, Universiti Putra Malaysia, 43400, UPM, Serdang, Selangor, Malaysia |
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Snippet | The production of Er3+-doped willemite glass-ceramic using waste soda lime silica (SLS) glass was reported in this study. The precursor glass and... |
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SubjectTerms | Erbium oxide Glass-ceramic Photoluminescence Willemite |
Title | Structural and optical properties of Er3+-doped willemite glass-ceramics from waste materials |
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